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Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

Dichloroacetyl chloride 79-36-7

Cas:79-36-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#79-36-7;CAT#A839664

Cas:79-36-7

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Pure Chemistry Scientific Inc.

Dichloroacetyl chloride Application:814059

Dichloroacetyl chloride

Cas:79-36-7

Min.Order:1 Gram

FOB Price: $500.0

Type:Trading Company

inquiry

Synthetic route

Trichloroethylene
79-01-6

Trichloroethylene

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With tributyl borane; oxygen at 80℃; under 2280.15 Torr; for 11h; Reagent/catalyst;90%
With oxygen; chlorine at 40 - 50℃; Irradiation.im UV-Licht;
With oxygen Irradiation.beim Behandeln des erhaltenen Gemisches aus Dichloracetylchlorid und Trichloraethylenoxyd mit wenig Dimethylamin oder anderen sekundaeren oder tertiaeren Aminen;
ethylphenylphosphinous chloride
15849-83-9, 75231-38-8, 75231-39-9

ethylphenylphosphinous chloride

trichloroacetic acid
76-03-9

trichloroacetic acid

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

ethylphenylphosphinic chloride
1499-22-5

ethylphenylphosphinic chloride

Conditions
ConditionsYield
for 1h; Ambient temperature; argon atmosphere;A 88%
B 50%
Ambient temperature;A 88%
B 50%
diethylchlorophosphine
686-69-1

diethylchlorophosphine

trichloroacetic acid
76-03-9

trichloroacetic acid

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

diethylphosphinic chloride
1112-37-4

diethylphosphinic chloride

Conditions
ConditionsYield
for 1h; Ambient temperature;A 87%
B 60%
ethyl ester of ethylphenylthiophosphinic acid
6587-98-0, 62621-04-9, 62621-07-2

ethyl ester of ethylphenylthiophosphinic acid

trichloroacetic acid
76-03-9

trichloroacetic acid

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

S-ethyl dichlorothiolacetate
41880-03-9

S-ethyl dichlorothiolacetate

C

ethylphenylphosphinic chloride
1499-22-5

ethylphenylphosphinic chloride

D

S-ethyl ethylphenylphosphinothioate
33626-88-9

S-ethyl ethylphenylphosphinothioate

Conditions
ConditionsYield
for 1h; Ambient temperature; argon atmosphere;A 64%
B 60%
C n/a
D n/a
2-chloropropionyl chloride
7623-09-8

2-chloropropionyl chloride

tropone azine
86428-01-5

tropone azine

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

3,3'-Dimethyl-[1,1']bi[cyclohepta[b]pyrrolyl]-2,2'-dione

3,3'-Dimethyl-[1,1']bi[cyclohepta[b]pyrrolyl]-2,2'-dione

C

3-Chloro-3,3'-dimethyl-3,3a-dihydro-[1,1']bi[cyclohepta[b]pyrrolyl]-2,2'-dione

3-Chloro-3,3'-dimethyl-3,3a-dihydro-[1,1']bi[cyclohepta[b]pyrrolyl]-2,2'-dione

Conditions
ConditionsYield
With triethylamine In dichloromethane at 40℃; for 21h;A 9%
B 22%
C 38%
dichloro-acetic acid
79-43-6

dichloro-acetic acid

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
Stage #1: dichloro-acetic acid With chloroform; oxygen; N,N-dimethyl-formamide at 30℃; for 3h; Irradiation;
Stage #2: at 30℃; for 2h;
7%
With thionyl chloride
With zinc(II) chloride; phosphorus trichloride
Ketene
463-51-4

Ketene

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With dichloromethane; chlorine at -50℃;
Ketene
463-51-4

Ketene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With chlorine in der Gasphase;
phosgene
75-44-5

phosgene

dichloro-acetic acid
79-43-6

dichloro-acetic acid

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With anionenexchanger at 130℃;
Trichloroethylene
79-01-6

Trichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
With oxygen Umsetzung der bis 107grad siedenden Anteile des Reaktionsprodukts mit Metallchloriden wie SbCl5,FeCl3 oder AlCl3;
pentachloroethane
76-01-7

pentachloroethane

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With sulfuric acid at 50 - 60℃;
2,2-dichloroacetaldehyde
79-02-7

2,2-dichloroacetaldehyde

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With chlorine mit Hilfe von UV-Licht;
With acetyl-cyclohexanesulfonyl peroxide; chlorine
(E)-1,2-dichloro-1-ethoxy-ethene
42345-82-4

(E)-1,2-dichloro-1-ethoxy-ethene

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With chlorine
dichloro-acetic acid
79-43-6

dichloro-acetic acid

Benzotrichlorid
98-07-7

Benzotrichlorid

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

benzoyl chloride
98-88-4

benzoyl chloride

Conditions
ConditionsYield
With zinc(II) chloride at 120℃;
With zinc(II) chloride at 120℃;
Ketene
463-51-4

Ketene

chloroacetyl chloride
79-04-9

chloroacetyl chloride

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With chlorine at -18℃;
chloroacetyl chloride
79-04-9

chloroacetyl chloride

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

Trichloroacetyl chloride
76-02-8

Trichloroacetyl chloride

Conditions
ConditionsYield
With pyridine; chlorine at 75 - 80℃;
Trichloroacetyl chloride
76-02-8

Trichloroacetyl chloride

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With quinoline; Pd-BaSO4; sulfur at 140℃; Reagens 4: Petroleum;
1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
With air Irradiation.bei 26-taegiger UV-Bestrahlung;
With oxygen Irradiation.bei 26-taegiger UV-Bestrahlung;
1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

1,1,1,2,2,3,3,4-octachloro-butane
88982-96-1

1,1,1,2,2,3,3,4-octachloro-butane

C

oxalic acid
144-62-7

oxalic acid

Conditions
ConditionsYield
bei 26-taegigem Bestrahlung mit UV-Licht unter Durchleiten von trockener Luft oder trockenem Sauerstoff.Irradiation;
trichloroethylene epoxide
16967-79-6

trichloroethylene epoxide

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Conditions
ConditionsYield
diethylamine at 60℃; for 1h; sealed tube; Yield given;
trichloroethylene epoxide
16967-79-6

trichloroethylene epoxide

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

chloral
75-87-6

chloral

Conditions
ConditionsYield
at 130℃; for 2h; Product distribution; Kinetics; Thermodynamic data; sealed tube, var.catalysts, oth. temperature, E(activ.);A 91 % Chromat.
B 9 % Chromat.
Conditions
ConditionsYield
With hydroxide In gas at 27.9℃; under 0.4 - 4.2 Torr; Product distribution; Thermodynamic data; Rate constant; other temperatures; A, E;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

trichloroethylene epoxide
16967-79-6

trichloroethylene epoxide

trans-1,2-Dichloroethylene epoxide
16650-12-7

trans-1,2-Dichloroethylene epoxide

D

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

Conditions
ConditionsYield
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

dichloromethyl 1,2,2-trichloroethyl ether
117702-58-6

dichloromethyl 1,2,2-trichloroethyl ether

trans-1,2-Dichloroethylene epoxide
16650-12-7

trans-1,2-Dichloroethylene epoxide

D

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

Conditions
ConditionsYield
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

1,2,2,2-tetrachloroethyl 1,2,2-trichloroethyl ether
117702-56-4

1,2,2,2-tetrachloroethyl 1,2,2-trichloroethyl ether

trans-1,2-Dichloroethylene epoxide
16650-12-7

trans-1,2-Dichloroethylene epoxide

D

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

Conditions
ConditionsYield
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

1,2,2-trichloroethyl dichloroacetate
117702-57-5

1,2,2-trichloroethyl dichloroacetate

trans-1,2-Dichloroethylene epoxide
16650-12-7

trans-1,2-Dichloroethylene epoxide

D

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

Conditions
ConditionsYield
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

meso-bis(1,2,2-trichloroethyl) ether
117702-53-1

meso-bis(1,2,2-trichloroethyl) ether

trans-1,2-Dichloroethylene epoxide
16650-12-7

trans-1,2-Dichloroethylene epoxide

D

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

Conditions
ConditionsYield
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

rac-bis(1,2,2-trichloroethyl) ether
117702-53-1, 117702-54-2

rac-bis(1,2,2-trichloroethyl) ether

trans-1,2-Dichloroethylene epoxide
16650-12-7

trans-1,2-Dichloroethylene epoxide

D

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

Conditions
ConditionsYield
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; for 56h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

pentachloroethane
76-01-7

pentachloroethane

C

2,2-dichloroacetaldehyde
79-02-7

2,2-dichloroacetaldehyde

D

meso-1,1,2,3,4,4-hexachloro-butane
32149-32-9

meso-1,1,2,3,4,4-hexachloro-butane

E

dichloromethyl 1,2,2-trichloroethyl ether
117702-58-6

dichloromethyl 1,2,2-trichloroethyl ether

F

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

Conditions
ConditionsYield
With oxygen; chlorine In neat (no solvent) at 30℃; under 1050.08 Torr; Mechanism; Rate constant; Product distribution; Irradiation;
Trichloroethylene
79-01-6

Trichloroethylene

A

dichloro-acetic acid
79-43-6

dichloro-acetic acid

B

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

C

1,1,3,3,4,4,-hexachloro-1-butene
34973-39-2

1,1,3,3,4,4,-hexachloro-1-butene

Conditions
ConditionsYield
In neat (no solvent) at 130℃; Product distribution; effect of the time and the temp.;
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

diethyl 2-[(4-methoxyphenyl)amino]malonate
24043-40-1

diethyl 2-[(4-methoxyphenyl)amino]malonate

2-[(2,2-Dichloro-acetyl)-(4-methoxy-phenyl)-amino]-malonic acid diethyl ester
106817-56-5

2-[(2,2-Dichloro-acetyl)-(4-methoxy-phenyl)-amino]-malonic acid diethyl ester

Conditions
ConditionsYield
In benzene for 2h; Heating;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Isopropylphenyl(trimethylsilyl)phosphan
29574-16-1

Isopropylphenyl(trimethylsilyl)phosphan

(Dichloracetyl)isopropylphenylphosphan
104192-61-2

(Dichloracetyl)isopropylphenylphosphan

Conditions
ConditionsYield
In diethyl ether at -80℃; for 5h;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Ethylphenyl(trimethylsilyl)phosphan
59877-22-4

Ethylphenyl(trimethylsilyl)phosphan

(Dichloracetyl)ethylphenylphosphan

(Dichloracetyl)ethylphenylphosphan

Conditions
ConditionsYield
In diethyl ether at -80℃; for 5h;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Phenyl-n-propyl(trimethylsilyl)phosphan
59877-23-5

Phenyl-n-propyl(trimethylsilyl)phosphan

(Dichloracetyl)phenyl-n-propylphosphan

(Dichloracetyl)phenyl-n-propylphosphan

Conditions
ConditionsYield
In diethyl ether at -80℃; for 5h;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

methyl (2E)-3-(2-aminophenyl)propenoate
88939-75-7

methyl (2E)-3-(2-aminophenyl)propenoate

(E)-Methyl 3-propenoate
133901-63-0

(E)-Methyl 3-propenoate

Conditions
ConditionsYield
With triethylamine In diethyl ether for 0.166667h; Ambient temperature;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

(2-tert-Butyl-5-methylphenoxy)magnesium bromide
53863-60-8

(2-tert-Butyl-5-methylphenoxy)magnesium bromide

2-tert-Butyl-5-methylphenyl dichloroacetate
127354-47-6

2-tert-Butyl-5-methylphenyl dichloroacetate

Conditions
ConditionsYield
In toluene for 5h; Ambient temperature; also aluminium phenolate;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

(-)-8-phenylmenthol
65253-04-5

(-)-8-phenylmenthol

(1R,2S,5R)-(+)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl dichloroacetate
152481-90-8

(1R,2S,5R)-(+)-2-(1-methyl-1-phenylethyl)-5-methylcyclohexyl dichloroacetate

Conditions
ConditionsYield
at 100℃;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

9-hydroxyphenalenone sodium salt
129087-30-5

9-hydroxyphenalenone sodium salt

9-dichloroacetoxyphenalenone
129087-27-0

9-dichloroacetoxyphenalenone

Conditions
ConditionsYield
In tetrahydrofuran for 24h; Ambient temperature;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

trimethylsilyldicyclohexylphosphane
104202-80-4

trimethylsilyldicyclohexylphosphane

(dichloroacetyl)dicyclohexylphosphane

(dichloroacetyl)dicyclohexylphosphane

Conditions
ConditionsYield
In diethyl ether at -25℃;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

3-(2-Hydroxy-3-methoxy-phenyl)-cyclohex-2-enone

3-(2-Hydroxy-3-methoxy-phenyl)-cyclohex-2-enone

Dichloro-acetic acid 2-methoxy-6-(3-oxo-cyclohex-1-enyl)-phenyl ester

Dichloro-acetic acid 2-methoxy-6-(3-oxo-cyclohex-1-enyl)-phenyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

2-(3-indole)-ethanol
526-55-6

2-(3-indole)-ethanol

2-(Indol-3'-yl)ethyl Dichloroacetate
141972-14-7

2-(Indol-3'-yl)ethyl Dichloroacetate

Conditions
ConditionsYield
With pyridine In dichloromethane for 18h; kept in the dark;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

(2,2-Bis-phenylsulfanyl-vinyl)-((S)-1-phenyl-ethyl)-amine
157734-48-0

(2,2-Bis-phenylsulfanyl-vinyl)-((S)-1-phenyl-ethyl)-amine

2,2-dichloro-N-<(S)-1-phenylethyl>-N-<2,2-bis(phenylthio)ethenyl>acetamide

2,2-dichloro-N-<(S)-1-phenylethyl>-N-<2,2-bis(phenylthio)ethenyl>acetamide

Conditions
ConditionsYield
With N,N-diethylaniline In benzene Heating;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

ethyl 3-(N,N-diethylamino)acrylate

ethyl 3-(N,N-diethylamino)acrylate

ethyl 2-dichloroacetyl-3-diethylaminoacrylate
1171114-12-7

ethyl 2-dichloroacetyl-3-diethylaminoacrylate

Conditions
ConditionsYield
With α-picoline In toluene at 0 - 20℃; for 1.5h;100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

1-[4-(4-amino-3-(pyrrolidin-1-yl)phenyl)piperazin-1-yl](1-methyl-1H-pyrrol-2-yl)methanone

1-[4-(4-amino-3-(pyrrolidin-1-yl)phenyl)piperazin-1-yl](1-methyl-1H-pyrrol-2-yl)methanone

1-[4-(4-N-dichloroacetyl-3-(pyrrolidin-1-yl)phenyl)piperazin-1-yl](1-methyl-1H-pyrrol-2-yl)methanone

1-[4-(4-N-dichloroacetyl-3-(pyrrolidin-1-yl)phenyl)piperazin-1-yl](1-methyl-1H-pyrrol-2-yl)methanone

Conditions
ConditionsYield
With triethylamine In dichloromethane100%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

(E)-cyclooctene
931-89-5

(E)-cyclooctene

9,9-Dichloro-10-oxo-trans-bicyclo<6.2.0>decane
18332-33-7, 18332-34-8, 22374-13-6

9,9-Dichloro-10-oxo-trans-bicyclo<6.2.0>decane

Conditions
ConditionsYield
With triethylamine In hexane99%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

2-(trimethylsilyl)thiazole
79265-30-8

2-(trimethylsilyl)thiazole

2-(2,2-Dichloro-1-trimethylsilanyloxy-vinyl)-thiazole
79265-33-1

2-(2,2-Dichloro-1-trimethylsilanyloxy-vinyl)-thiazole

Conditions
ConditionsYield
With triethylamine In hexane Ambient temperature;99%
With triethylamine In hexane for 4h;80%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

4-[1-Diisopropylamino-meth-(E)-ylidene]-3,4-dihydro-2H-benzo[b]thiepin-5-one
106364-99-2

4-[1-Diisopropylamino-meth-(E)-ylidene]-3,4-dihydro-2H-benzo[b]thiepin-5-one

3,3-Dichloro-4-diisopropylamino-3,4,5,6-tetrahydro-1-oxa-7-thia-dibenzo[a,c]cyclohepten-2-one
106365-11-1

3,3-Dichloro-4-diisopropylamino-3,4,5,6-tetrahydro-1-oxa-7-thia-dibenzo[a,c]cyclohepten-2-one

Conditions
ConditionsYield
With triethylamine In toluene for 0.5h; Ambient temperature;99%
tert-butyl (S)-4-hydroxy-2-methylpent-2E-enoate
866572-55-6

tert-butyl (S)-4-hydroxy-2-methylpent-2E-enoate

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

(E)-(S)-4-(2,2-Dichloro-acetoxy)-2-methyl-pent-2-enoic acid tert-butyl ester
866572-63-6

(E)-(S)-4-(2,2-Dichloro-acetoxy)-2-methyl-pent-2-enoic acid tert-butyl ester

Conditions
ConditionsYield
With pyridine; dmap In tetrahydrofuran for 2h;99%
With pyridine; dmap In tetrahydrofuran at 25℃; for 2h;99%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

2,2-difluoroacetyl fluoride
2925-22-6

2,2-difluoroacetyl fluoride

Conditions
ConditionsYield
With potassium fluoride; C30H22Cl4CrN4O2 at 80℃; for 2h; Reagent/catalyst;99%
With hydrogen fluoride; fluorinated chromium III oxide at 200 - 250℃; for 0.00555556h; Product distribution / selectivity; Gas phase;53%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

trans-2,5-diallylpyrrolidine

trans-2,5-diallylpyrrolidine

1-(2,5-diallyl-1-pyrrolidino)-2,2-dichloroethan-1-one

1-(2,5-diallyl-1-pyrrolidino)-2,2-dichloroethan-1-one

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane; water at -15 - -10℃; Inert atmosphere;99%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

5-tert-butyl-3-methylbenzene-1,2-diol
2213-66-3

5-tert-butyl-3-methylbenzene-1,2-diol

5-(tert-butyl)-3-methyl-1,2-phenylene bis(2,2-dichloroacetate)

5-(tert-butyl)-3-methyl-1,2-phenylene bis(2,2-dichloroacetate)

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;99%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Estrone
53-16-7

Estrone

C20H22Cl2O3

C20H22Cl2O3

Conditions
ConditionsYield
With dmap In dichloromethane at 20℃; for 24h;99%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

ethyl 3-{[{2-amino-1-(methylamino)phen-4-yl}carbonyl](pyridyn-2-yl)amino}propanoate
212322-56-0

ethyl 3-{[{2-amino-1-(methylamino)phen-4-yl}carbonyl](pyridyn-2-yl)amino}propanoate

ethyl 3-{[(2-dichloromethyl-1-methyl-1H-benzimidazole-5-yl)carbonyl]-(2-pyridinyl)amino}propanoate

ethyl 3-{[(2-dichloromethyl-1-methyl-1H-benzimidazole-5-yl)carbonyl]-(2-pyridinyl)amino}propanoate

Conditions
ConditionsYield
In acetonitrile at -15 - 60℃;98.8%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

aniline
62-53-3

aniline

N-phenyl-2,2-dichloroacetamide
2563-99-7

N-phenyl-2,2-dichloroacetamide

Conditions
ConditionsYield
Stage #1: aniline With sodium hydrogencarbonate at 20℃; for 7h; Sonication;
Stage #2: dichloroacethyl chloride In tetrahydrofuran at 60℃; for 8h; Microwave irradiation;
98.6%
With triethylamine In dichloromethane Cooling;86.2%
With triethylamine In dichloromethane86%
2-aminopyridine
504-29-0

2-aminopyridine

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

2,2-dichloro-N-(pyridine-2-yl)acetamide
39089-41-3

2,2-dichloro-N-(pyridine-2-yl)acetamide

Conditions
ConditionsYield
for 1h;98%
With pyridine
With benzene
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

isopropylamine
75-31-0

isopropylamine

N-Isopropyl-2,2-dichloroacetamide
39063-24-6

N-Isopropyl-2,2-dichloroacetamide

Conditions
ConditionsYield
In dichloromethane98%
With 1,2-dichloro-ethane at -20 - -10℃;
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

phenol
108-95-2

phenol

phenyl dichloroacetate
10565-20-5

phenyl dichloroacetate

Conditions
ConditionsYield
With 1,1,1,3,3-pentafluoro-2,3-dichloropropane at 60 - 80℃; for 9h;98%
With triethylamine In dichloromethane Cooling;94.2%
for 3h; Reflux; Alkaline conditions;82%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

2-isopropenylaniline
52562-19-3

2-isopropenylaniline

2,2-Dichloro-N-acetamide
133901-65-2

2,2-Dichloro-N-acetamide

Conditions
ConditionsYield
With triethylamine In diethyl ether for 0.166667h; Ambient temperature;98%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

Aluminum; 2-tert-butyl-4-methyl-phenolate
127354-53-4

Aluminum; 2-tert-butyl-4-methyl-phenolate

A

ω,ω-Dichloro-2-hydroxy-3-tert-butyl-5-methylacetophenone
127354-45-4

ω,ω-Dichloro-2-hydroxy-3-tert-butyl-5-methylacetophenone

B

2-tert-Butyl-4-methylphenyl dichloroacetate
127354-46-5

2-tert-Butyl-4-methylphenyl dichloroacetate

Conditions
ConditionsYield
In toluene for 5h; Ambient temperature;A 98%
B 2%
dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

5-[1-Diphenylamino-meth-(E)-ylidene]-6,7-dihydro-5H-benzo[b]thiophen-4-one
84670-66-6

5-[1-Diphenylamino-meth-(E)-ylidene]-6,7-dihydro-5H-benzo[b]thiophen-4-one

3,3-Dichloro-4-diphenylamino-3,4,5,6-tetrahydro-thieno[2,3-h]chromen-2-one
90236-80-9

3,3-Dichloro-4-diphenylamino-3,4,5,6-tetrahydro-thieno[2,3-h]chromen-2-one

Conditions
ConditionsYield
With triethylamine98%

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