CAS No.3779-61-1,(E)-3,7-dimethylocta-1,3,6-triene Suppliers

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Nanjing Raymon Biotech Co., Ltd.

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1,3,6-Octatriene,3,7-dimethyl-, (3E)-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the package

1,3,6-Octatriene,3,7-dimethyl-, (3E)-

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1,3,6-Octatriene,3,7-dimethyl-, (3E)-

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Synthetic route

: 94987-59-4
2-methyl-4-(3-methyl-3-sulfolen-2-yl)-2-butene

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
In pyridine at 125℃; for 7h;	85%

: 53776-92-4
(E)-3-methyl-5-bromopenta-1,3-diene

: 38614-36-7
2-methylpropen-1-ylmagnesium bromide

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
With dilithium tetrachlorocuprate In tetrahydrofuran; 1,2-dimethoxyethane at 0 - 20℃; for 18.75h; Grignard reaction; optical yield given as %de;	68%

: 106-24-1
Geraniol

A: 78-70-6
3,7-dimethylocta-1,6-dien-3-ol

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
With germacrene A synthase from Nostoc sp. PCC7120 (NS1) In terpene synthase buffer at 25℃; for 18h; Enzymatic reaction;	A 66% B 25% C 9%

...Expand

: 106-24-1
Geraniol

A: 3338-55-4
(Z)-ocimene

B: 3779-61-1
trans ocimene

C: 138-86-3
limonene.

Conditions

Conditions	Yield
With sesquiterpene synthases Cop4 from Coprinus cinereus In terpene synthase buffer at 25℃; for 18h; Enzymatic reaction;	A 61% B 9.1% C 23.7%

...Expand

: 2-(geranyloxy)-3,5,7-trimethyltropone

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

D: 2885-58-7
3,5,7-trimethyltropolone

Conditions

Conditions	Yield
at 180℃; pyrolysis;	A 30% B 8% C 49% D n/a
at 140℃; pyrolysis;	A 23% B 12% C 36% D n/a

...Expand

: 106-24-1
Geraniol

A: 78-70-6
3,7-dimethylocta-1,6-dien-3-ol

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

D: 138-86-3
limonene.

Conditions

Conditions	Yield
With sesquiterpene synthases Cop6 from Coprinus cinereus In terpene synthase buffer at 25℃; for 18h; Enzymatic reaction;	A 34.6% B 9.2% C 7.11% D 45%

...Expand

: 3,5,7-trimethyl-2-(neryloxy)tropone

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
at 140℃;	A 29% B 9% C 27%
at 140℃; pyrolysis;	A 29% B 9% C 27%

...Expand

: 106-24-1
Geraniol

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

D: 586-62-9
Terpinolene

E: 138-86-3
limonene.

Conditions

Conditions	Yield
With tin(ll) chloride In dimethyl sulfoxide at 139.84℃; for 2h;	A 27% B 24% C 17% D 10% E 22%

...Expand

: 2-(geranyl-oxy)tropone

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

D: 3-(1,5-dimethyl-1-vinyl-4-hexenyl)tropolone

Conditions

Conditions	Yield
at 180℃; for 15h; Further byproducts given;	A 15% B 6% C 19% D n/a
at 180℃; for 0.25h; pyrolysis; Further byproducts given;	A 15% B 6% C 19% D n/a
at 180℃; for 15h; pyrolysis; Further byproducts given;	A 15 % Chromat. B 6 % Chromat. C 19 % Chromat. D n/a

...Expand

: 105-87-3
3,7-dimethyl-2E,6-octadien-1-yl acetate

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran for 48h; Product distribution; Ambient temperature; other dienylacetate, var. basic reagents;	A 41 % Chromat. B n/a C n/a
With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 16h; Inert atmosphere;

...Expand

: 105-87-3
3,7-dimethyl-2E,6-octadien-1-yl acetate

A: 3338-55-4
(Z)-ocimene

B: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); 2-Propynylzinc bromide In tetrahydrofuran for 3h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

: 562-74-3
TERPINEN-4-OL

A: 3338-55-4
(Z)-ocimene

B: 3779-61-1
trans ocimene

C: 99-87-6
4-methylisopropylbenzene

D: 586-82-3
(+/-)-4-isopropyl-1-methyl-3-cyclohexen-1-ol

E: 470-67-7
4-methyl-1-propan-2-yl-7-oxabicyclo[2.2.1]heptane

: neoisothujyl alcohol

Conditions

Conditions	Yield
With abietic acid In water at 100℃; Product distribution; sealed tube;	A n/a B n/a C 25 % Chromat. D 24 % Chromat. E 11 % Chromat. F 17 % Chromat.

...Expand

: 82859-38-9
(2E)-1-iodo-3,7-dimethylocta-2,6-diene

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

D: 138-86-3
limonene.

Conditions

Conditions	Yield
With triethylamine In hexane at 25℃; for 6h; Irradiation; Yield given. Yields of byproduct given;
With triethylamine In hexane at 25℃; for 6h; Product distribution; Irradiation;

...Expand

: 89111-64-8
neryl iodide

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

D: 586-62-9
Terpinolene

E: 138-86-3
limonene.

Conditions

Conditions	Yield
With triethylamine In hexane at 25℃; for 6h; Product distribution; Irradiation;
With triethylamine In tetrahydrofuran at 50℃; for 2h; Product distribution; Irradiation; also in the presence of CuCl; similar product distribution by photoirradiation of geranyl iodide;

...Expand

: 89111-64-8
neryl iodide

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3779-61-1
trans ocimene

C: 586-62-9
Terpinolene

D: 138-86-3
limonene.

Conditions

Conditions	Yield
With triethylamine In hexane at 25℃; for 6h; Irradiation; Yield given. Yields of byproduct given;

...Expand

: O-nerylisourea

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Pd(0)-bis(diphenylphosphino)ethane In N,N-dimethyl-formamide at 120℃; for 5h; Yield given. Yields of byproduct given;

...Expand

: O-geranylisourea

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Pd(0)-bis(diphenylphosphino)ethane In N,N-dimethyl-formamide at 120℃; for 5h; Yield given. Yields of byproduct given;

...Expand

: 115-95-7
linalool acetate

A: 123-35-3
7-methyl-3-methene-1,6-octadiene

B: 3338-55-4
(Z)-ocimene

C: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran Product distribution; Mechanism; other allylic acetates; var. solv.; also in presence var. bases and organometallic reagents; kinetic isotope effect;

...Expand

: 106-24-1
Geraniol

A: 78-70-6
3,7-dimethylocta-1,6-dien-3-ol

B: 123-35-3
7-methyl-3-methene-1,6-octadiene

C: 3779-61-1
trans ocimene

D: 98-55-5
terpineol

Conditions

Conditions	Yield
With sulfuric acid; potassium tartrate In ethanol at 50℃; for 4h; pH=3; Product distribution; Further Variations:; pH-values; Reaction partners; Reagents; Temperatures; Hydrolysis;

...Expand

: 106-25-2
Nerol

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 82 percent 2: NaI / acetone / 1 h / 0 - 2 °C 3: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme

: 106-24-1
Geraniol

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 86 percent 2: NaI / acetone / 1 h / 0 - 2 °C 3: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme

: 20536-36-1
neryl chloride

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: NaI / acetone / 1 h / 0 - 2 °C 2: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme

: 5389-87-7
1-chloro-3,7-dimethylocta-2,6-diene

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: NaI / acetone / 1 h / 0 - 2 °C 2: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme

: 5392-40-5
(E/Z)-3,7-dimethyl-2,6-octadienal

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 2: 82 percent 3: NaI / acetone / 1 h / 0 - 2 °C 4: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme
Multi-step reaction with 4 steps 2: 86 percent 3: NaI / acetone / 1 h / 0 - 2 °C 4: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme

: 80-56-8, 177698-18-9
Pinene

A: 3338-55-4
(Z)-ocimene

B: 3779-61-1
trans ocimene

C: 138-86-3
limonene.

Conditions

Conditions	Yield
at 336.84℃; Kinetics; Mechanism; Temperature;

...Expand

: 62054-49-3
ethyl (E)-3-formyl-2-butenoate

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 0 °C 1.2: -78 - 20 °C 2.1: lithium aluminium tetrahydride / diethyl ether / 1 h / Inert atmosphere; Reflux 3.1: phosphorus tribromide / diethyl ether / 1 h / 0 °C / Inert atmosphere 4.1: dilithium tetrachlorocuprate / tetrahydrofuran; 1,2-dimethoxyethane / 18.75 h / 0 - 20 °C View Scheme

: 1572-08-3
(E)-3-methylpenta-2,4-dien-1-ol

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: phosphorus tribromide / diethyl ether / 1 h / 0 °C / Inert atmosphere 2: dilithium tetrachlorocuprate / tetrahydrofuran; 1,2-dimethoxyethane / 18.75 h / 0 - 20 °C View Scheme

: 37850-26-3
methyl-3 pentadiene-2,4 oate d'ethyle E

: 3779-61-1
trans ocimene

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / diethyl ether / 1 h / Inert atmosphere; Reflux 2: phosphorus tribromide / diethyl ether / 1 h / 0 °C / Inert atmosphere 3: dilithium tetrachlorocuprate / tetrahydrofuran; 1,2-dimethoxyethane / 18.75 h / 0 - 20 °C View Scheme

: 763-10-0
geranyl diphosphate

A: 99-83-2
p-mentha-1,5-diene

B: 123-35-3
7-methyl-3-methene-1,6-octadiene

C: 3338-55-4
(Z)-ocimene

D: 3779-61-1
trans ocimene

E: 586-62-9
Terpinolene

F: 138-86-3
limonene.

Conditions

Conditions	Yield
With recombinant (+)-cadinene synthase from Gossypium arboreum; magnesium chloride; D,L-dithiothreitol In pentane at 25℃; for 24h; pH=7.5; HEPES buffer; Enzymatic reaction;

...Expand

: 3779-61-1
trans ocimene

: 20426-48-6
(E)-1-(3-chlorophenyl)-3-phenylprop-2-en-1-one

: (3-chlorophenyl)[3-methyl-2-(3-methylbut-2-en-1-yl)-6-phenylcyclohex-3-en-1-yl]methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	74%

: 3779-61-1
trans ocimene

: 614-47-1
1,3-diphenyl-propen-3-one

: [3-methyl-2-(3-methylbut-2-en-1-yl)-6-phenylcyclohex-3-en-1-yl](phenyl)methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 24h; Reagent/catalyst; Temperature; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	72%

: 3779-61-1
trans ocimene

: 156723-02-3
(+/-)-12-hydroxy-9(10->20)-5aH-abeo-abieta-1(10),8(9),12(13)-triene-11,14-dione

: C30H42O3

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In toluene at 0 - 50℃; for 11.5h; Inert atmosphere;	71%

: 3779-61-1
trans ocimene

: 2960-55-6
(E)-3-(4-nitrophenyl)-1-phenylprop-2-en-1-one

: [3-methyl-2-(3-methylbut-2-en-1-yl)-6-(4-nitrophenyl)cyclohex-3-en-1-yl](phenyl)methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In dichloromethane at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	71%

: 3779-61-1
trans ocimene

: 80783-99-9, 124931-15-3, 113474-86-5
N-methoxy-N-methylcinnamamide

: (1RS,5SR,6RS)-N-methoxy-N,4-dimethyl-5-(3-methylbut-2-en-1-yl)-6-phenylcyclohex-3-ene-1-carboxamide

Conditions

Conditions	Yield
In neat (no solvent) at 140℃; for 72h; Diels-Alder Cycloaddition; Inert atmosphere; Sealed tube; regioselective reaction;	70%

: 3779-61-1
trans ocimene

: 22966-22-9
(E)-1-(4-chlorophenyl)-3-phenyl-2-propen-1-one

: (4-chlorophenyl)[3-methyl-2-(3-methylbut-2-en-1-yl)-6-phenylcyclohex-3-en-1-yl]methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	70%

: 3779-61-1
trans ocimene

: 24721-26-4, 956-04-7, 22252-16-0
4-chlorochalcone

: [3-methyl-2-(3-methylbut-2-en-1-yl)-6-(4-chlorophenyl)cyclohex-3-en-1-yl](phenyl)methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	69%

: 3779-61-1
trans ocimene

: 75927-49-0
pinacol vinylboronate

: (E)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-{(E)-but-2-en-2-yl}-6-methylhepta-1,5-diene

Conditions

Conditions	Yield
With (η6-naphthalene)(η4-1,5-cyclooctadiene)ruthenium(0) In benzene at 30℃; for 1h; Inert atmosphere; Schlenk technique;	67%

: 3779-61-1
trans ocimene

: C15H10ClNO3

: [3-methyl-2-(3-methylbut-2-en-1-yl)-6-(3-nitrophenyl)cyclohex-3-en-1-yl](phenyl)methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	64%

: 3779-61-1
trans ocimene

: 14802-30-3
(E)-1-(4-methylphenyl)-3-phenyl-2-propen-1-one

: [3-methyl-2-(3-methylbut-2-en-1-yl)-6-phenylcyclohex-3-en-1-yl](4-tolyl)methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	62%

: 3779-61-1
trans ocimene

: 22966-09-2
(2E)-3-(4-bromophenyl)-1-phenylprop-2-en-1-one

: [3-methyl-2-(3-methylbut-2-en-1-yl)-6-(4-bromophenyl)cyclohex-3-en-1-yl](phenyl)methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	62%

: 3779-61-1
trans ocimene

: (S)-12-hydroxy-9(10->20)-5aH-abeo-abieta-1(10),8(9),12(13)-triene-11,14-dione

: 142132-39-6
(+)-perovskone

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 50℃; for 11.5h; Inert atmosphere;	57%

: 3779-61-1
trans ocimene

: 72758-69-1, 2403-27-2, 22966-23-0
(E)-1-(4-bromophenyl)-3-phenylprop-2-en-1-one

: (4-bromophenyl)[3-methyl-2-(3-methylbut-2-en-1-yl)-6-phenylcyclohex-3-en-1-yl]methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	56%

: 3779-61-1
trans ocimene

: 1443009-32-2
C20H24O6

: 1443009-33-3
C30H40O6

Conditions

Conditions	Yield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene at 150℃; for 5h; Inert atmosphere; Sealed tube;	55%
In toluene at 150℃; for 5h; Inert atmosphere; Sealed tube;	55%

: 21264-30-2, 90243-59-7, 14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 3779-61-1
trans ocimene

: (((CH3)2CCHCH2CHC(CH3)CHCH2OCOCH3)PdCl)2

Conditions

Conditions	Yield
With lithium acetate; acetic acid In N,N,N,N,N,N-hexamethylphosphoric triamide a soln. of (MeCN)2PdCl2 in HMPA followed by trans-ocimene was added under N2 to a soln. of LiOAc*2H2O in AcOH and HMPA (total HMPA:water=10/1 v/v), mixt. was stirred at room temp. for 8 h; reaction mixt. was extd. with benzene, ext. washed with water, dried over CaCl2, solvent was removed under reduced pressure, residue purified by column chromy. on SiO2 with 10/3 benzene-EtOAc; elem. anal.;	54%

Yield

With lithium acetate; acetic acid In N,N,N,N,N,N-hexamethylphosphoric triamide a soln. of (MeCN)2PdCl2 in HMPA followed by trans-ocimene was added under N2 to a soln. of LiOAc*2H2O in AcOH and HMPA (total HMPA:water=10/1 v/v), mixt. was stirred at room temp. for 8 h; reaction mixt. was extd. with benzene, ext. washed with water, dried over CaCl2, solvent was removed under reduced pressure, residue purified by column chromy. on SiO2 with 10/3 benzene-EtOAc; elem. anal.;

54%

: 3779-61-1
trans ocimene

: C17H18O4

: C27H34O4

Conditions

Conditions	Yield
In toluene at 150℃; for 7h; Diels-Alder Cycloaddition; Inert atmosphere; Sealed tube; stereoselective reaction;	54%

: 3779-61-1
trans ocimene

: 76015-59-3
C15H14O3

: 958296-41-8
bolivianine

Conditions

Conditions	Yield
In toluene at 150℃; for 2h; Inert atmosphere; Sealed tube;	52%
In toluene at 150℃; for 2h; Inert atmosphere; Sealed tube;	52%

: 3779-61-1
trans ocimene

: 22966-24-1
(E)-1-(3-methoxyphenyl)-3-phenylprop-2-en-1-one

: (3-methoxyphenyl)[3-methyl-2-(3-methylbut-2-en-1-yl)-6-phenylcyclohex-3-en-1-yl]methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In dichloromethane at 28℃; for 6h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	52%

: 3779-61-1
trans ocimene

: 156723-02-3
(+/-)-12-hydroxy-9(10->20)-5aH-abeo-abieta-1(10),8(9),12(13)-triene-11,14-dione

: (+/-)-perovskone

: C30H42O3

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate In dichloromethane at 0 - 50℃; for 8.5h; Inert atmosphere;	A 50% B 15%

...Expand

: 21264-30-2, 90243-59-7, 14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 3779-61-1
trans ocimene

: (((CH3)2CCHCH2CHC(CH3)CHCH2OH)PdCl)2

B: (((CH3)2CCHCH2CH(OH)C(CH3)CHCH2)PdCl)2

Conditions

Conditions	Yield
With water In acetone trans-ocimene was added under N2 to a soln. of (MeCN)2PdCl2 in water and acetone (1:5 v/v), mixt. was stirred at -5°C for 8 h; reaction mixt. was extd. with benzene, ext. washed with water, dried over CaCl2, solvent was removed under reduced pressure, residue purified by column chromy. on SiO2 (eluent 5/1 benzene-EtOAc); elem. anals.;	A 26% B 49%
With water In N,N,N,N,N,N-hexamethylphosphoric triamide trans-ocimene was added under N2 to a soln. of (MeCN)2PdCl2 in water and (Me2N)3PO (1:5 v/v), mixt. was stirred at -5°C for 8 h; reaction mixt. was extd. with benzene, ext. washed with water, dried over CaCl2, solvent was removed under reduced pressure, residue purified by column chromy. on SiO2 (eluent 5/1 benzene-EtOAc); elem. anals.;	A 37% B 12%
With water In N,N-dimethyl-formamide trans-ocimene was added under N2 to a soln. of (MeCN)2PdCl2 in water and DMF (1:5 v/v), mixt. was stirred at -5°C for 8 h; reaction mixt. was extd. with benzene, ext. washed with water, dried over CaCl2, solvent was removed under reduced pressure, residue purified by column chromy. on SiO2 (eluent 5/1 benzene-EtOAc); elem. anals.;	A 30% B 35%

...Expand

: 14371-10-9
(E)-3-phenylpropenal

: 3779-61-1
trans ocimene

: (1SR,2SR,3aRS,7SR,7aSR)-4-methyl-7-phenyl-2-(prop-1-en-2-yl)-2,3,3a,6,7,7a-hexahydro-1H-indene-1-ol

Conditions

Conditions	Yield
In neat (no solvent) at 140℃; for 72h; Inert atmosphere; Sealed tube;	45%

: 3779-61-1
trans ocimene

: 22252-14-8, 72758-77-1, 4224-87-7
(E)-3-(4-methylphenyl)-1-phenyl-2-propen-1-one

: [3-methyl-2-(3-methylbut-2-en-1-yl)-6-(4-tolyl)cyclohex-3-en-1-yl](phenyl)methanone

Conditions

Conditions	Yield
With aluminum tri-bromide In toluene at 28℃; for 3h; Diels-Alder Cycloaddition; Inert atmosphere; diastereoselective reaction;	44%

: 920282-22-0, 53623-19-1
bis(acetonitrile)palladium(II) bromide

: 3779-61-1
trans ocimene

: (((CH3)2CCHCH2CHC(CH3)CHCH2OH)PdBr)2

B: (((CH3)2CCHCH2CH(OH)C(CH3)CHCH2)PdBr)2

Conditions

Conditions	Yield
With water In N,N,N,N,N,N-hexamethylphosphoric triamide trans-ocimene was added under N2 to a soln. of (MeCN)2PdBr2 in water and (Me2N)3PO (1:10 v/v), mixt. was stirred at room temp. for 10 h; reaction mixt. was extd. with benzene, ext. washed with water, dried over CaCl2, solvent was removed under reduced pressure, residue purified by column chromy. on SiO2;	A 35% B 19%

...Expand

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