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Cas:105-87-3
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inquiryProduct description: Product name Geranyl acetate CAS number 105-87-3 Assay ≥99% Appearance Colorless transparent liquid Capacity 200mt/year Application Flavour and fragrance
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Geranyl acetate Basic information Product Name: Geranyl acetate Synonyms: (2E)-3,7-Dimethyl-2,6-octadienyl acetate;(E)-3,7-Dimethyl-2,6-octadien-1-yl acetate;2,6-dimethyl-2,6-octadiene-8
Cas:105-87-3
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Cas:105-87-3
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inquiryAppearance:Colourless neat Storage:2-8°C Package:200kg/Drum Application:Perfumery, flavoring Transportation:Express/Sea/Air Port:Any port in China
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inquiryGeranyl acetate CAS:105-87-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia
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high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 100% |
With pyridine In tetrahydrofuran at 0 - 20℃; Acetylation; | 100% |
With pyridine; dmap at 20℃; for 1h; Acetylation; | 99% |
Conditions | Yield |
---|---|
With dilithium tetra(tert-butyl)zincate In toluene at 0℃; for 1h; Inert atmosphere; | 100% |
With N,N'-bismesityl-imidazol-2-ylidene In tetrahydrofuran at 20℃; for 1h; | 99% |
1,3-bis(2,4,6-trimethyl-phenyl)imidazol-2-ylidene In tetrahydrofuran at 20℃; for 1h; | 99% |
Conditions | Yield |
---|---|
With Candida antarctica lipase B at 50℃; for 4h; Molecular sieve; Ionic liquid; Green chemistry; Enzymatic reaction; | 99.9% |
With hydroquinone at 120℃; Temperature; Reagent/catalyst; | 99.2% |
With 1,3-propanesultone; N-ethyl-N-methylbutan-1-amine; toluene-4-sulfonic acid at 110℃; for 2h; Temperature; Reagent/catalyst; | 97% |
Conditions | Yield |
---|---|
With potassium fluoride on basic alumina In toluene for 2h; | 98% |
With dmap; triethylamine at 0℃; for 3h; | 94% |
With pyridine at 0 - 20℃; for 5h; | 84% |
With pyridine | 72% |
Conditions | Yield |
---|---|
With pyridine; dmap; acetic anhydride | 98% |
With acetic acid at 110℃; for 2h; | 96.8% |
Multi-step reaction with 2 steps 1: pyridine; phosphorus tribromoide View Scheme |
Conditions | Yield |
---|---|
With N,N'-biscyclohexyl-imidazol-2-ylidene; 5A molecular sieve In tetrahydrofuran at 20℃; for 0.5h; | 97% |
With caesium carbonate at 125℃; for 25h; | 97% |
With heterogeneous zinc/imidazole catalyst at 90℃; for 5h; Inert atmosphere; Schlenk technique; | 94% |
Conditions | Yield |
---|---|
With caesium carbonate at 125℃; for 30h; | 96% |
Nerol
Geraniol
acetic anhydride
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With Tri-n-octylamine; dmap at 125℃; for 1h; Heating / reflux; | 92% |
Conditions | Yield |
---|---|
With aluminum oxide at 25 - 30℃; for 1h; | 91% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
In acetic anhydride for 6h; Heating; | 90% |
Geraniol
benzylidene 1,1-diacetate
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With potassium carbonate at 90℃; for 16h; | 89% |
(E)-1-O-acetyl-4-chloro-3-methyl-2-buten-1-ol
3-methyl-2-butenylmagnesium chloride
A
3,7-dimethyl-2E,6-octadien-1-yl acetate
B
lavandulyl acetate
Conditions | Yield |
---|---|
With CuCN*2LiCl In tetrahydrofuran at 0℃; for 0.3h; | A 8% B 88% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 24h; | 88% |
Conditions | Yield |
---|---|
With pyridine for 24h; Ambient temperature; | 87% |
3,7-dimethylocta-1,6-dien-3-ol
acetic acid
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone for 1h; Heating; | 87% |
geranyl 2-tetrahydropyranyl ether
acetic anhydride
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With zirconium(IV) chloride In acetonitrile at 20℃; for 0.166667h; | 83% |
With titanium tetrachloride In dichloromethane at 0 - 25℃; for 6h; Acetylation; | 80% |
geranyl 2-tetrahydropyranyl ether
ethyl acetate
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With indium (III) iodide for 12h; Heating; | 78% |
(E)-1-(methoxymethoxy)-3,7-dimethylocta-2,6-diene
ethyl acetate
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With indium (III) iodide for 15h; Heating; | 78% |
Geraniol
2,2'-bipyridyl-6-yl acetate
A
3,7-dimethyl-2E,6-octadien-1-yl acetate
B
<2,2'-bipyridin>-6(1H)-one
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile for 72h; Ambient temperature; | A 77% B n/a |
1-acetyl-2,3-dihydro-5,7-dinitroindole
Geraniol
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
In acetonitrile for 16h; UV-irradiation; | 72% |
3,7-dimethylocta-1,6-dien-3-ol
acetic anhydride
A
3,7-dimethyl-2E,6-octadien-1-yl acetate
B
linalool acetate
Conditions | Yield |
---|---|
With scandium tris(trifluoromethanesulfonate) at -20℃; for 2.5h; | A 8 % Spectr. B 68% |
With scandium tris(trifluoromethanesulfonate) at -20℃; for 2.5h; | A 8% B 68% |
With trimethylsilyl trifluoromethanesulfonate at -20 - 0℃; Product distribution; |
2-methyl-3-buten-2-ol
3-methyl-3-buten-1-yl acetate
A
3,7-dimethyl-2E,6-octadien-1-yl acetate
B
1-Acetoxy-3,7-dimethyl-6-octen-3-ol
C
7-Methyl-3-methylen-6-octenolacetat
D
Acetic acid (E)-3,7-dimethyl-octa-3,6-dienyl ester
Conditions | Yield |
---|---|
With methanesulfonic acid In nitromethane at 0℃; for 1.5h; | A n/a B 61% C n/a D n/a |
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 120℃; for 50h; | 58% |
3,7-dimethylocta-1,6-dien-3-ol
acetonitrile
A
3,7-dimethyl-2E,6-octadien-1-yl acetate
B
(E)-N‐(3,7-dimethylocta‐2,6‐dien‐1‐yl)acetamide
Conditions | Yield |
---|---|
With acetic anhydride; CoCl2 at 80℃; for 20h; | A n/a B 52% |
geranyl phenyl sulfide
acetic anhydride
acetic acid
A
7-methyl-3-methene-1,6-octadiene
B
3,7-dimethyl-2E,6-octadien-1-yl acetate
C
(Z)-ocimene
Conditions | Yield |
---|---|
With lithium acetate; copper diacetate; copper at 85 - 90℃; | A n/a B 43% C n/a |
trans-7-acetoxy-1,1,5-trimethyl-2-phenylselenyloct-5-en-1-ol
A
3,7-dimethyl-2E,6-octadien-1-yl acetate
B
2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenylcyclohexane
Conditions | Yield |
---|---|
formic acid In dichloromethane at 0℃; for 2.5h; | A 14.6% B 19.3% |
formic acid In dichloromethane at 0℃; for 2.5h; Product distribution; various acid catalysts; | A 14.6% B 19.3% |
2-(1,1-dimethyl-allyl)-3-methyl-butane-1,3-diol
acetic anhydride
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With pyridine at 160℃; Erhitzen des Reaktionsprodukts auf 350grad; |
3,7-dimethyl-2E,6-octadien-1-yl acetate
n-butylmagnesium iodide
(6E)-2,6-dimethyl-2,6-dodecadiene
Conditions | Yield |
---|---|
With ortho-N,N-dimethylamino benzylthiolatocopper(I) In tetrahydrofuran; toluene at -30℃; for 0.0833333h; | 100% |
With [CuSC6H4(CH2NMe2)-2]3 In tetrahydrofuran at -30℃; for 0.0833333h; | |
2-[(dimethylamino)methyl]-1-thiophenolato-copper(I) In tetrahydrofuran at -30℃; for 0.0833333h; Yield given; |
3,7-dimethyl-2E,6-octadien-1-yl acetate
n-butylmagnesium iodide
2,6-dimethyl-6-ethenyl-2-decene
Conditions | Yield |
---|---|
With ortho-N,N-dimethylamino benzylthiolatocopper(I) In diethyl ether at 0℃; for 2h; Product distribution; Mechanism; var. arenethiolatocopper(I) cat., solvent, time, temp.; | 100% |
With ortho-N,N-dimethylamino benzylthiolatocopper(I) In diethyl ether; toluene at 0℃; for 2h; | 100% |
With [CuSC6H4(CH2NMe2)-2]3 In diethyl ether at 0℃; for 2h; | |
2-[(dimethylamino)methyl]-1-thiophenolato-copper(I) In diethyl ether at 0℃; for 2h; Yield given; |
3,7-dimethyl-2E,6-octadien-1-yl acetate
(E)-5-(3,3-dimethyloxiran-2-yl)-3-methylpent-2-enyl acetate
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at -20 - 20℃; for 2h; | 100% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0℃; for 1h; | 99% |
With sodium acetate In dichloromethane at 0℃; for 2h; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In methanol at 25℃; for 0.166667h; | 99% |
With methanol at 80℃; for 6h; Inert atmosphere; Schlenk technique; | 99% |
With methanol; oxo[hexa(trifluoroacetato)]tetrazinc for 12h; Reflux; Inert atmosphere; | 96% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
(2E)-acetic acid 6-bromo-7-hydroxy-3,7-dimethyl-oct-2-enyl ester
Conditions | Yield |
---|---|
With N-Bromosuccinimide In 1,4-dioxane; water at 0 - 20℃; for 5h; | 98% |
With [bis(acetoxy)iodo]benzene; water; lithium bromide In acetonitrile at -10℃; for 0.25h; Inert atmosphere; regioselective reaction; | 70% |
With N-Bromosuccinimide In water; tert-butyl alcohol | |
With N-Bromosuccinimide; water In 1,2-dimethoxyethane at 0℃; for 2h; | |
With N-Bromosuccinimide; water In tetrahydrofuran for 0.75h; |
morpholine
3,7-dimethyl-2E,6-octadien-1-yl acetate
(E)-4-(3,7-dimethylocta-2,6-dienyl)morpholine
Conditions | Yield |
---|---|
bis(η3-allyl-μ-chloropalladium(II)); 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene In toluene at 20℃; for 20h; | 98% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
(E)-6,7-dibromo-3,7-dimethyloct-2-en-1-yl acetate
Conditions | Yield |
---|---|
With 3-(trimethylsilyl)-2-oxazolidinone; hydrogen bromide In dichloromethane at 0℃; for 0.5h; | 97% |
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; cetyltrimethylammonim bromide In dichloromethane; chloroform | 95% |
With [bis(acetoxy)iodo]benzene; lithium bromide In acetonitrile at 0℃; for 0.0833333h; Reagent/catalyst; Inert atmosphere; Molecular sieve; chemoselective reaction; | 91% |
With [bis(acetoxy)iodo]benzene; lithium bromide In acetonitrile at 0℃; for 0.0833333h; Inert atmosphere; Molecular sieve; regioselective reaction; | 91% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
chloroform
(2,2-dichloro-3,3-dimethylcycloprop-1-yl)-3-methylpent-2-en-1-yl acetate
Conditions | Yield |
---|---|
With potassium hydroxide; tert-butylammonium hexafluorophosphate(V) In benzene at 15℃; for 6h; | 97% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
p-methoxybenzyl chloride
trans-1-(4,8-dimethylnona-3,7-dien-1-yl)-4-methoxybenzene
Conditions | Yield |
---|---|
Stage #1: p-methoxybenzyl chloride With magnesium; ethylene dibromide In tetrahydrofuran at 0 - 25℃; Inert atmosphere; Stage #2: 3,7-dimethyl-2E,6-octadien-1-yl acetate With lithium chloride; copper dichloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; iso-butanol at -10 - 0℃; for 3.33333h; Inert atmosphere; | 97% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
essigsaeure-<(E,R)-6,7-dihydroxy-3,7-dimethyl-2-octenyl>ester
Conditions | Yield |
---|---|
With methanesulfonamide; AD-mix-β In tert-butyl alcohol at 0℃; for 24h; Sharpless Dihydroxylation; enantioselective reaction; | 96% |
With potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; potassium hexacyanoferrate(III) In water; tert-butyl alcohol at 4℃; for 24h; Sharpless Dihydroxylation; Inert atmosphere; | 85% |
With AD-mi-β; water; tert-butyl alcohol at 0℃; for 15h; | 80% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
A
7-chloro-3,7-dimethyl-2E-octen-1-yl acetate
B
1,7-dichloro-3,7-dimethyloct-2(E)-ene
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at -78℃; for 0.25h; | A 96% B 2% |
With hydrogenchloride In diethyl ether at -78℃; | A 68% B 5% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
sodium tetraphenyl borate
(2E)-1-phenyl-3,7-dimethyl-2,6-octadiene
Conditions | Yield |
---|---|
With metalloprotein-inspired polymeric imidazole/palladium In water; isopropyl alcohol at 50℃; for 4h; | 96% |
With poly[(N-vinylimidazole)-co-(N-isopropylacrylamide)]-based palladium catalyst In water; isopropyl alcohol at 50℃; for 4h; | 96% |
With chloro-[2-(9-phenyl-1,10-phenanthrolin-2-yl)phenyl]palladium In methanol at 50℃; for 48h; Inert atmosphere; | 64% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
bis(pinacol)diborane
(E)-2-(3,7-dimethylocta-2,6-dien-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel(0); tricyclohexylphosphine In ethyl acetate at 60℃; for 12h; Inert atmosphere; stereoselective reaction; | 96% |
With bis(1,5-cyclooctadiene)nickel (0); tricyclohexylphosphine In ethyl acetate at 60℃; for 10.5h; Inert atmosphere; | 54% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
(2E,6E)-3,7-dimethyl-8-oxoocta-2,6-dien-1-yl acetate
Conditions | Yield |
---|---|
With selenium(IV) oxide In ethanol Reflux; Inert atmosphere; regioselective reaction; | 95% |
With selenium(IV) oxide In ethanol for 1h; Heating; | 82% |
Stage #1: 3,7-dimethyl-2E,6-octadien-1-yl acetate With selenium(IV) oxide; salicylic acid In dichloromethane at 0 - 20℃; for 29h; Oxidation; Stage #2: With manganese(IV) oxide In dichloromethane at 0 - 20℃; Oxidation; Further stages.; | 73% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
1,7-dichloro-3,7-dimethyloct-2(E)-ene
Conditions | Yield |
---|---|
With acetyl chloride In ethanol at 30℃; for 0.25h; Markovnikov hydrochlorination; | 95% |
Conditions | Yield |
---|---|
With potassium hydroxide; tert-butylammonium hexafluorophosphate(V) In benzene at 15℃; for 6h; | 95% |
Conditions | Yield |
---|---|
Stage #1: ethylmagnesium bromide With copper(II) thiophene-2-carboxylate; 1-(chloro(pyrrolidin-1-yl)methylene)pyrrolidinium tetrafluoroborate In diethyl ether at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: 3,7-dimethyl-2E,6-octadien-1-yl acetate In diethyl ether for 1.25h; Inert atmosphere; | 95% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
O-(p-toluenesulfonyl)-N-methylhydroxylamine
(E)-3-methyl-5-(1,3,3-trimethylaziridin-2-yl)pent-2-en-1-yl acetate
Conditions | Yield |
---|---|
With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]} In 2,2,2-trifluoroethanol at 20℃; for 1h; regioselective reaction; | 94% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; N-ethyl-N,N-diisopropylamine In water; isopropyl alcohol at 80℃; for 0.166667h; microwave irradiation; | 93% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
B
(2E)-6-chloro-3,7-dimethyl-2,7-octadienyl acetate
Conditions | Yield |
---|---|
With N-chloro-succinimide; selenenyl bromide In dichloromethane at 20℃; | A n/a B 93% |
3,7-dimethyl-2E,6-octadien-1-yl acetate
(2R*,3R*)-2,3-epoxy-3,7-dimethyl-6-octenyl acetate
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In water; acetonitrile at 70℃; for 24h; | 93% |
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