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Cas:79-36-7
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With tributyl borane; oxygen at 80℃; under 2280.15 Torr; for 11h; Reagent/catalyst; | 90% |
With oxygen; chlorine at 40 - 50℃; Irradiation.im UV-Licht; | |
With oxygen Irradiation.beim Behandeln des erhaltenen Gemisches aus Dichloracetylchlorid und Trichloraethylenoxyd mit wenig Dimethylamin oder anderen sekundaeren oder tertiaeren Aminen; |
ethylphenylphosphinous chloride
trichloroacetic acid
A
dichloroacethyl chloride
B
ethylphenylphosphinic chloride
Conditions | Yield |
---|---|
for 1h; Ambient temperature; argon atmosphere; | A 88% B 50% |
Ambient temperature; | A 88% B 50% |
diethylchlorophosphine
trichloroacetic acid
A
dichloroacethyl chloride
B
diethylphosphinic chloride
Conditions | Yield |
---|---|
for 1h; Ambient temperature; | A 87% B 60% |
ethyl ester of ethylphenylthiophosphinic acid
trichloroacetic acid
A
dichloroacethyl chloride
B
S-ethyl dichlorothiolacetate
C
ethylphenylphosphinic chloride
D
S-ethyl ethylphenylphosphinothioate
Conditions | Yield |
---|---|
for 1h; Ambient temperature; argon atmosphere; | A 64% B 60% C n/a D n/a |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 40℃; for 21h; | A 9% B 22% C 38% |
Conditions | Yield |
---|---|
Stage #1: dichloro-acetic acid With chloroform; oxygen; N,N-dimethyl-formamide at 30℃; for 3h; Irradiation; Stage #2: at 30℃; for 2h; | 7% |
With thionyl chloride | |
With zinc(II) chloride; phosphorus trichloride |
Conditions | Yield |
---|---|
With dichloromethane; chlorine at -50℃; |
Conditions | Yield |
---|---|
With chlorine in der Gasphase; |
Conditions | Yield |
---|---|
With anionenexchanger at 130℃; |
Conditions | Yield |
---|---|
With oxygen Umsetzung der bis 107grad siedenden Anteile des Reaktionsprodukts mit Metallchloriden wie SbCl5,FeCl3 oder AlCl3; |
Conditions | Yield |
---|---|
With sulfuric acid at 50 - 60℃; |
Conditions | Yield |
---|---|
With chlorine mit Hilfe von UV-Licht; | |
With acetyl-cyclohexanesulfonyl peroxide; chlorine |
(E)-1,2-dichloro-1-ethoxy-ethene
dichloroacethyl chloride
Conditions | Yield |
---|---|
With chlorine |
dichloro-acetic acid
Benzotrichlorid
A
dichloroacethyl chloride
B
benzoyl chloride
Conditions | Yield |
---|---|
With zinc(II) chloride at 120℃; | |
With zinc(II) chloride at 120℃; |
Conditions | Yield |
---|---|
With chlorine at -18℃; |
Conditions | Yield |
---|---|
With pyridine; chlorine at 75 - 80℃; |
Conditions | Yield |
---|---|
With quinoline; Pd-BaSO4; sulfur at 140℃; Reagens 4: Petroleum; |
Conditions | Yield |
---|---|
With air Irradiation.bei 26-taegiger UV-Bestrahlung; | |
With oxygen Irradiation.bei 26-taegiger UV-Bestrahlung; |
1,1,2,2-tetrachloroethane
A
dichloroacethyl chloride
B
1,1,1,2,2,3,3,4-octachloro-butane
C
oxalic acid
Conditions | Yield |
---|---|
bei 26-taegigem Bestrahlung mit UV-Licht unter Durchleiten von trockener Luft oder trockenem Sauerstoff.Irradiation; |
trichloroethylene epoxide
dichloroacethyl chloride
Conditions | Yield |
---|---|
diethylamine at 60℃; for 1h; sealed tube; Yield given; |
Conditions | Yield |
---|---|
at 130℃; for 2h; Product distribution; Kinetics; Thermodynamic data; sealed tube, var.catalysts, oth. temperature, E(activ.); | A 91 % Chromat. B 9 % Chromat. |
1,1,2,2-tetrachloroethylene
A
phosgene
B
dichloroacethyl chloride
C
dichloromethyl radical
D
Trichloroethenol
Conditions | Yield |
---|---|
With hydroxide In gas at 27.9℃; under 0.4 - 4.2 Torr; Product distribution; Thermodynamic data; Rate constant; other temperatures; A, E; |
trans-1,2-dichloroethylene
A
dichloroacethyl chloride
B
trichloroethylene epoxide
trans-1,2-Dichloroethylene epoxide
D
1,1,2,2-tetrachloroethane
Conditions | Yield |
---|---|
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
trans-1,2-dichloroethylene
A
dichloroacethyl chloride
B
dichloromethyl 1,2,2-trichloroethyl ether
trans-1,2-Dichloroethylene epoxide
D
1,1,2,2-tetrachloroethane
Conditions | Yield |
---|---|
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
trans-1,2-dichloroethylene
A
dichloroacethyl chloride
B
1,2,2,2-tetrachloroethyl 1,2,2-trichloroethyl ether
trans-1,2-Dichloroethylene epoxide
D
1,1,2,2-tetrachloroethane
Conditions | Yield |
---|---|
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
trans-1,2-dichloroethylene
A
dichloroacethyl chloride
B
1,2,2-trichloroethyl dichloroacetate
trans-1,2-Dichloroethylene epoxide
D
1,1,2,2-tetrachloroethane
Conditions | Yield |
---|---|
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
trans-1,2-dichloroethylene
A
dichloroacethyl chloride
B
meso-bis(1,2,2-trichloroethyl) ether
trans-1,2-Dichloroethylene epoxide
D
1,1,2,2-tetrachloroethane
Conditions | Yield |
---|---|
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
trans-1,2-dichloroethylene
A
dichloroacethyl chloride
rac-bis(1,2,2-trichloroethyl) ether
trans-1,2-Dichloroethylene epoxide
D
1,1,2,2-tetrachloroethane
Conditions | Yield |
---|---|
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
trans-1,2-dichloroethylene
A
dichloroacethyl chloride
B
pentachloroethane
C
2,2-dichloroacetaldehyde
D
meso-1,1,2,3,4,4-hexachloro-butane
E
dichloromethyl 1,2,2-trichloroethyl ether
F
1,1,2,2-tetrachloroethane
Conditions | Yield |
---|---|
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; Mechanism; Rate constant; Product distribution; Irradiation; |
Trichloroethylene
A
dichloro-acetic acid
B
dichloroacethyl chloride
C
1,1,3,3,4,4,-hexachloro-1-butene
Conditions | Yield |
---|---|
In neat (no solvent) at 130℃; Product distribution; effect of the time and the temp.; |
dichloroacethyl chloride
diethyl 2-[(4-methoxyphenyl)amino]malonate
2-[(2,2-Dichloro-acetyl)-(4-methoxy-phenyl)-amino]-malonic acid diethyl ester
Conditions | Yield |
---|---|
In benzene for 2h; Heating; | 100% |
dichloroacethyl chloride
Isopropylphenyl(trimethylsilyl)phosphan
(Dichloracetyl)isopropylphenylphosphan
Conditions | Yield |
---|---|
In diethyl ether at -80℃; for 5h; | 100% |
dichloroacethyl chloride
Ethylphenyl(trimethylsilyl)phosphan
Conditions | Yield |
---|---|
In diethyl ether at -80℃; for 5h; | 100% |
dichloroacethyl chloride
Phenyl-n-propyl(trimethylsilyl)phosphan
Conditions | Yield |
---|---|
In diethyl ether at -80℃; for 5h; | 100% |
dichloroacethyl chloride
methyl (2E)-3-(2-aminophenyl)propenoate
(E)-Methyl 3-propenoate
Conditions | Yield |
---|---|
With triethylamine In diethyl ether for 0.166667h; Ambient temperature; | 100% |
dichloroacethyl chloride
(2-tert-Butyl-5-methylphenoxy)magnesium bromide
2-tert-Butyl-5-methylphenyl dichloroacetate
Conditions | Yield |
---|---|
In toluene for 5h; Ambient temperature; also aluminium phenolate; | 100% |
dichloroacethyl chloride
(-)-8-phenylmenthol
(1R,2S,5R)-(+)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl dichloroacetate
Conditions | Yield |
---|---|
at 100℃; | 100% |
dichloroacethyl chloride
9-hydroxyphenalenone sodium salt
9-dichloroacetoxyphenalenone
Conditions | Yield |
---|---|
In tetrahydrofuran for 24h; Ambient temperature; | 100% |
dichloroacethyl chloride
trimethylsilyldicyclohexylphosphane
Conditions | Yield |
---|---|
In diethyl ether at -25℃; | 100% |
dichloroacethyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
dichloroacethyl chloride
2-(3-indole)-ethanol
2-(Indol-3'-yl)ethyl Dichloroacetate
Conditions | Yield |
---|---|
With pyridine In dichloromethane for 18h; kept in the dark; | 100% |
dichloroacethyl chloride
(2,2-Bis-phenylsulfanyl-vinyl)-((S)-1-phenyl-ethyl)-amine
Conditions | Yield |
---|---|
With N,N-diethylaniline In benzene Heating; | 100% |
dichloroacethyl chloride
ethyl 2-dichloroacetyl-3-diethylaminoacrylate
Conditions | Yield |
---|---|
With α-picoline In toluene at 0 - 20℃; for 1.5h; | 100% |
dichloroacethyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
dichloroacethyl chloride
(E)-cyclooctene
9,9-Dichloro-10-oxo-trans-bicyclo<6.2.0>decane
Conditions | Yield |
---|---|
With triethylamine In hexane | 99% |
dichloroacethyl chloride
2-(trimethylsilyl)thiazole
2-(2,2-Dichloro-1-trimethylsilanyloxy-vinyl)-thiazole
Conditions | Yield |
---|---|
With triethylamine In hexane Ambient temperature; | 99% |
With triethylamine In hexane for 4h; | 80% |
dichloroacethyl chloride
4-[1-Diisopropylamino-meth-(E)-ylidene]-3,4-dihydro-2H-benzo[b]thiepin-5-one
3,3-Dichloro-4-diisopropylamino-3,4,5,6-tetrahydro-1-oxa-7-thia-dibenzo[a,c]cyclohepten-2-one
Conditions | Yield |
---|---|
With triethylamine In toluene for 0.5h; Ambient temperature; | 99% |
tert-butyl (S)-4-hydroxy-2-methylpent-2E-enoate
dichloroacethyl chloride
(E)-(S)-4-(2,2-Dichloro-acetoxy)-2-methyl-pent-2-enoic acid tert-butyl ester
Conditions | Yield |
---|---|
With pyridine; dmap In tetrahydrofuran for 2h; | 99% |
With pyridine; dmap In tetrahydrofuran at 25℃; for 2h; | 99% |
Conditions | Yield |
---|---|
With potassium fluoride; C30H22Cl4CrN4O2 at 80℃; for 2h; Reagent/catalyst; | 99% |
With hydrogen fluoride; fluorinated chromium III oxide at 200 - 250℃; for 0.00555556h; Product distribution / selectivity; Gas phase; | 53% |
dichloroacethyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water at -15 - -10℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; for 24h; | 99% |
dichloroacethyl chloride
ethyl 3-{[{2-amino-1-(methylamino)phen-4-yl}carbonyl](pyridyn-2-yl)amino}propanoate
Conditions | Yield |
---|---|
In acetonitrile at -15 - 60℃; | 98.8% |
Conditions | Yield |
---|---|
Stage #1: aniline With sodium hydrogencarbonate at 20℃; for 7h; Sonication; Stage #2: dichloroacethyl chloride In tetrahydrofuran at 60℃; for 8h; Microwave irradiation; | 98.6% |
With triethylamine In dichloromethane Cooling; | 86.2% |
With triethylamine In dichloromethane | 86% |
2-aminopyridine
dichloroacethyl chloride
2,2-dichloro-N-(pyridine-2-yl)acetamide
Conditions | Yield |
---|---|
for 1h; | 98% |
With pyridine | |
With benzene |
dichloroacethyl chloride
isopropylamine
N-Isopropyl-2,2-dichloroacetamide
Conditions | Yield |
---|---|
In dichloromethane | 98% |
With 1,2-dichloro-ethane at -20 - -10℃; |
Conditions | Yield |
---|---|
With 1,1,1,3,3-pentafluoro-2,3-dichloropropane at 60 - 80℃; for 9h; | 98% |
With triethylamine In dichloromethane Cooling; | 94.2% |
for 3h; Reflux; Alkaline conditions; | 82% |
dichloroacethyl chloride
2-isopropenylaniline
2,2-Dichloro-N-acetamide
Conditions | Yield |
---|---|
With triethylamine In diethyl ether for 0.166667h; Ambient temperature; | 98% |
dichloroacethyl chloride
Aluminum; 2-tert-butyl-4-methyl-phenolate
A
ω,ω-Dichloro-2-hydroxy-3-tert-butyl-5-methylacetophenone
B
2-tert-Butyl-4-methylphenyl dichloroacetate
Conditions | Yield |
---|---|
In toluene for 5h; Ambient temperature; | A 98% B 2% |
dichloroacethyl chloride
5-[1-Diphenylamino-meth-(E)-ylidene]-6,7-dihydro-5H-benzo[b]thiophen-4-one
3,3-Dichloro-4-diphenylamino-3,4,5,6-tetrahydro-thieno[2,3-h]chromen-2-one
Conditions | Yield |
---|---|
With triethylamine | 98% |
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