Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parc
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:526-55-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:526-55-6
Min.Order:0 Metric Ton
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inquiryService we can provide: 1. Mixed container: We can mix different items in one container. 2. Quality control: Before shipment, we can provide free sample for test. Inspection before shipping. 3. Packing: We can pack according to your requirem
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:526-55-6
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:526-55-6
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:526-55-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:526-55-6
Min.Order:1 Metric Ton
FOB Price: $90.0 / 100.0
Type:Trading Company
inquiryHubei CuiRan Biotechnology Co., Ltd is a leading company in the research, development, manufacture and marketing of High Quality Phytochemicals and Extracts(especially Active Ingredients from Traditional Chinese Medicine,Traditional Chinese Medicine)
ProductName:Indole-3-ethanol(Tryptophol) Synonyms:beta-3-Indolylethanol;3-(2-Hydroxyethyl)indole;2-(1H-Indol-3-yl)ethan-1-ol CASNo:526-55-6 Appearance:yellowish crystals Storage:store in dry and cool place Package: 25kg/drum, or as per your req
Product Name: Tryptophol Synonyms: INDOLE-3-ETHANOL;B-3-INDOLEETHANOL;B-3-INDOLYLETHANOL;BETA-3-INDOLYLETHANOL;3-(BETA-HYDROXYETHYL)INDOLE;3-INDOLEETHANOL;2-(1H-INDOL-3-YL)ETHAN-1-OL;2-(1H-INDOL-3-YL)-ETHANOL CAS: 526-55-6 MF: C10H11NO MW:
Cas:526-55-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:526-55-6
Min.Order:1 Kilogram
FOB Price: $40.0 / 50.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
526-55-6 C10H11NO TryptopholAppearance:white powder Storage:Normal temperature Package:according to customers' requirements Application:Heterocyclic Compounds;Indoles;Simple Indoles Transportation:By air(EMS or EUB or FedEx
Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
GMP factoryFull experience of large numbers containers loading in main Chinese seaports Packing with pallet as buyer's special request Best service after shipment with e-mail Cargos together with container sales seervice available Rich experience for
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Product name: Indole-3-Ethanol CAS No.:526-55-6 Molecule Formula:C10H11NO Molecule Weight:161.20 Purity: 99.0% Package: 25kg/drum Description:White to almost white crystalline powder Manufacture Standards:Enterprise Standard
Cas:526-55-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:526-55-6
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Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 3h; Reflux; | 100% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 10h; Inert atmosphere; | 96% |
Stage #1: indole-3-acetic acid With 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane at 20℃; for 12h; Inert atmosphere; Stage #2: With silica gel In methanol at 50℃; for 3h; | 92% |
2-(3-indolyl)oxoacetic acid methyl ester
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 12h; | 100% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 70℃; for 5h; Inert atmosphere; | 80% |
With sodium borohydrid In isopropyl alcohol |
3-(2-((tert-butyldimethylsilyl)oxy)ethyl)-1H-indole
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With aluminium(III) chloride hexahydrate In methanol at 100℃; for 0.25h; Solvent; Temperature; Microwave irradiation; Sealed tube; chemoselective reaction; | 98% |
With cerium (IV) sulfate tetrahydrate In methanol at 130℃; for 0.333333h; Microwave irradiation; | 90% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran | 96% |
With isopropyl alcohol In hexane at 0 - 20℃; for 0.583333h; Bouveault-Blanc Reduction; Inert atmosphere; | 81% |
With tetrabutylammonium borohydride In dichloromethane for 10h; Heating; | 69% |
Conditions | Yield |
---|---|
With methanol; Na/SiO2 In tetrahydrofuran at 0 - 25℃; Bouveault-Blanc reduction; Inert atmosphere; | 95% |
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; for 20h; Inert atmosphere; | 81% |
Stage #1: ethyl 3-indoleacetate With polyethylsiloxane; LiTi(OPr-i)4 at 100℃; for 24h; Stage #2: With sodium hydroxide In tetrahydrofuran for 3h; Heating; | 49% |
With lithium aluminium tetrahydride; diethyl ether | |
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 99 %Spectr. |
Conditions | Yield |
---|---|
With sulfuric acid In N,N-dimethyl acetamide; water at 100℃; | 92% |
With L-(+)-tartaric acid-urea melt at 70℃; for 1h; Fischer Indole Synthesis; | 90% |
With montmorillonite K-10 In N,N-dimethyl acetamide; water at 80℃; for 2h; | 75% |
1-triethylsilanyl-4-(triethylsilanyloxy)but-1-yne
2-bromoaniline
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
Stage #1: 1-triethylsilanyl-4-(triethylsilanyloxy)but-1-yne; 2-bromoaniline With 2 mol% Pd/C; sodium carbonate In N,N-dimethyl-formamide at 120℃; for 18h; Larock heteroannulation; Inert atmosphere; Stage #2: With hydrogenchloride In water regioselective reaction; | 87% |
2,3-dihydro-1H-indole-3-ethanol
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With dichloro[1,3-bis(2-methylphenyl)-2-imidazolidinylidene](benzylidene) (tricyclohexylphosphine) ruthenium(II); oxygen In ethyl acetate at 70℃; under 760.051 Torr; for 46h; Sealed tube; | 85% |
Conditions | Yield |
---|---|
With samarium diiodide; water; triethylamine In tetrahydrofuran at 23℃; for 18h; Inert atmosphere; chemoselective reaction; | 82% |
Multi-step reaction with 2 steps 1: aqueous NaOH 2: lithium alanate; diethyl ether View Scheme |
carbon monoxide
2-[3-(tetrahydro-2H-pyran-2-yloxy)prop-1-yn-1-yl]aniline
A
acetic acid 2-(1H-indol-3-yl)ethyl ester
B
2-(3-indole)-ethanol
C
3-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]-1H-indole
Conditions | Yield |
---|---|
With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen; 1,2-bis-(diphenylphosphino)ethane In toluene at 100℃; under 18751.9 Torr; for 8h; regioselective reaction; | A n/a B n/a C 78% |
carbon monoxide
(E)-3-(2-aminophenyl)prop-2-en-1-ol
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen; triphenylphosphine In toluene at 70℃; under 15514.4 Torr; for 70h; | 73% |
Conditions | Yield |
---|---|
With carbonylchloro[4,5-bis(diisopropylphosphinomethyl)acridine]hydridoruthenium(II); water In 1,4-dioxane at 135℃; for 48h; Pressure; Schlenk technique; Inert atmosphere; | 62% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With polymer-supported potassium thiophenolate In tetrahydrofuran; ethylene glycol at 140℃; | 50% |
A
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With ammonia; sodium In tetrahydrofuran at -78 - -50℃; for 4h; | A 22% B 50% |
methanol
2-(Indol-3'-yl)ethyl Trichloroacetate
A
2-(3-indole)-ethanol
B
1,3,4,7-tetrahydro-7,7-dimethoxyoxocino<4,5,6-cd>indol-6-one
Conditions | Yield |
---|---|
With acetonitrile for 0.416667h; Irradiation; | A 48% B 42% |
3-phenylpropanoic acid methyl ester
indole-2,3-dione
lithium diisopropyl amide
A
2-(3-indole)-ethanol
B
β-(phenylmethyl)-1H-indole-ethanol
Conditions | Yield |
---|---|
In tetrahydrofuran; cyclohexane; water; 3-Phenylpropionic acid | A 46.9% B n/a |
Conditions | Yield |
---|---|
With acetic acid In water Reflux; | 46% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With Leptosphaeria maculans In acetonitrile for 24h; Enzymatic reaction; | 32% |
2-(1H-indol-3-yl)-N,N-dimethylacetamide
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With ethanol; sodium In hexane; paraffin oil at 0℃; for 0.0833333h; | 32% |
2-ethoxytetrahydrofuran
phenylhydrazine hydrochloride
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
In ethanol Heating; | 21.5% |
indole
2-acetylaminoethanol
A
2-(3-indole)-ethanol
B
N-Acetyltryptamine
Conditions | Yield |
---|---|
With dichloro(pentamethylcyclopentadienyl) iridium; potassium acetate at 150℃; for 48h; Reagent/catalyst; Inert atmosphere; Sealed tube; | A 10% B 12% C 21% |
carbon monoxide
allyl alcohol
phenylhydrazine
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With hydrogen; toluene-4-sulfonic acid; 6,6′-[(3,3′-di-tert-butyl-5,5′-dimethoxy-1,1′-biphenyl-2,2′-diyl)bis(oxy)]bis(di-benzo[d,f][1,3,2]dioxaphosphepin); acetylacetonatodicarbonylrhodium(l) In 1,4-dioxane at 60 - 100℃; under 15001.2 Torr; for 43h; | 17% |
2-(1-Triisopropylsilanyl-1H-indol-3-yl)-ethanol
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 25℃; for 0.166667h; Yield given; |
4-(trimethylsilyl)but-3-yn-1-ol
2-iodophenylamine
A
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
Yield given; Multistep reaction; |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With sodium methylate In methanol |
Conditions | Yield |
---|---|
With diethyl ether; benzene und folgenden Erhitzen des Reaktionsgemisches auf ca. 100grad nach Abdestillieren des Aethers.; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: diethyl ether 2: diethyl ether / 12 h / 20 °C 3: 100 percent / LiAlH4 / tetrahydrofuran / 12 h / 20 °C View Scheme |
indolyl-3-glyoxylyl chloride
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether / 12 h / 20 °C 2: 100 percent / LiAlH4 / tetrahydrofuran / 12 h / 20 °C View Scheme | |
With sodium borohydrid In diethylene glycol dimethyl ether | |
Multi-step reaction with 2 steps 1: diethyl ether / 0 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / 0.5 h / Reflux; Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: diethyl ether / 0 °C / Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 80 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: NaOMe / methanol View Scheme | |
Multi-step reaction with 2 steps 2: NaOMe / methanol View Scheme |
dichloroacethyl chloride
2-(3-indole)-ethanol
2-(Indol-3'-yl)ethyl Dichloroacetate
Conditions | Yield |
---|---|
With pyridine In dichloromethane for 18h; kept in the dark; | 100% |
2-(3-indole)-ethanol
acetic anhydride
acetic acid 2-(1H-indol-3-yl)ethyl ester
Conditions | Yield |
---|---|
With pyridine; dmap In dichloromethane for 24h; Ambient temperature; | 100% |
With pyridine at 20℃; for 15h; Inert atmosphere; | 99% |
With pyridine for 1h; Ambient temperature; | 55.3 g |
With pyridine at 20℃; for 15h; Inert atmosphere; |
2-(3-indole)-ethanol
tert-butyldimethylsilyl chloride
3-(2-((tert-butyldimethylsilyl)oxy)ethyl)-1H-indole
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran at 0 - 20℃; for 0.5h; Inert atmosphere; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide for 16h; Ambient temperature; | 99% |
2-(3-indole)-ethanol
triisopropylsilyl chloride
3-(2-((triisopropylsilyl)oxy)ethyl)-1H-indole
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; Substitution; | 99% |
2-(3-indole)-ethanol
2,3-dihydro-1H-indole-3-ethanol
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid at 0 - 20℃; for 3.5h; | 100% |
With sodium cyanoborohydride; acetic acid at 0 - 20℃; for 5h; | 38% |
With sodium cyanoborohydride; acetic acid at 0 - 20℃; for 3.5h; Inert atmosphere; | 37.4% |
2-(3-indole)-ethanol
3-dimethylaminomethyl-4-(3-fluorophenyl)-4-hydroxy-cyclohexanone
Conditions | Yield |
---|---|
Stage #1: 2-(3-indole)-ethanol; 3-dimethylaminomethyl-4-(3-fluorophenyl)-4-hydroxy-cyclohexanone With methanesulfonic acid In dichloromethane at 20℃; for 24h; Stage #2: With sodium hydroxide In water Stage #3: With sodium hydroxide In water | 100% |
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 80℃; for 2h; | 99% |
With 2-iodoxybenzoic acid In acetonitrile at 80℃; for 3h; | 91% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide | 87% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 99% |
In N,N-dimethyl-formamide | 99% |
2-(3-indole)-ethanol
4-(Dimethylamino-phenyl-methyl)-cyclohexanone
1,1-[3-(dimethylamino-(phenyl)-methyl)-pentamethylene]-1,3,4,9-tetrahydropyrano[3,4-b]indole
Conditions | Yield |
---|---|
Stage #1: 2-(3-indole)-ethanol; 4-(Dimethylamino-phenyl-methyl)-cyclohexanone With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 6h; Stage #2: With sodium hydroxide; water In dichloromethane | 99% |
2-(3-indole)-ethanol
4-[(4-Chloro-phenyl)-dimethylamino-methyl]-cyclohexanone
1,1-[3-(dimethylamino-(4-chlorophenyl)-methyl)-pentamethylene]-1,3,4,9-tetrahydro-pyrano[3,4-b]indole
Conditions | Yield |
---|---|
Stage #1: 2-(3-indole)-ethanol; 4-[(4-Chloro-phenyl)-dimethylamino-methyl]-cyclohexanone With trifluorormethanesulfonic acid In dichloromethane at 20℃; Stage #2: With sodium hydroxide; water In dichloromethane | 99% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 4h; | 99% |
2-(3-indole)-ethanol
tert-butyl (4,4-dimethoxycyclohexa-2,5-dien-1-ylidene)carbamate
Conditions | Yield |
---|---|
With (R)-6,6'-bis(9-phenanthryl)-1,1'-spirobiindanyl-7,7'-diyl hydrogen phosphate In toluene at 30℃; for 12h; Molecular sieve; stereoselective reaction; | 99% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With (R)-6,6'-bis(9-phenanthryl)-1,1'-spirobiindanyl-7,7'-diyl hydrogen phosphate In toluene at 30℃; for 12h; Molecular sieve; stereoselective reaction; | 99% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform at 40℃; for 8h; chemoselective reaction; | 99% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform at 30℃; for 3h; Molecular sieve; diastereoselective reaction; | 99% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform at 40℃; for 8h; chemoselective reaction; | 99% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform at 40℃; for 8h; chemoselective reaction; | 99% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform at 40℃; for 8h; chemoselective reaction; | 99% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With 5,11,17,23,29,35-hexakis(tert-butyl)-37,38,39,40,41-hexakis(hydroxy)calix[6]arene; copper diacetate; 1-azido-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one; 1-butyl-2,3-methylimidazolium tetrafluoroborate In dimethyl sulfoxide at 45℃; for 1.5h; Solvent; Reagent/catalyst; Inert atmosphere; | 98.5% |
2-(3-indole)-ethanol
2,2-dimethoxy-propane
1,1-dimethyl-1,3,4,9-tetrahydropyrano[3,4-b]indole
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate; water In toluene at 80℃; oxa Pictet-Spengler reaction; | 98% |
With iron(II) triflate In toluene at 70℃; for 24h; Pictet-Spengler Synthesis; Green chemistry; | 98% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; triethyl borane; palladium diacetate In tetrahydrofuran at 20℃; for 48h; Inert atmosphere; diastereoselective reaction; | 98% |
2-(3-indole)-ethanol
methanesulfonic acid
4-morpholino-4-phenylcyclohexanone
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 16h; | 98% |
2-(3-indole)-ethanol
4-methylacetophenone dimethyl acetal
Conditions | Yield |
---|---|
With 2,3,4,5-tetrabromo-6-(((1R,2R)-2-(3-(4-nitro-3-(trifluoromethyl)phenyl)thioureido)-cyclohexyl)carbamoyl)benzoic acid In toluene at -30℃; for 18h; Pictet-Spengler Synthesis; Molecular sieve; Inert atmosphere; enantioselective reaction; | 98% |
Conditions | Yield |
---|---|
With iron(II) triflate; (S)-(+)-N-(3,5-dioxa-4-phosphacyclohepta-[2,1-a;3,4-a′]dinaphthalen-4-yl)dibenz[b,f]azepine; bis(1,5-cyclooctadiene)diiridium(I) dichloride In diethyl ether at 20℃; for 8h; Reagent/catalyst; Time; Temperature; Solvent; enantioselective reaction; | 97% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In tetrahydrofuran at 25℃; for 5h; Molecular sieve; Inert atmosphere; | 97% |
2-(3-indole)-ethanol
[bromo(difluoro)methyl](trimethyl)silane
Conditions | Yield |
---|---|
With potassium hydrogenfluoride In dichloromethane at 20℃; for 2h; | 97% |
With potassium hydrogen difluoride In dichloromethane; water at 20℃; for 10h; Reagent/catalyst; | 93% |
2-(3-indole)-ethanol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform at 30℃; for 3h; Catalytic behavior; Reagent/catalyst; Temperature; Solvent; Molecular sieve; diastereoselective reaction; | 97% |
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