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inquiryProName: (R)-(+)-Limonene Manufacturer/High qua... CasNo: 5989-27-5 Molecular Formula: C10H16 Appearance: colorless oily liquid Application: It is an important raw material and in... DeliveryTime: prompt PackAge: accordin
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inquiry(+)-Dipentene CAS:5989-27-5 Specification Items Specification Result Assay ≥95% 95.02% Apperance Colorless or light yellow transp
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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(R)-(+)-Limonene CAS NO.5989-27-5 Application:(R)-(+)-Limonene CAS NO.5989-27-5
Xiamen Luyunjia Trading Co.,Ltd Package:1kg/bag; 2689kg/drum, or as customer's request. Application:Xiamen Luyunjia Trading Co.,Ltd Transportation:DHL, EMS, FedEx, TNT, AIR, SEA Port:Beijing,Shanghai,Guangzhou ,China main port
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inquiryRaw material ,higher purity, support by origional factory, fully large stock [Physical/Chemical Property] Melting Point -75-73°C Specific optical rotation 112o (10% IN ETHANOL) Boiling point 176-177°C (lit.) Density 0
D-Limonene: is a monoterpene found to prevent mammary cancer by activating hepatic glutathione-S-transferase (GST) and uridine diphosphoglucuronosyl transferase (UGT). D-Limonene is an isoprenylation inhibitor of small G-proteins. Servic
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D-limonene
Conditions | Yield |
---|---|
With ammonia; lithium | 80% |
L-carveol
D-limonene
Conditions | Yield |
---|---|
With 2-nitrobenzenesulfonyl hydrazide; triphenylphosphine; diethylazodicarboxylate In various solvent(s) -30 deg, 1 h; 23 deg C 30 min; | 78% |
Conditions | Yield |
---|---|
With triethylsilane; lithium perchlorate In diethyl ether for 16h; Ambient temperature; | 68% |
D-limonene
Conditions | Yield |
---|---|
With aluminum amalgam In tetrahydrofuran; water at 20℃; for 4h; | 58% |
D-limonene
Conditions | Yield |
---|---|
With acetic acid at 120℃; | 22% |
Conditions | Yield |
---|---|
With fired clay at 25℃; | |
With fired clay; acetic anhydride; acetic acid at 10℃; | |
With fired clay; acetic anhydride; acetic acid at 25℃; |
Pinene
2,4,6-Trinitrophenol
benzene
A
D-limonene
C
(+)-camphene
D
limonene.
Conditions | Yield |
---|---|
at 120℃; d-α-pinene; |
2-Benzoylbenzoic acid
(+)-α-pinene
formamide
D-limonene
Conditions | Yield |
---|---|
at 140℃; |
2-Benzoylbenzoic acid
(1R,5R)-(+)-β-pinene
formamide
D-limonene
Conditions | Yield |
---|---|
at 140℃; |
(R)-(+)-binaphthol mononeryl ether
A
Terpinolene
B
D-limonene
C
(-)-(S)-limonene
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; tri-tert-butylphenol; diisobutylaluminium hydride 2.) 3 h, -130 deg C, CCl3F; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
With (2,4,6-tri-tert-butylphenoxy)-isobutylaluminium trifluormethanesulfonate In trichlorofluoromethane at -130℃; for 3h; further reagents; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
(-)-{1-(R)-[(1E)-2-methylbuta-1,3-dienyloxy]ethyl}benzene
isoprene
A
D-limonene
B
(-)-trans-carveol
C
(+)-trans-carveol
D
(-)-(S)-limonene
Conditions | Yield |
---|---|
at 50℃; under 135011 Torr; for 60h; Product distribution; other conditions; other 1-(1-arylalkoxy)-2-methyl-1,3-butadienes; enantioselectivity of the reaction; |
[(S)-2,2-Dimethyl-1-((E)-2-methyl-buta-1,3-dienyloxy)-propyl]-benzene
isoprene
A
D-limonene
B
(-)-trans-carveol
C
(+)-trans-carveol
D
(-)-(S)-limonene
Conditions | Yield |
---|---|
at 50℃; under 135011 Torr; for 60h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
[(R)-2,2-Dimethyl-1-((E)-2-methyl-buta-1,3-dienyloxy)-propyl]-benzene
isoprene
A
D-limonene
B
(-)-trans-carveol
C
(+)-trans-carveol
D
(-)-(S)-limonene
Conditions | Yield |
---|---|
at 50℃; under 135011 Torr; for 60h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
[(S)-2-Methyl-1-((E)-2-methyl-buta-1,3-dienyloxy)-propyl]-benzene
isoprene
A
D-limonene
B
(-)-trans-carveol
C
(+)-trans-carveol
D
(-)-(S)-limonene
Conditions | Yield |
---|---|
at 50℃; under 135011 Torr; for 60h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
D-limonene
Conditions | Yield |
---|---|
With dihydrogen peroxide In tert-butyl alcohol 1.) 25 deg C, 110 h, 2.) 150 deg C, 1 torr, 1 h; Yield given; |
methanol
(1R,4R,5R)-4,7,7-trimethyl-6-thiabicyclo[3.2.1]octane
A
trans-1,4-menthane
B
cis-1-isopropyl-4-methyl-cyclohexane
C
D-limonene
D
(+)-p-menth-1-ene
linalool
A
7-methyl-3-methene-1,6-octadiene
B
Geraniol
C
terpineol
D
D-limonene
Conditions | Yield |
---|---|
at 159℃; |
formic acid
Pinene
A
Terpinolene
B
D-limonene
C
limonene.
Conditions | Yield |
---|---|
d-α-pinene; |
Conditions | Yield |
---|---|
at 0℃; d-limonene tetrabromide; |
Conditions | Yield |
---|---|
d-limonene tetrabromide; |
Conditions | Yield |
---|---|
Mechanism; |
Conditions | Yield |
---|---|
Mechanism; |
(+)-α-pinene
acetic acid
A
terpineol
B
D-limonene
rac-endo-borneol
D
1,7,7-trimethyl bicyclo[2.2.1]heptan-2-ol
Conditions | Yield |
---|---|
at 30℃; anschl. Verseifen; |
Conditions | Yield |
---|---|
at 10℃; |
(1S)-endo-fenchylamine
acetic acid
A
D-limonene
B
α-fenchene
C
(+)-cyclofenchene
Conditions | Yield |
---|---|
Produkt 5: (+)-α-Terpineol, Produkt 6: (-)-α-Fenchol, Produkt 7: (-)-β-Fenchol und Produkt 8: (-)-α-Fenchenhydrat; |
α-terpinyl chloride
A
Terpinolene
B
D-limonene
C
(-)-(S)-limonene
Conditions | Yield |
---|---|
With 2,4,6-trimethyl-pyridine for 8h; Heating; Title compound not separated from byproducts; |
A
1-methyl-4-isopropyl-1,3-cyclohexadiene
B
α-terpinyl chloride
C
D-limonene
D
(-)-(S)-limonene
Conditions | Yield |
---|---|
With tin(IV) chloride In various solvent(s) at -78℃; for 12h; Product distribution; Further Variations:; Solvents; Reagents; Temperatures; time; |
Conditions | Yield |
---|---|
With tin(ll) chloride In dichloromethane at -97℃; for 6h; Product distribution; Further Variations:; Solvents; Temperatures; time; |
Conditions | Yield |
---|---|
With iron(III) chloride; lithium aluminium tetrahydride; hydrogen In tetrahydrofuran at 18℃; under 7500.75 Torr; for 20h; Inert atmosphere; Sealed tube; | 100% |
With ethanol; lithium; nickel dichloride; 4,4'-di-tert-butylbiphenyl In tetrahydrofuran at 20℃; for 22h; | 99% |
With platinum(IV) oxide; hydrogen under 775.743 Torr; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With urea hydrogen peroxide adduct; methyltrioxorhenium(VII) In dichloromethane at 20℃; for 0.5h; | 99% |
With tert.-butylhydroperoxide In decane at 55℃; for 3h; in air; regioselective reaction; | 95% |
With C15H34N(1+)*H2O4P(1-); Tri(dodecyltrimethylammonium) dodecatungstophosphate; dihydrogen peroxide In water; toluene at 65℃; for 6h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With fac-tris(2-phenylpyridinato-N,C2')iridium(III) In toluene at 20℃; for 36h; Sealed tube; Irradiation; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; polystyrene; {2-(aminomethyl)pyridine}methyl(trioxo)rhenium(VII) In dichloromethane; water; acetonitrile at -10℃; for 2h; | 98% |
With dihydrogen peroxide; divinylbenzene cross-linked poly(4-vinylpyridine); methyltrioxorhenium(VII) In dichloromethane; water; acetonitrile at 25℃; for 1.5h; | 89% |
Multi-step reaction with 2 steps 1: bis[(4R)-2(4-Et-3,4-dihydro-2-oxazolyl)phenolato-N,O]O(O2)Mo; aq. tert-butyl hydroperoxide / toluene / 22 h / 20 °C 2: (μ-O)[MoO2(NCS)-2-(3,4-dihydro-4-MeOMe-oxazolyl-Ph)Py-N,N]2; aq. tert-butyl hydroperoxide / toluene / 22 h / 20 °C View Scheme |
D-limonene
Conditions | Yield |
---|---|
With zeolite NaY; oxygen Irradiation; photooxygenation; | 97% |
Conditions | Yield |
---|---|
Stage #1: diphenylsilane With [(2-dicyclohexylphosphinocyclopentene-1-(2,6-dimethylphenyl)imine)Ni(allyl)]OTf In benzene-d6 at 20℃; for 0.0833333h; Inert atmosphere; Glovebox; Stage #2: D-limonene In benzene-d6 at 20℃; for 12h; Inert atmosphere; Sealed tube; | 97% |
With [N,N'-(1,2-dimethyl-1,2-ethanediylidene)bis[3-(diphenylphosphino)-1-propanamine]]Ni In benzene-d6 at 70℃; for 168h; Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
With n-butyllithium; 2,6-bis-[1-(2,6-diethylphenylimino)ethyl]pyridine iron(II) chloride In hexane; toluene at 20℃; for 1h; Inert atmosphere; regioselective reaction; | 96% |
Stage #1: phenylsilane With (C5Me5)(iPr2MeP)H2FeH(N2); trityl tetrakis(pentafluorophenyl)borate In fluorobenzene at -35 - 20℃; Stage #2: D-limonene In fluorobenzene at 20℃; for 20h; regioselective reaction; | 92% |
yttrium(pentamethylcyclopentadienyl)2CH(trimethylsilyl)2 In benzene for 96h; Ambient temperature; | 61% |
(η5-C5Me4(i)Pr)2YMe*THF for 96h; Product distribution; Ambient temperature; other catalysts; | |
With [(2,6-iPr2PhBDI)Mn(μ-H)]2 In benzene-d6 at 130℃; for 144h; Inert atmosphere; |
D-limonene
A
(R)-8,9-limonene oxide
(1RS,2SR,4R)-limonene-1,2-epoxide
Conditions | Yield |
---|---|
With 1H-imidazole; dihydrogen peroxide; sodium N-dodecanoyl-L-proplinate; Mn[5-(4-C6H4CO-(N-L-proline))-10,15,20-Ph3-porphyrinyl]Cl In ethanol; water at 25℃; for 0.166667h; Product distribution; Further Variations:; Catalysts; Reagents; | A n/a B 95% |
Conditions | Yield |
---|---|
With acetyl chloride In ethanol at 30℃; for 0.166667h; Markovnikov hydrochlorination; | 95% |
Multi-step reaction with 2 steps 1: 250 - 270 °C 2: diethyl ether; hydrogen chloride View Scheme |
D-limonene
A
trans-1,4-menthane
B
cis-1-isopropyl-4-methyl-cyclohexane
C
(+)-p-menth-1-ene
Conditions | Yield |
---|---|
With hydrogen; 2 In neat (no solvent) | A 2% B 4% C 94% |
With ruthenium; hydrogen at 30℃; under 900.09 Torr; Reagent/catalyst; |
Conditions | Yield |
---|---|
With hydrogen; chloro(1,5-cyclooctadiene)rhodium(I) dimer In acetonitrile at 80℃; under 60004.8 Torr; for 20h; | 93% |
Stage #1: morpholine; carbon monoxide; D-limonene With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen In tetrahydrofuran at 100℃; Autoclave; Stage #2: With hydrogen In tetrahydrofuran at 100℃; under 30003 Torr; Autoclave; | 79% |
D-limonene
(1S,2R,4R)-1-methyl-4-(prop-1-en-2-yl)cyclohexane-1,2-diol
Conditions | Yield |
---|---|
With oxygen; potassium carbonate In water at 25℃; under 1551.49 Torr; for 72h; enantioselective reaction; | 92% |
D-limonene
2-bromo-1-hydroxy-p-menth-8-ene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In water; acetone at 10℃; | 91% |
D-limonene
(1S,4R)-2-chloro-4-(1-methylvinyl)-1-methylcyclohexanol
Conditions | Yield |
---|---|
With sodium hypochlorite; water; copper(II) acetate monohydrate In 1,2-dichloro-ethane at 60℃; for 9h; Temperature; Solvent; | 90.2% |
D-limonene
p-menth-1-ene
Conditions | Yield |
---|---|
With hydrogen; platinum on activated charcoal pressure of 60 lb/sq in. to 43.5 lb/sq in.; | 90% |
With copper at 200℃; inactive substances; | |
With hydrogen; platinum dihydrolimonene; | |
With sodium tetrahydroborate In methanol at 20℃; Catalytic behavior; Reagent/catalyst; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: D-limonene With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran at 0 - 25℃; for 2.5h; Inert atmosphere; Stage #2: With palladium 10% on activated carbon; hydrogen In tetrahydrofuran under 760.051 Torr; Inert atmosphere; Stage #3: With 2-methyl-2-nitrosopropane dimer In tetrahydrofuran for 0.75h; regioselective reaction; | 90% |
ethanol
carbon monoxide
D-limonene
B
3-(4-methylcyclohex-3-enyl)butanal
Conditions | Yield |
---|---|
With methoxy(cyclooctadiene)rhodium(I) dimer; tri(o-t-butylphenyl)phosphite; hydrogen at 80℃; under 60804.1 Torr; for 4h; Inert atmosphere; Autoclave; | A 90% B n/a |
D-limonene
(2RS)-2-<(1R)-4-methylcyclohex-3-enyl>propanol
Conditions | Yield |
---|---|
Stage #1: D-limonene With PS-9-BBN In tetrahydrofuran at 40℃; for 24h; Stage #2: With tetra(n-butyl)ammonium hydroxide; dihydrogen peroxide In tetrahydrofuran; methanol at 0 - 50℃; for 4h; | 89% |
Stage #1: D-limonene With 9-bora-bicyclo[3.3.1]nonane at 20℃; Inert atmosphere; Stage #2: With dihydrogen peroxide; sodium hydroxide In ethanol at 50℃; for 2h; | 89.6% |
Stage #1: D-limonene With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran at 20℃; for 2h; Stage #2: With sodium hydroxide; dihydrogen peroxide In tetrahydrofuran; water temp. < 10 deg C; Stage #3: In tetrahydrofuran; water at 40℃; for 2h; | 80% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon at 140℃; for 1h; | 89% |
With iodine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 0.75h; Reflux; | 82% |
With dodecane; hydrogen at 300℃; under 11251.1 Torr; for 2h; Catalytic behavior; Temperature; Autoclave; Inert atmosphere; | 57% |
Conditions | Yield |
---|---|
Stage #1: piperazine; carbon monoxide; D-limonene With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen In tetrahydrofuran at 100℃; Autoclave; Stage #2: With hydrogen In tetrahydrofuran at 100℃; under 30003 Torr; Autoclave; | 89% |
D-limonene
Conditions | Yield |
---|---|
With sodium hypobromide; copper(II) acetate monohydrate In water; 1,2-dichloro-ethane at 80℃; for 6h; Reagent/catalyst; Temperature; | 88.3% |
With N-Bromosuccinimide; water In acetone at 0 - 5℃; | 85% |
With N-Bromosuccinimide; water In acetone at 0 - 25℃; for 1h; Large scale; chemoselective reaction; | |
With N-Bromosuccinimide In water; acetone at 0 - 25℃; for 1h; | |
With N-Bromosuccinimide In water; acetone at 0℃; for 0.666667h; Inert atmosphere; Schlenk technique; Glovebox; |
D-limonene
(+)-limonene tetrabromide
Conditions | Yield |
---|---|
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; cetyltrimethylammonim bromide In dichloromethane; chloroform | 87% |
D-limonene
(R)-4-methyl-3-(3'-oxobutyl)pent-4-enal
Conditions | Yield |
---|---|
Stage #1: D-limonene With pyridine; ozone In methanol at -50℃; for 12h; Inert atmosphere; Stage #2: With dimethylsulfide In methanol at -50℃; | 86% |
Stage #1: D-limonene With oxygen; ozone In methanol; dichloromethane at -70℃; Stage #2: With dimethylsulfide at 20℃; for 5h; | 70% |
Stage #1: D-limonene With ozone In methanol; dichloromethane at -70℃; Stage #2: With dimethylsulfide In methanol; dichloromethane at 20℃; for 5h; | 70% |
Conditions | Yield |
---|---|
With manganese triacetate; acetic acid at 70℃; for 2h; | 86% |
Conditions | Yield |
---|---|
With manganese triacetate; acetic acid at 70℃; for 1.5h; | 86% |
Conditions | Yield |
---|---|
With manganese triacetate; acetic acid at 70℃; for 1.5h; | 86% |
Conditions | Yield |
---|---|
With platinum(IV) oxide; hydrogen at 20℃; under 760.051 Torr; Overall yield = 16 g; | A n/a B 85% |
With (bis-1,2-diphenylphosphinoethane)Co(CH2SiMe3)2; hydrogen In benzene at 25℃; under 3040.2 Torr; for 6h; Time; | A 55% B 42% |
With hydrogen; platinum(IV) oxide In methanol under 760 Torr; below 20 deg C; Yield given. Yields of byproduct given; | |
With platinum(IV) oxide; hydrogen In ethanol at 20℃; under 760.051 Torr; for 5.4h; |
D-limonene
(R)-8,9-limonene oxide
Conditions | Yield |
---|---|
With perchloric acid; dihydrogen peroxide In water; acetonitrile; tert-butyl alcohol at 60℃; for 0.166667h; stereoselective reaction; | 85% |
With fluorapatite; dihydrogen peroxide; tris(cetylpyridinium) 12-tungstophosphate In water at 25℃; for 14h; | 61% |
With tert.-butylhydroperoxide In water; acetonitrile at 70℃; for 24h; | 35% |
Conditions | Yield |
---|---|
With zinc(II) chloride at 20℃; for 2h; | 85% |
With zinc(II) chloride at 20℃; Inert atmosphere; | 85% |
With zinc(II) chloride |
Conditions | Yield |
---|---|
Stage #1: propylamine; carbon monoxide; D-limonene With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen In tetrahydrofuran at 100℃; Autoclave; Stage #2: With hydrogen In tetrahydrofuran at 100℃; under 30003 Torr; Autoclave; | 85% |
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