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img _fcksaAppearance:liquid Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and Dye
Cas:138-86-3
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inquiryProName: Cinene CasNo: 138-86-3 Molecular Formula: C10H16 Appearance: Look at the detailed information Application: intermediates DeliveryTime: according to the clients requirement PackAge
Cas:138-86-3
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inquiryOffer 2kinds of Dipentene Appearance:clear to pale yellow liquid with a lemon-like odor Storage:Keep in a cool, dry, dark location in a tightly sealed container or cylinder. Keep away from incompatible materials, ignition sources and untrained indi
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Product name DL-Limonene Cas number 138-86-3 EINECS NO. 205-341-0 Appearance:Clear colorless to yellow liquid
We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:138-86-3
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Cas:138-86-3
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:200kg/drum, or as per your request. Application:Used as Pharmaceutical Intermedia
Cas:138-86-3
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inquiryProduct name: Dipentene(CAS:138-86-3) CAS No.:138-86-3 Molecule Formula:C10H16 Molecule Weight:136.23 Purity: 92.0% Package: 175kg/drum Description:Clear transparent liquid Manufacture Standards:Enterprise Standard
Cas:138-86-3
Min.Order:1 Kilogram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
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Hangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special chemicals and other fine chemicals. We could give you: 1.Best quality in your re
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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Cas:138-86-3
Min.Order:1 Kilogram
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inquiryRaw material ,higher purity, support by origional factory, fully large stock Stable. Flammable. Incompatible with strong oxidizing agents. Pleasant, pine-like; lemon-like.Used as raw materials for synthetic rubber, spices, and solvents Used as ena
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Cas:138-86-3
Min.Order:10 Kilogram
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inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and
Conditions | Yield |
---|---|
In liquid sulphur dioxide Ambient temperature; | A 97% B 3% |
In liquid sulphur dioxide Rate constant; Mechanism; Kinetics; Ambient temperature; | A 97% B 3% |
Conditions | Yield |
---|---|
With lithium; biphenyl In 1,2-dimethoxyethane for 4h; Heating; other solvents, other temperatures, other reaction times, other catalysts; | 96% |
With lithium In tetrahydrofuran for 82h; Heating; | 86% |
With isopropyl alcohol In toluene at 110℃; for 24h; Inert atmosphere; chemoselective reaction; | 68 %Chromat. |
Carvone
limonene.
Conditions | Yield |
---|---|
With H2SiEt2; tris(pentafluorophenyl)borate In dichloromethane | 86% |
With boron trifluoride diethyl etherate; sodium cyanoborohydride In tetrahydrofuran for 3h; Ambient temperature; | 50% |
(2Z,6E)-3,7-dimethyl-8-trimethylsilyl-2,6-octadien-1-ol
limonene.
Conditions | Yield |
---|---|
With titanium tetrachloride; N-methylaniline In dichloromethane at -23℃; for 1h; | 77% |
(2Z,6E)-3,7-dimethyl-8-tributylstannyl-2,6-octadien-1-ol
limonene.
Conditions | Yield |
---|---|
With titanium tetrachloride; N-methylaniline In dichloromethane at -23℃; for 2h; | 73% |
Conditions | Yield |
---|---|
With methanol; toluene-4-sulfonic acid at 25℃; for 18h; Inert atmosphere; Sealed tube; UV-irradiation; | 73% |
limonene.
Conditions | Yield |
---|---|
With biphenyl; lithium In 1,2-dimethoxyethane for 16h; Heating; | 71% |
Beta-pinene
A
Pinene
B
1-methyl-4-isopropenylbenzene
C
camphene
E
limonene.
Conditions | Yield |
---|---|
With hydrogen at 140℃; for 4h; Temperature; Reagent/catalyst; | A n/a B n/a C n/a D 65.6% E n/a |
Conditions | Yield |
---|---|
With sesquiterpene synthases Cop4 from Coprinus cinereus In terpene synthase buffer at 25℃; for 18h; Enzymatic reaction; | A 61% B 9.1% C 23.7% |
Acetic acid (2Z,6E)-3,7-dimethyl-8-tributylstannanyl-octa-2,6-dienyl ester
limonene.
Conditions | Yield |
---|---|
With methylaluminium bis(trifluoroacetate) In hexane at 25℃; for 21h; | 51% |
(-)-Carvone
limonene.
Conditions | Yield |
---|---|
Mechanism; Wolff-Kishner-red.; | 50% |
Wolff-Kishner-red.; |
Conditions | Yield |
---|---|
With terephthalonitrile In acetonitrile Irradiation; Further byproducts given; | A 21% B n/a C n/a D 50% |
α-terpinyl chloride
zinc diacetate
A
Terpinolene
B
terpinyl acetate
C
limonene.
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 40℃; for 80h; Product distribution; Heating; other solvents and temperatures; | A n/a B 48% C n/a |
With pyridine In dichloromethane at 40℃; for 80h; Heating; Yields of byproduct given; | A n/a B 48% C n/a |
(4-Isopropenyl-cyclohex-1-enylmethyl)-trimethyl-silane
limonene.
Conditions | Yield |
---|---|
With cesium fluoride In dimethyl sulfoxide at 100℃; for 0.5h; | 46% |
Geraniol
A
3,7-dimethylocta-1,6-dien-3-ol
B
(Z)-ocimene
C
trans ocimene
D
limonene.
Conditions | Yield |
---|---|
With sesquiterpene synthases Cop6 from Coprinus cinereus In terpene synthase buffer at 25℃; for 18h; Enzymatic reaction; | A 34.6% B 9.2% C 7.11% D 45% |
neryl chloride
A
Terpinolene
B
α-terpinyl chloride
C
limonene.
Conditions | Yield |
---|---|
With 1,3-bis[3,5-bis(trifluoromethyl)phenyl]urea; sodium hydrogencarbonate In chloroform-d1 at 25℃; for 24h; Inert atmosphere; Sealed tube; | A 17.47% B 43.15% C 19.28% |
3,7-dimethylocta-1,6-dien-3-ol
A
3,7-Dimethyl-octa-1,3,6-trien
B
Terpinolene
C
limonene.
Conditions | Yield |
---|---|
With rhenium(VII) oxide In toluene at 100℃; for 24h; | A 32% B 22% C 43% |
With sulfuric acid In toluene at 100℃; for 24h; | A 11% B 25% C 20% |
Conditions | Yield |
---|---|
With sodium sulfide; Aliquat 336 In water; benzene for 1h; Ambient temperature; | 41% |
Beta-pinene
A
Pinene
B
Terpinolene
C
1-methyl-4-isopropyl-1,3-cyclohexadiene
D
crithmene
dl-camphene
F
limonene.
Conditions | Yield |
---|---|
aluminum oxide at 232℃; Thermodynamic data; Mechanism; isomerization; | A 27% B n/a C n/a D n/a E 38% F n/a |
With pyridine; aluminum oxide at 232℃; Thermodynamic data; Mechanism; isomerization, variation of partial pressure of pyridine; | A 11% B n/a C n/a D n/a E 28% F n/a |
Pinene
acetic acid
A
Terpinolene
B
camphene
C
terpinyl acetate
D
limonene.
Conditions | Yield |
---|---|
With 1-(3-sulfonic acid)propyl-3-poly(ethylene glycol) octadecylamine polyoxyethylene ether tetrafluoroborate at 30℃; for 10h; Catalytic behavior; Concentration; Reagent/catalyst; Temperature; Time; | A 13.99 %Chromat. B 17.23 %Chromat. C 35.7% D 16.55 %Chromat. |
terephthalonitrile
methanol
(-)-α-pinene
acetonitrile
cis-6-(4-cyanophenyl)-4-(1-methoxy-1-methylethyl)-1-methylcyclohexene
trans-6-(4-cyanophenyl)-4-(1-methoxy-1-methylethyl)-1-methylcyclohexene
D
limonene.
Conditions | Yield |
---|---|
With biphenyl at 10℃; for 72h; Mechanism; Irradiation; other monoterpenes; | A 23% B 28% C 35% D n/a |
Conditions | Yield |
---|---|
With terephthalonitrile; biphenyl In methanol for 72h; Irradiation; | A 35% B n/a |
A
Beta-pinene
B
Pinene
C
Terpinolene
D
crithmene
E
limonene.
Conditions | Yield |
---|---|
With SCO7700 protein; sodium chloride; magnesium chloride; 2,2'-piperazine-1,4-diyl-bis-ethanesulfonic acid In pentane at 30℃; for 18h; pH=7.0; Kinetics; Reagent/catalyst; | A 23% B 6% C 29% D 10% E 32% |
trans-terpin
A
Terpinolene
B
terpineol
C
limonene.
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 3.5h; | A 32% B 13% C 27% |
With toluene-4-sulfonic acid In dichloromethane at 20℃; for 3.5h; | A 25% B 10% C 32% |
With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 3.5h; | A 31% B 24% C 21% |
With iron(III) chloride adsorbed on silica gel In dichloromethane at 20℃; for 3.5h; | A 23% B 25% C 30% |
Conditions | Yield |
---|---|
under 13 - 20 Torr; Inert atmosphere; Pyrolysis; Reflux; | A 24.82% B 30.92% C 26.06% |
3,7-dimethyl-oct-6-enal
A
7-methyl-3-methene-1,6-octadiene
B
3,7-Dimethyl-octa-1,3,6-trien
C
1-methyl-4-isopropyl-1,3-cyclohexadiene
D
3,8-p-Menthadien
E
limonene.
Conditions | Yield |
---|---|
With aluminum oxide; carbon dioxide In hexane at 190℃; Supercritical conditions; | A 15.8% B 6.2% C 11.9% D 30.8% E 5.2% |
Pinene
A
Terpinolene
B
1-methyl-4-isopropyl-1,3-cyclohexadiene
C
camphene
D
crithmene
E
limonene.
Conditions | Yield |
---|---|
With Conventional beta-zeolite at 70℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Reflux; | A 8.7% B 7.2% C 19.7% D 4.4% E 30.7% |
With mesoporous beta type zeolite at 70℃; for 0.5h; |
terephthalonitrile
methanol
(-)-α-pinene
cis-6-(4-cyanophenyl)-4-(1-methoxy-1-methylethyl)-1-methylcyclohexene
trans-6-(4-cyanophenyl)-4-(1-methoxy-1-methylethyl)-1-methylcyclohexene
C
limonene.
Conditions | Yield |
---|---|
With biphenyl In acetonitrile for 72h; Irradiation; | A 23% B 28% C n/a |
Acetic acid (2Z,6E)-3,7-dimethyl-8-trimethylsilanyl-octa-2,6-dienyl ester
limonene.
Conditions | Yield |
---|---|
With methylaluminium bis(trifluoroacetate) In hexane at 25℃; for 17h; | 28% |
Conditions | Yield |
---|---|
With n-butyllithium; potassium 2-methylbutan-2-olate Mechanism; 1) r.t., 17 h, 2) reflux, 6 h; further reagent: D2O; | 100% |
Multi-step reaction with 3 steps 1: copper (II)-formate; nickel-formate / 175 °C 2: manganese (II)-acetate; lead (II)-acetate / 45 °C / Einleiten von Luft 3: charcoal / 53 Torr View Scheme | |
Multi-step reaction with 3 steps 1: activated copper; nickel / 175 °C 2: manganese (II)-acetate; lead (II)-acetate / 45 °C / Einleiten von Luft 3: charcoal / 53 Torr View Scheme |
Conditions | Yield |
---|---|
With iodine at 250℃; for 1h; Autoclave; Inert atmosphere; | 99.5% |
limonene.
p-menth-1-ene
Conditions | Yield |
---|---|
With fac-[Mn(1,2-bis(di-isopropylphosphino)ethane)(CO)3(CH2CH2CH3)]; hydrogen In diethyl ether at 25℃; under 37503.8 Torr; for 24h; | 99% |
With borohydride exchange resin-nickel boride In methanol for 1h; Heating; | 95% |
With LaNi5 hydride In tetrahydrofuran; methanol for 11h; Ambient temperature; | 88% |
Conditions | Yield |
---|---|
With iron(III) chloride; sodium; ethylenediamine at 50 - 100℃; Inert atmosphere; | 99% |
With hydrogen at 350℃; under 760.051 Torr; | 91% |
With 5 weight% palladium(0) nanoparticles supported on mesoporous natural phosphate In neat (no solvent) for 24h; Reflux; | 88% |
Conditions | Yield |
---|---|
With sodium percarbonate; acetic anhydride In acetic acid butyl ester at 60℃; for 12h; Product distribution / selectivity; | 99% |
With dihydrogen peroxide; sodium acetate; acetic anhydride In toluene at 5 - 25℃; for 5h; Time; Temperature; | 92% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 15℃; for 1.83333h; | 86% |
Conditions | Yield |
---|---|
With C40H56N2RuSi4; hydrogen In toluene at 25℃; under 7600.51 Torr; for 6h; Schlenk technique; Autoclave; | 99% |
With C40H56FeN2Si4(2-); hydrogen In 1,2-dimethoxyethane at 80℃; under 7600.51 Torr; for 10h; Schlenk technique; Autoclave; | 50% |
limonene.
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
Conditions | Yield |
---|---|
With C26H36CoN3O In tetrahydrofuran at 25℃; for 12h; Inert atmosphere; Glovebox; enantioselective reaction; | A 97% B n/a |
3-Mercaptopropyltriethoxysilane
limonene.
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In toluene at 70℃; for 6.5h; Inert atmosphere; | 97% |
With 2,2'-azobis(isobutyronitrile) In toluene at 70℃; for 6h; Inert atmosphere; | 97% |
With 2,2'-azobis(isobutyronitrile) In toluene at 70℃; for 6h; Inert atmosphere; | 97% |
3-Mercaptopropyltriethoxysilane
limonene.
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In toluene at 70℃; for 6h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With oxygen; manganese triacetate; pivalaldehyde In various solvent(s) at 25℃; for 1h; | 96% |
With 1,2-diphenyl-1,1,2,2-tetrahydroperoxyethane; potassium hydroxide In acetonitrile at 20℃; for 0.833333h; | 96% |
With oxygen; sodium hydrogencarbonate; isobutyraldehyde; RuCl2(biox)2 In dichloromethane at 25℃; for 8h; | 92% |
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex at 60℃; for 6h; Inert atmosphere; | 96% |
chloroform
limonene.
4-(1-methyl-2,2-dichlorocyclopropyl)-7,7-dichloro-1-methylbicyclo<4.1.0>heptane
Conditions | Yield |
---|---|
With sodium hydroxide for 3h; Irradiation; ultrasound; | 95% |
ethanol
limonene.
4-(2-ethoxypropan-2-yl)-1-methylcyclohex-1-ene
Conditions | Yield |
---|---|
askanite-bentonite clay at 20℃; for 70h; Addition; Etherification; | 95% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In ethanol at 70℃; for 6h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With fac-tris(2-phenylpyridinato-N,C2')iridium(III); tert-dodecanethiol; potassium carbonate In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; Irradiation; chemoselective reaction; | 93% |
tetraethylammonium acetate
limonene.
A
α-pinene-7-ol acetate
B
carvyl acetate
Conditions | Yield |
---|---|
With palladium diacetate; p-benzoquinone In chloroform at 20℃; Product distribution; Further Variations:; Reagents; | A 90% B 10% |
Conditions | Yield |
---|---|
With disodium tetracarbonylferrate In tetrahydrofuran at 25℃; for 16h; Glovebox; Inert atmosphere; | 90% |
With Benzoylformic acid In Petroleum ether for 18h; Sealed tube; Irradiation; Green chemistry; | 79% |
Conditions | Yield |
---|---|
With 1H-imidazole; sodium periodate; MnCl-TPP-(PEO750)4 In water; acetonitrile at 20℃; for 24h; | 89% |
Stage #1: limonene. With ozone In methanol; dichloromethane at -78℃; for 2.5h; Inert atmosphere; Stage #2: With dimethylsulfide In dichloromethane at -78 - 20℃; for 3h; Inert atmosphere; | 80% |
With oxygen; uranyl acetate In pyridine Irradiation; | |
Multi-step reaction with 2 steps 1: O2 / UO2(OAc)2*2H2O / pyridine / Irradiation 2: benzene / 30 h / Heating View Scheme |
trichloroacetonitrile
limonene.
(E)-1,1,1-Trichloro-4-(4-methyl-cyclohex-3-enyl)-pent-3-en-2-one
Conditions | Yield |
---|---|
With boron trichloride In dichloromethane at -78℃; | 89% |
Conditions | Yield |
---|---|
With 3 Å molecular sieves at 100℃; for 0.166667h; Microwave irradiation; | 89% |
isopropyl alcohol
limonene.
4-(1-isopropoxy-1-methylethyl)-1-methyl-cyclohexene
Conditions | Yield |
---|---|
With iron(III) chloride In dichloromethane at 0 - 20℃; for 1.2h; | 87% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In ethanol at 70℃; for 12h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; (dimethylammonium)[MoO3(Hbpdc)]*1.7H2O at 55℃; for 24h; Solvent; Temperature; Time; regioselective reaction; | A n/a B 86% |
With tert.-butylhydroperoxide; C72H100Mo8N8O26 In decane; α,α,α-trifluorotoluene at 55℃; for 24h; regioselective reaction; | A 76% B 22% |
Stage #1: limonene. With MoO(NtBu)(2,6-iPr2C6H3O)2py In toluene at 20℃; Inert atmosphere; Stage #2: With tert.-butylhydroperoxide In decane; toluene at 90℃; for 4h; Inert atmosphere; | A 26% B 58% |
limonene.
4-chlorobenzohydroximoyl chloride
Conditions | Yield |
---|---|
Stage #1: 4-chlorobenzohydroximoyl chloride With triethylamine Stage #2: limonene. In dichloromethane at 20℃; for 72h; | 85% |
chloroform
limonene.
A
7,7-Dichloro-4-isopropenyl-1-methyl-bicyclo[4.1.0]heptane
B
4-(1-methyl-2,2-dichlorocyclopropyl)-7,7-dichloro-1-methylbicyclo<4.1.0>heptane
Conditions | Yield |
---|---|
With potassium hydroxide; 18-crown-6 ether In dichloromethane at 40℃; for 4h; Yields of byproduct given; | A n/a B 84% |
With potassium hydroxide; p-t-butylcalix<6>arene derivative In dichloromethane at 40℃; for 4h; | A 55% B 17% |
With potassium hydroxide; p-t-butylcalix<6>arene derivative In dichloromethane at 30℃; Rate constant; other catalyst; |
Conditions | Yield |
---|---|
With formic acid; phosphoric acid In dichloromethane at 75℃; | 83% |
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