Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:545-06-2
Min.Order:100 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryCAS No.: 545-06-2 Other Names: Cyanotrichloromethane MF: C2Cl3N EINECS No.: 208-885-7 Place of Origin: China (Mainland) Type: Agrochemical Intermediates Purity: 98% Brand Name: TNJ Application: Agrochemical Interm
Cas:545-06-2
Min.Order:18 Metric Ton
Negotiable
Type:Trading Company
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:545-06-2
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryProduct Name: Trichloroacetonitrile Synonyms: trichloromethylcarbonitrile;Trichlroacetonitrile;TRICHLOROACETONITRILE, 1000MG, NEAT;Trichloroacetonitrile,97%;TRICHLORACETONITRILE;2,2,2-Trichloroacetonitrile;Trichlorocyanomethane;Trichloroacetonitri
Cas:545-06-2
Min.Order:1 Kilogram
FOB Price: $230.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:545-06-2
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:545-06-2
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryProduct name: Trichloroacetonitrile CAS No.:545-06-2 Molecule Formula:C2Cl3N Molecule Weight:144.39 Purity: 98.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard
Cas:545-06-2
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:545-06-2
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Sealed in a cool ,dry and microtherm place , avoid light . Package: 1kg/drum or 25kg/drum or as per your request. Application: pesticide Transportation:By
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:545-06-2
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:545-06-2
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Xiamen Luyunjia Trading Co.,Ltd Package:1kg/bag; 5156kg/drum, or as customer's request. Application:Xiamen Luyunjia Trading Co.,Ltd Transportation:DHL, EMS, FedEx, TNT, AIR, SEA Port:Beijing,Shanghai,Guangzhou ,China main port
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
Cas:545-06-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryin storeAppearance:Colorless - very pale yellow transparent liquid Package:100g Application:Organic Chemicals
Trichloroacetonitrile Basic information Product Name: Trichloroacetonitrile Synonyms: TRIBROMOACETONITRILE;TRICHLOROACETONITRILE;trichloromethyl cyanide;acetonitril
Cas:545-06-2
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryShanghai AngewChemCo., Ltd. is an innovative enterprise on fine chemicals and pharmaceuticals. Based on Shanghai R&D center and Hunan chemical manufacturing plant, we offer chemical research, process development, and large-scale production. Com
Cas:545-06-2
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
Cas:545-06-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryBetterbiochem is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in
Cas:545-06-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryProfile Hebei Ruishun Trade Co.LTD, registered capital of $1 million ,have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center,Seek development by credit reputation. Our products have a large
BaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art
1) Provide costomers with "one-stop"packaging service,from research,development,production,export and so on. 2) We have our own R&D and production base,equipped with advanced production equipment and precision testing the Unitef Stat
Cas:545-06-2
Min.Order:1 Gram
FOB Price: $150.0 / 200.0
Type:Trading Company
inquiryN-{2-[2,2,2-Trichloro-eth-(E)-ylidene-hydrazinocarbonyl]-phenyl}-benzamide
A
2-phenyl-4(3H)-quinazolinone
B
trichloroacetonitrile
Conditions | Yield |
---|---|
at 200 - 240℃; under 1 Torr; | A n/a B 64% |
Conditions | Yield |
---|---|
With trichlorophosphate | |
With phosphorus pentaoxide | |
With phosphorus pentaoxide |
trichloroacetyl-triphenoxyphosphoranyliden-amine
A
phosphoric acid triphenyl ester
B
trichloroacetonitrile
Conditions | Yield |
---|---|
at 300℃; |
2,2,2-trichloro-acetimidic acid phenyl ester
A
trichloroacetonitrile
B
phenol
Conditions | Yield |
---|---|
at 180℃; |
(2,2,2-trichloro-1-phenoxy-ethyliden)-amidophosphoric acid diphenyl ester
trichloroacetonitrile
Conditions | Yield |
---|---|
at 250 - 300℃; |
Conditions | Yield |
---|---|
With chlorine at 60℃; | |
With hydrogenchloride; chlorine |
Conditions | Yield |
---|---|
With sulfuryl dichloride; platinum at 200 - 500℃; | |
With chlorine; platinum at 200 - 500℃; | |
With hydrogenchloride; chlorine |
<2,2,2-trichloro-1-<(pentachloroethyl)imino>ethyl>phosphorimidic trichloride
A
trichloroacetamide
B
trichloroacetonitrile
C
trichloroacetic acid
Conditions | Yield |
---|---|
With water for 0.25h; Heating; |
Conditions | Yield |
---|---|
With chlorine; iron(III) chloride at 24.9℃; for 168h; Product distribution; also in the presence of 2, various conc.; |
acetonitrile
A
dichloroacetonitrile
B
chloroacetonitrile
C
trichloroacetonitrile
Conditions | Yield |
---|---|
With chlorine at 22.9℃; under 700 Torr; Irradiation; Yield given. Title compound not separated from byproducts; | |
With chlorine at 22.9℃; under 700 Torr; Kinetics; Irradiation; different reaction temperature and pressure; |
Conditions | Yield |
---|---|
at 60℃; Irradiation; |
Conditions | Yield |
---|---|
With chlorine; pyrographite at 300℃; |
Conditions | Yield |
---|---|
at 200℃; |
trichlorophosphazotrichlorooxoethane
A
trichloroacetonitrile
B
trichlorophosphate
Conditions | Yield |
---|---|
at 260℃; |
tetrachloroethyliden-amidophosphoryl chloride
A
trichloroacetonitrile
B
trichlorophosphate
Conditions | Yield |
---|---|
at 220℃; |
(1S)-1-[3,5-bis(trifluoromethyl)phenyl]ethyl-2,2,2-trichloroethanimidoate
C20H31FO7S2
A
C30H37F7O7S2
B
C30H37F7O7S2
C
trichloroacetonitrile
Conditions | Yield |
---|---|
Stage #1: (1S)-1-[3,5-bis(trifluoromethyl)phenyl]ethyl-2,2,2-trichloroethanimidoate; C20H31FO7S2 With tetrafluorohydroboric acid In dichloromethane; cyclohexane at -17 - 20℃; for 23.6667h; Stage #2: With sodium hydroxide In dichloromethane; cyclohexane; water at 18 - 20℃; for 0.25h; |
2-phenylethanol
trichloroacetonitrile
β-phenylethyl trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane | 100% |
With sodium | |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; |
trichloroacetonitrile
benzyl alcohol
O-benzyl 2,2,2-trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In n-heptane at 0℃; for 0.25h; Solvent; | 100% |
With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide In dichloromethane; water at -15 - 20℃; for 1.5h; | 99% |
With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate In dichloromethane at -15 - 25℃; for 1h; | 97% |
Conditions | Yield |
---|---|
With sulfuric acid In nitrobenzene; chlorobenzene at 60℃; Rate constant; Thermodynamic data; Mechanism; various temperatures, ΔG (excit.), ΔH (excit.), ΔS (excit.); | 100% |
With sulfuric acid at 25℃; | 100% |
With C19H23Cl2N6PRuS3*3ClH; water at 100℃; for 1h; Inert atmosphere; Schlenk technique; | 86% |
3,4-dihydro-isoquinoline 2-oxide
trichloroacetonitrile
2-Trichloromethyl-5,9b-dihydro-4H-3-oxa-1,3a-diaza-cyclopenta[a]naphthalene
Conditions | Yield |
---|---|
In toluene at 100℃; for 0.0333333h; | 100% |
2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranose
trichloroacetonitrile
O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)trichloroacetimidate
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane at 20℃; for 2h; Molecular sieve; | 100% |
With 4 A molecular sieve; sodium hydride; potassium carbonate 1.) dichloromethane, 6.5 h; 2.) dichloromethane, 5 h, r.t.; Yield given. Multistep reaction; |
2,3,4,6-Tetra-O-benzyl-D-glucopyranose
trichloroacetonitrile
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
In dichloromethane at 0℃; for 1h; Molecular sieve; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0℃; for 2h; | 98% |
With sodium hydride In dichloromethane for 2.5h; Ambient temperature; | 96% |
2,3,4,5-tetra-O-acetyl-D-glucopyranose
trichloroacetonitrile
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 1h; | 100% |
polystyrene supported organic base (PS-DBU) In dichloromethane at 20℃; for 1.5h; | 99% |
1,8-diazabicyclo[5.4.0]undec-7-ene at 0℃; for 1.5h; Addition; | 95% |
2,3,4,6-tetra-O-acetyl-α/β-D-galactopyranose
trichloroacetonitrile
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 1h; | 100% |
With potassium carbonate In dichloromethane at 20℃; | 96.1% |
1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0℃; for 1.5h; Addition; | 95% |
C-phenyl-N-methylnitrone
trichloroacetonitrile
5-trichloromethyl-2-methyl-3-phenyl-2,3-dihydro-1,2,4-oxadiazole
Conditions | Yield |
---|---|
In toluene at 110℃; for 0.0333333h; | 100% |
2,3,4-tri-O-benzyl-L-rhamnopyranose
trichloroacetonitrile
(2S,3R,4R,5S,6S)-3,4,5-tris(benzyloxy)-6-methyltetrahydro-2H-pyran-2-yl 2,2,2-trichloroacetimidate
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane for 3.5h; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere; | 86% |
With sodium hydride In dichloromethane for 0.5h; Ambient temperature; | 85% |
With sodium hydride In dichloromethane at 20℃; for 1.5h; | 81% |
2,3,4,6-tetra-O-benzyl-D-mannopyranose
trichloroacetonitrile
2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 18h; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere; | 92% |
With sodium hydride In dichloromethane for 30h; Ambient temperature; | 86% |
(2R,3S)-2,3-epoxynerol
trichloroacetonitrile
2,2,2-Trichloro-acetimidic acid (2R,3S)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranylmethyl ester
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0℃; for 1h; | 100% |
6-O-acetyl-2,3,4-tri-O-benzyl-α/β-D-galactopyranoside
trichloroacetonitrile
6-O-acetyl-2,3,4-tri-O-benzyl-α/β-D-galactopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane for 4.5h; | 100% |
2-oxo-3-(ethoxycarbonyl)-3,4-dihydro-β-carboline
trichloroacetonitrile
(4R,10bR)-2-Trichloromethyl-4,5,10,10b-tetrahydro-3-oxa-1,3a,10-triaza-cyclopenta[a]fluorene-4-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
In toluene at 80℃; for 0.0333333h; | 100% |
trichloroacetonitrile
O-(2,3,4-tri-O-benzyl-α-D-xylopyranosyl)-(1-3)-O-(2,4-di-O-benzyl-α-D-xylopyranosyl)-(1-3)-2,4,6-tri-O-acetyl-α,β-D-glucopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With CsCO3 In dichloromethane for 2h; Ambient temperature; | 100% |
3-O-<3-O-(2,3,4,6-tetra-O-benzoyl-α-D-galactopyranosyl)-6-O-acetyl-2,4-di-O-benzoyl-β-D-galactopyranosyl>-6-O-acetyl-4-O-benzyl-2-deoxy-2-phthalimido-α/β-D-glucopyranose
trichloroacetonitrile
3-O-<3-O-(2,3,4,6-tetra-O-benzoyl-α-D-galactopyranosyl)-6-O-acetyl-2,4-di-O-benzoyl-β-D-galactopyranosyl>-6-O-acetyl-4-O-benzyl-2-deoxy-2-phthalimido-α/β-D-glucopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane for 4.5h; Ambient temperature; | 100% |
trichloroacetonitrile
4-Methoxybenzyl alcohol
O-(4-methoxybenzyl)-trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In hexane at 0℃; for 0.25h; Solvent; | 100% |
Stage #1: 4-Methoxybenzyl alcohol With sodium hydride In diethyl ether at 20℃; for 0.25h; Inert atmosphere; Stage #2: trichloroacetonitrile In diethyl ether at 0℃; | 98% |
Stage #1: 4-Methoxybenzyl alcohol With sodium hydride In diethyl ether at 20℃; for 0.5h; Stage #2: trichloroacetonitrile In diethyl ether at 0 - 20℃; Further stages.; | 96% |
trichloroacetonitrile
(2E)-3-phenyl-2-propen-1-ol
1-(1-imino-2,2,2-trichloroethoxy)-3-phenyl-2(E)-propene
Conditions | Yield |
---|---|
With sodium hydride In diethyl ether at -10℃; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0℃; for 0.25h; | 98% |
Stage #1: (2E)-3-phenyl-2-propen-1-ol With sodium hydride In diethyl ether; mineral oil at 20℃; Stage #2: trichloroacetonitrile In diethyl ether; mineral oil at -10 - 20℃; | 97% |
trichloroacetonitrile
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0℃; for 0.5h; | 100% |
trichloroacetonitrile
O-(3-O-allyl-6-O-levulinoyl-2,4-di-O-toluoyl-β-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-toluoyl-β-D-glucopyranosyl)-(1->6)-O-(3-O-allyl-2,4-di-O-toluoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-toluoyl-α-D-glucopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 24h; Ambient temperature; | 100% |
2,3,4,6-Tetra-O-benzyl-D-glucopyranose
trichloroacetonitrile
2,3,4,6-tetra-O-benzyl-D-glucopyranose trichloroacetimidate
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane at 20℃; for 23h; Esterification; | 100% |
With PTBD In dichloromethane at 20℃; for 2h; | 100% |
With potassium carbonate In dichloromethane at 20℃; for 4h; Inert atmosphere; | 100% |
biphenyl-4-yl methanol
trichloroacetonitrile
4-phenylbenzyl trichloroacetimidate
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide In dichloromethane; water at 0 - 25℃; | 100% |
Stage #1: biphenyl-4-yl methanol With sodium hydride In diethyl ether; oil at 20℃; for 0.0833333h; Stage #2: trichloroacetonitrile In diethyl ether; oil at 20℃; for 2h; | 97% |
With sodium hydride In diethyl ether 1.) 20 min, 2.) r.t., 1 h; | 69% |
With sodium hydride In diethyl ether at 20℃; for 1h; | |
Stage #1: biphenyl-4-yl methanol With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Stage #2: trichloroacetonitrile In tetrahydrofuran at 20℃; for 2h; |
trichloroacetonitrile
2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranoside
O-(2-O-benzoyl-3,4,6-tri-O-benzyl-D-glucopyranosyl)trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 0℃; for 0.25h; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at -30℃; for 0.5h; Addition; | 90% |
trichloroacetonitrile
methyl O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->2)-3,4-di-O-acetyl-1-O-trichloroacetimidoyl-α-D-glucopyranuronate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at -5℃; for 2h; Addition; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at -5℃; for 2h; Yield given; |
6-O-acetyl-1,5-anhydro-2,3-dideoxy-D-erythro-hex-2-enitol
trichloroacetonitrile
6-O-acetyl-1,5-anhydro-2,3-dideoxy-4-O-(1-imino-2,2,2-trichloroethyl)-D-erythro-hex-2-enitol
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane Addition; | 100% |
trichloroacetonitrile
p-methoxyphenyl 6-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside
p-methoxyphenyl 6-O-acetyl-2,3-dideoxy-4-O-(1-imino-2,2,2-trichloroethyl)-α-D-erythro-hex-2-enopyranoside
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at -17℃; for 0.25h; Addition; | 100% |
trichloroacetonitrile
6-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl 6-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside
6-O-acetyl-2,3-dideoxy-4-O-(1-imino-2,2,2-trichloroethyl)-α-D-erythro-hex-2-enopyranosyl 6-O-acetyl-2,3-dideoxy-4-O-(1-imino-2,2,2-trichloroethyl)-α-D-erythro-hex-2-enopyranoside
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane Addition; | 100% |
trichloroacetonitrile
6-O-benzyl-3-O-[(S)-3-(benzyloxy)tetradecanoyl]-2-deoxy-4-O-(1,5-dihydro-3-oxo-3λ5-3H-2,4,3-benzodioxaphosphepin-3-yl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane at 20℃; for 0.5h; Addition; | 100% |
trichloroacetonitrile
6-O-benzyl-3-O-[(R)-3-(benzyloxy)tetradecanoyl]-2-deoxy-4-O-(1,5-dihydro-3-oxo-3λ5-3H-2,4,3-benzodioxaphosphepin-3-yl)-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane at 20℃; for 1h; Addition; | 100% |
trichloroacetonitrile
3-O,4-S-Dibenzoyl-2,6-dideoxy-4-thio-D-ribo-hexopyranosyl trichloroacetimidate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 1h; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 1h; Ambient temperature; |
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