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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Butyltintrichloride Manufacturer/High quality/Best price/In stock

Cas:1118-46-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Butyltin Trichloride supplier in China

Cas:1118-46-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

Butyltin trichloride

Cas:1118-46-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply N-butyltin trichloride

Cas:1118-46-3

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% Butyltintrichloride 1118-46-3 ISO Producer

Cas:1118-46-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Butyltin trichloride

Cas:1118-46-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Product Name: Butyltin trichloride Synonyms: butylstanniumtrichloride;butyltrichloro-stannan;chloridn-butylcinicity;chloridn-butylcinicity(czech);mono-n-butyltintrichloride;monotributyltintrichloride;n-butyl-titrichloride;Stannane, but

1118-46-3 Butyltin trichloride

Cas:1118-46-3

Min.Order:1 Gram

FOB Price: $8900.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 2) All Purity≥98% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be sent out in 24 hours after payment.Tracking number available 2) Secure and disc

Butyltin trichloride CAS:1118-46-3

Cas:1118-46-3

Min.Order:1 Kilogram

FOB Price: $150.0 / 200.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 1118-46-3 with best quality

Cas:1118-46-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product name: Butyltin Trichloride CAS No.: 1118-46-3 Molecular formula: C4H9Cl3Sn EINECS No.: 214-263-6 Molecular weight: 282.18 Package: 25kgs or 200kgs plastic drum

Butyltin Trichloride

Cas:1118-46-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

Butyltintrichloride Manufacturer/High quality/Best price/In stock

Cas:1118-46-3

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

Type:Manufacturers

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Butyltintrichloride 1118-46-3

Cas:1118-46-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: Butyltin trichloride CAS: 1118-46-3 MF: C4H9Cl3Sn MW: 282.18 EINECS: 214-263-6 Mol File: 1118-46-3.mol Butyltin trichloride Structure Butyltin trichloride Chemical Properties Melting point -63°C Boiling point

Butyltin trichloride

Cas:1118-46-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

Butyltin trichloride/MBTC/CAS:1118-46-3

Cas:1118-46-3

Min.Order:1 Kilogram

FOB Price: $10.0 / 15.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

Butyltin trichloride CAS:1118-46-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter

Butyltin trichloride CAS:1118-46-3

Cas:1118-46-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Butyltintrichloride

Cas:1118-46-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

Butyltintrichloride CAS NO.1118-46-3

Cas:1118-46-3

Min.Order:10 Gram

Negotiable

Type:Trading Company

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Lonwin Chemical Group Limited

Butyltintrichloride CAS: 1118-46-3 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The IR spectru

Factory supply Butyltintrichloride

Cas:1118-46-3

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Butyltintrichloride

Cas:1118-46-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Free sample Butyltin trichloride CAS:1118-46-3 with fast delivery

Cas:1118-46-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

BUTYLTIN TRICHLORIDE

Cas:1118-46-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Butyltin trichloride

Cas:1118-46-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Butyltin Trichloride

Cas:1118-46-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Hangzhou Lingrui Chemical Co.,Ltd.

Butyltin trichloride CAS NO.1118-46-3Appearance:White or off-white Solid Storage:Store in dry, dark and ventilated place. Package:according to customers' requirements Application:Organic synthesis Transportation:By air(EMS or EUB or FedEx or TNT ect.

Butyltin trichloride CAS NO.1118-46-3

Cas:1118-46-3

Min.Order:1 Gram

Negotiable

Type:Other

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Free sample Butyltin trichloride CAS:1118-46-3 with fast delivery

Cas:1118-46-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colourless or light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceu

Butyltintrichloride

Cas:1118-46-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Siwei Development Group Ltd.

Product name: Butyltin Trichloride CAS No.:1118-46-3 Molecule Formula:C4H9Cl3Sn Molecule Weight:282.18 Purity: 98.0% Package: 25kg/drum Description:clear or yellowish oily liquid Manufacture Standards:Enterprise Standard

Best Quality Butyltin Trichloride

Cas:1118-46-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Reliable Quality Butyltin trichloride

Cas:1118-46-3

Min.Order:0

Negotiable

Type:Trading Company

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HANGZHOU TIANYE CHEMICALS CO., LTD.

We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:Butyltin trichloride CAS No:1118-46-3

Butyltin trichloride

Cas:1118-46-3

Min.Order:1 Gram

Negotiable

Type:Trading Company

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Free sample Butyltin trichloride CAS:1118-46-3 with fast delivery

Cas:1118-46-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Synthetic route

tetra-n-butyltin(IV)
1461-25-2

tetra-n-butyltin(IV)

tin(IV) chloride
7646-78-8

tin(IV) chloride

A

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

B

dibutyltin chloride
683-18-1

dibutyltin chloride

Conditions
ConditionsYield
molar ratio of Sn(C4H9)4:SnCl4 = 1:3, 8 h, 203°C;A 96%
B n/a
molar ratio of Sn(C4H9)4:SnCl4 = 1:3, 8 h, 203°C;A 96%
B n/a
molar ratio of Sn(C4H9)4:SnCl4 = 1:2, 3 h, 100°C;
dibutyltin chloride
683-18-1

dibutyltin chloride

tin(IV) chloride
7646-78-8

tin(IV) chloride

A

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

B

tin(ll) chloride

tin(ll) chloride

Conditions
ConditionsYield
cis-dichlorobis(triphenylphosphine)platinum(II) In toluene stirred for 2 h at 110°C, catalyst added stirred for 12 h at 110°C; cooled to room temp., filtered, ppt. (SnCl2) washed (toluene), dried, filtrate evapd. (vac.), distilled (90°C/11 mm Hg);A 83%
B 3.7%
cis-dichlorobis(triphenylphosphine)platinum(II) In toluene stirred for 12 h at 110°C; cooled to room temp., filtered, ppt. (SnCl2) washed (toluene), dried, filtrate evapd. (vac.), distilled (90°C/11 mm Hg); elem. anal.;A 80%
B 13%
cis-dichlorobis(triphenylphosphine)platinum(II) In o-xylene stirred for 12 h at 110°C; cooled to room temp., filtered, ppt. (SnCl2) washed (toluene), dried; NMR;A n/a
B 19%
hydrogenchloride
7647-01-0

hydrogenchloride

butyltriphenyltin
2847-57-6

butyltriphenyltin

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

Conditions
ConditionsYield
In diethyl ether; dichloromethane at -78 - 20℃; for 12.5h;80%
In diethyl ether; dichloromethane at -78 - 20℃; for 12.5h;80%
n-Butyl chloride
109-69-3

n-Butyl chloride

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

Conditions
ConditionsYield
With stannous chloride; iodine; magnesium In tetrahydrofuran; toluene55%
2-Phenylbutyryl chloride
36854-57-6

2-Phenylbutyryl chloride

butyltriphenyltin
2847-57-6

butyltriphenyltin

A

1,2-diphenyl-butan-1-one
16282-16-9

1,2-diphenyl-butan-1-one

B

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

Conditions
ConditionsYield
With indium In neat (no solvent) at 80℃; for 0.25h; Inert atmosphere; Sonication; regioselective reaction;A 25%
B n/a
butyl magnesium bromide
693-04-9

butyl magnesium bromide

SnCl4

SnCl4

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

tetra-n-butyltin(IV)
1461-25-2

tetra-n-butyltin(IV)

tin(IV) chloride
7646-78-8

tin(IV) chloride

A

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

B

dibutyltin chloride
683-18-1

dibutyltin chloride

C

tributyltin chloride
1461-22-9

tributyltin chloride

Conditions
ConditionsYield
With aluminium trichloride 6 h, 100°C;
200°C, 10 Torr;
molar ratio of educts = 1:1, 0-20°C;
With aluminium trichloride 6 h, 100°C;
200°C, 10 Torr;
tetra-n-butyltin(IV)
1461-25-2

tetra-n-butyltin(IV)

tin(IV) chloride
7646-78-8

tin(IV) chloride

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

Conditions
ConditionsYield
6 h, 160°C;
tetra-n-butyltin(IV)
1461-25-2

tetra-n-butyltin(IV)

tin(IV) chloride
7646-78-8

tin(IV) chloride

A

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

B

tributyltin chloride
1461-22-9

tributyltin chloride

Conditions
ConditionsYield
molar ratio of educts = 1:1, 0-50°C;
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

tetramethylstannane
594-27-4

tetramethylstannane

A

dimethyltin dichloride
753-73-1

dimethyltin dichloride

B

butyl-methyl-tin dichloride
15649-24-8

butyl-methyl-tin dichloride

Conditions
ConditionsYield
2-fold excess of C4H9SnCl3, 180°C, 2h;A n/a
B 99.4%
2-fold excess of C4H9SnCl3, 180°C, 2h;A n/a
B 99.4%
ammonium hydroxide
1336-21-6

ammonium hydroxide

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

sodium carbonate
497-19-8

sodium carbonate

n-butylstannoic acid
2273-43-0

n-butylstannoic acid

Conditions
ConditionsYield
In water at 60℃; for 2.5h; Temperature;99.4%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

sodium O,O-diisopropyl dithiophosphate
27205-99-8

sodium O,O-diisopropyl dithiophosphate

BuSn(S2P(OPr-i)2)2Cl

BuSn(S2P(OPr-i)2)2Cl

Conditions
ConditionsYield
In benzene byproducts: sodium chloride; BuSnCl3 in benzene added to suspn. (Pr-i-O)2PS2Na in benzene (molar ratio 1:2) and mixt. refluxed for 3 h; NaCl filtered off, solvent removed under reduced pressure; elem. anal.;99%
1-benzylimidazole
4238-71-5

1-benzylimidazole

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

[C4H9SnCl3(C6H5CH2C3H3N2)2]
175351-02-7

[C4H9SnCl3(C6H5CH2C3H3N2)2]

Conditions
ConditionsYield
In diethyl ether room temp.; filtration, washing (Et2O); elem. anal.;99%
thiobenzoic acid potassium salt
28170-13-0

thiobenzoic acid potassium salt

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

(butyl)Sn(Cl)2(thiobenzoate)
869111-75-1

(butyl)Sn(Cl)2(thiobenzoate)

Conditions
ConditionsYield
In dichloromethane byproducts: KCl; soln. of butyltin trichloride added to suspn. of potassium thiobenzoate at room temp., stirred for 1 h; ppt. filtered off, solvent evapd. under reduced pressure, dried at 0.05 Torr and 28 °C; elem. anal.;99%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

sodium O,O-diisopropyl dithiophosphate
27205-99-8

sodium O,O-diisopropyl dithiophosphate

BuSn(S2P(OPr-i)2)3

BuSn(S2P(OPr-i)2)3

Conditions
ConditionsYield
In benzene byproducts: sodium chloride; BuSnCl3 in benzene added to suspn. (Pr-i-O)2PS2Na in benzene (molar ratio 1:3) and mixt. refluxed for 3 h; NaCl filtered off, solvent removed under reduced pressure; elem. anal.;98%
ammonium O,O-(2,2-dimethyltrimethylene)dithiophosphate
74862-75-2

ammonium O,O-(2,2-dimethyltrimethylene)dithiophosphate

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

CH3(CH2)3SnCl[S2(POCH2C(CH3)2CH2O)]2
104063-75-4

CH3(CH2)3SnCl[S2(POCH2C(CH3)2CH2O)]2

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; a soln. of monoorganotin(IV) chloride is added to a suspn. of ammonium O,O-alkylenedithiophosphate in 1:2 molar ratio (room temp.); mixt. stirred (3-4 h); filtered; solvent removed (reduced pressure); elem. anal.;97%
ammonium tetramethylethylene dithiophosphate
86428-81-1

ammonium tetramethylethylene dithiophosphate

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

CH3(CH2)3Sn[S2(POC(CH3)2C(CH3)2O)]3
104050-69-3

CH3(CH2)3Sn[S2(POC(CH3)2C(CH3)2O)]3

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; a soln. of monoorganotin(IV) chloride is added to a suspn. of ammonium O,O-alkylenedithiophosphate in 1:3 molar ratio (room temp.); mixt. stirred (3-4 h); filtered; solvent removed (reduced pressure); elem. anal.;97%
methanol
67-56-1

methanol

2-[[(2-hydroxyphenyl)imino]methyl]phenol
1761-56-4

2-[[(2-hydroxyphenyl)imino]methyl]phenol

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

[Sn(n-Bu)Cl(2-([(2-hydroxyphenyl)imino]methyl)phenolato)(methanol)]
404834-66-8

[Sn(n-Bu)Cl(2-([(2-hydroxyphenyl)imino]methyl)phenolato)(methanol)]

Conditions
ConditionsYield
In methanol (N2); Sn compd. added to a hot ligand soln., stirred for 8 h; ppt. filtered off, washed (MeOH); elem. anal.;96%
3-phthalimidopropanoic acid
3339-73-9

3-phthalimidopropanoic acid

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

sodium methylate
124-41-4

sodium methylate

C4H9Sn(COC6H4CONCH2CH2COO)3

C4H9Sn(COC6H4CONCH2CH2COO)3

Conditions
ConditionsYield
In methanol byproducts: NaCl; mixing organic compounds, refluxing for about 2 h, addn. of tin compound, refluxing for 6 h; filtn., evapn. of filtrate under reduced pressure, recrystn. (chloroform-hexane), elem. anal.;95%
1-methyl-1H-imidazole
616-47-7

1-methyl-1H-imidazole

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

trichlorobutylbis(1-methylimidazole)tin(IV)
207740-04-3

trichlorobutylbis(1-methylimidazole)tin(IV)

Conditions
ConditionsYield
In diethyl ether N2-atmosphere; stirring Sn-compd. with excess of ligand (room temp., pptn.); filtration (after 3 h), washing (Et2O); elem. anal.;95%
1H-imidazole
288-32-4

1H-imidazole

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

trichlorobutylbis(imidazole)tin(IV)
220335-19-3

trichlorobutylbis(imidazole)tin(IV)

Conditions
ConditionsYield
In diethyl ether N2-atmosphere; stirring (room temp., 6 h); filtering, washing (Et2O), drying (vac., 20°C, 0.1 Torr); elem. anal.;95%
thiobenzoic acid potassium salt
28170-13-0

thiobenzoic acid potassium salt

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

(butyl)Sn(Cl)(thiobenzoate)2
869111-74-0

(butyl)Sn(Cl)(thiobenzoate)2

Conditions
ConditionsYield
In dichloromethane byproducts: KCl; soln. of butyltin trichloride added to suspn. of potassium thiobenzoate at room temp., stirred for 1 h; ppt. filtered off, solvent evapd. under reduced pressure, dried at 0.05 Torr and 28 °C, recrystd. from diethyl ether/n-hexane mixture; elem. anal.;95%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

sodium O,O-diisopropyl dithiophosphate
27205-99-8

sodium O,O-diisopropyl dithiophosphate

BuSn(S2P(OPr-i)2)Cl2

BuSn(S2P(OPr-i)2)Cl2

Conditions
ConditionsYield
In benzene byproducts: sodium chloride; BuSnCl3 in benzene added to suspn. (i-PrO)2PS2Na in benzene (molar ratio 1:1) and mixt. refluxed for 3 h; NaCl filtered off, solvent removed under reduced pressure; elem. anal.;94%
sodium O,O'-di(3,5-dimethylphenyl)dithiophosphate
1582766-55-9

sodium O,O'-di(3,5-dimethylphenyl)dithiophosphate

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

C40H54O4P2S4Sn

C40H54O4P2S4Sn

Conditions
ConditionsYield
In toluene at 20℃; for 24h; Inert atmosphere; Schlenk technique;94%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

2-hydroxyethanethiol
60-24-2

2-hydroxyethanethiol

(Sn(C4H9)(Cl)((OCH2CH2S)2Sn(C4H9))2)

(Sn(C4H9)(Cl)((OCH2CH2S)2Sn(C4H9))2)

Conditions
ConditionsYield
With sodium In ethanol under Ar atm. 2-mercaptoethanol and metallic sodium were mixed in ethanol with stirring, soln. was refluxed for 1 h, soln. was cooled and BuSnCl3 was added and mixt. was refluxed for another 4 h; ppt. was filtered off in vac., washed with ethanol, stirred with water for 1 h and recrystd. from CH2Cl2; elem. anal.;93.3%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

aluminum isopropoxide
555-31-7

aluminum isopropoxide

[(C4H9)Sn(Al(OCH(CH3)2)4)2Cl]
845510-80-7

[(C4H9)Sn(Al(OCH(CH3)2)4)2Cl]

Conditions
ConditionsYield
With potassium In benzene byproducts: KCl; K and Al(OCH(CH3)2)3 (2 equiv.) were reacted in isopropyl/benzene; obtained soln. was added to soln. of Sn compd. in benzene; mixt. was refluxedfor 5 h; filtered; volatiles removed (vac.); distd. at 132°C/0.15 mm; elem. anal.;93%
1,1'-bis(imidazolyl)methane
84661-56-3

1,1'-bis(imidazolyl)methane

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

(bis(1-imidazolyl)methane)((n-Bu)SnCl3)

(bis(1-imidazolyl)methane)((n-Bu)SnCl3)

Conditions
ConditionsYield
In diethyl ether; ethanol soln. of Sn compd. and ligand in Et2O/EtOH (1/1) was stirred at room temp. for 48 h under N2; filtered; dried (vac.); washed (Et2O); recrystd. (EtOH); elem. anal.;93%
N-phthaloylglycine
4702-13-0

N-phthaloylglycine

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

sodium methylate
124-41-4

sodium methylate

C4H9Sn(COC6H4CONCH(H)COO)3

C4H9Sn(COC6H4CONCH(H)COO)3

Conditions
ConditionsYield
In methanol byproducts: NaCl; mixing organic compounds, refluxing for about 2 h, addn. of tin compound, refluxing for 6 h; filtn., evapn. of filtrate under reduced pressure, recrystn. (chloroform-hexane), elem. anal.;92%
1,5-diphenylpentane-1,3,5-trione
1467-40-9

1,5-diphenylpentane-1,3,5-trione

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

Sn(C4H9)(C6H5C(O)CHC(O)CHC(O)C6H5)Cl(C5H5N)
103238-33-1

Sn(C4H9)(C6H5C(O)CHC(O)CHC(O)C6H5)Cl(C5H5N)

Conditions
ConditionsYield
With pyridine; sodium In isopropyl alcohol; benzene byproducts: C5H5N*HCl; exclusion of moisture; addn. of Na to solvent mixt., set aside 6 h, refluxed for 1 h, addn. of ligand in benzene followed by addn. of Sn-compd.in benzene, ppt. of NaCl; ratio 1:1:3; filtered, evapd. (vac.), recrystd. (benzene); elem. anal.;92%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

disodium 1,2-ethanedithiolate
23851-06-1, 23851-16-3

disodium 1,2-ethanedithiolate

tetraethylammonium chloride
56-34-8

tetraethylammonium chloride

tetraethylammonium bis(ethane-1,2-dithiolato)-n-butylstannate
113161-03-8

tetraethylammonium bis(ethane-1,2-dithiolato)-n-butylstannate

Conditions
ConditionsYield
In acetone byproducts: NaCl; Et4NCl and BuSnCl3 stirred at room temp. for 0.5h under N2; dithiolate dropwise added; heated for 3h at 50 °C and stirred at room temp. overnight;; filtration; evapn.; crystn. from acetonitrile/ether at 7 °C; elem. anal.;;91%
ammonium O,O-(2,2-dimethyltrimethylene)dithiophosphate
74862-75-2

ammonium O,O-(2,2-dimethyltrimethylene)dithiophosphate

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

Sn(C4H9){S2P(OCH2C(CH3)2CH2O)}3

Sn(C4H9){S2P(OCH2C(CH3)2CH2O)}3

Conditions
ConditionsYield
In benzene byproducts: NH4Cl; a soln. of monoorganotin(IV) chloride is added to a suspn. of ammonium O,O-alkylenedithiophosphate in 1:3 molar ratio (room temp.); mixt. stirred (3-4 h); filtered; solvent removed (reduced pressure); elem. anal.;91%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

silver cyclohexanecarboxylate
13126-82-4

silver cyclohexanecarboxylate

bis(n-butyloxotin cyclohexanoato)-n-butyltin tricyclohexanoate dimer

bis(n-butyloxotin cyclohexanoato)-n-butyltin tricyclohexanoate dimer

Conditions
ConditionsYield
With H2O In tetrachloromethane byproducts: AgCl, HCl; addn. of Ag-compd to a stirred soln. of n-BuSnCl3 in CCl4, 2 h reflux, filtration of AgCl, evapn., standing of oil for 3 days in a stoppered flask at 25°C; washing of crystals with 100% ethanol; more crystals by recrystn. of oil in CHCl3/hexane, CH2Cl2/hexane and diethyl ether; hydrolysis of oil with 50% ethanol gives a white powder, filtration under suction, washing with 100% ethanol, drying; elem. anal.;91%
With H2O In chloroform byproducts: AgCl, HCl; addn. of Ag-compd to a soln. of n-BuSnCl3 in CHCl3, 2 h reflux, addn. of Na2SO4 as drying agent; filtration, evapn., dissoln. of oil in hexane, addn. of n-butylamine, 1week in the refrigerator, washing of crystals in cold hexane, drying;90%
3-thiapentan-1,5-dithiol
3570-55-6

3-thiapentan-1,5-dithiol

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

2-chloro-2-n-butyl-1,3,6-trithia-2-stannocane

2-chloro-2-n-butyl-1,3,6-trithia-2-stannocane

Conditions
ConditionsYield
In benzene equimolar amts., refluxing for 10 h; collection (filtration), recrystn. (CH2Cl2/hexane); elem. anal.;91%
Pyridine-2,6-dicarboxylic acid
499-83-2

Pyridine-2,6-dicarboxylic acid

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

[Sn(butyl)Cl(2,6-pyridinedicarboxylato)]
855483-11-3

[Sn(butyl)Cl(2,6-pyridinedicarboxylato)]

Conditions
ConditionsYield
With N(C2H5)3 In ethanol byproducts: N(C2H5)3HCl; (N2); using Schlenk techniques; addn. of NEt3 and SnBuCl3 in EtOH to soln. of 2,6-pyridinedicarboxylic acid in EtOH; stirring for 12 h; removal of solvent under reduced pressure, washing with hot water; recrystn. in mixt. of MeOH/H2O (14:1); elem. anal.;91%
o-hydroxyacetophenone-n-butylimine
54216-00-1

o-hydroxyacetophenone-n-butylimine

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

trans-(n-Bu)SnCl3(N-(n-butyl)-2-hydroxyacetophenylideneimine)2

trans-(n-Bu)SnCl3(N-(n-butyl)-2-hydroxyacetophenylideneimine)2

Conditions
ConditionsYield
In hexane absence of moisture, varying educt ratio; elem. anal.;91%
o-hydroxyacetophenone-n-propylimine
58308-13-7

o-hydroxyacetophenone-n-propylimine

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

trans-(n-Bu)SnCl3(N-(n-propyl)-2-hydroxyacetophenylideneimine)2

trans-(n-Bu)SnCl3(N-(n-propyl)-2-hydroxyacetophenylideneimine)2

Conditions
ConditionsYield
In hexane absence of moisture, varying educt ratio; pptn. or crystn.; elem. anal.;91%
sodium O,O'-di(4-chloro-3-methylphenyl)dithiophosphate
1481752-10-6

sodium O,O'-di(4-chloro-3-methylphenyl)dithiophosphate

Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

C36H42Cl4O4P2S4Sn

C36H42Cl4O4P2S4Sn

Conditions
ConditionsYield
In toluene at 20℃; for 24h; Inert atmosphere; Schlenk technique;91%
Trichlorbutylstannan
1118-46-3

Trichlorbutylstannan

diisobutylaluminium hydride
1191-15-7

diisobutylaluminium hydride

n-butyltin hydride
2406-65-7

n-butyltin hydride

Conditions
ConditionsYield
In dibutyl ether reaction at 0°C;;90%
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