Our service: 1.We have experience in exporting Pharmaceutical intermediates . 2.Professional packing with professional materials 3. We have products in stock, and we will deliver them soon when your PO arrived. Meanwhile we will give you the trackin
Cas:2627-69-2
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inquiryItems Specification Results Appearance White powder Conform Purity >98% Conf
Cas:2627-69-2
Min.Order:1 Gram
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Type:Manufacturers
inquiryDescription: Name:Acadesine CAS Number: 2627-69-2 Pu
Cas:2627-69-2
Min.Order:1 Kilogram
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inquiryWe can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need CMO
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inquiryBuilding Healthy Life Professional Factory We has a complete production and operating system, with an annual output capacity of 2000 tons. It can produce variety of content and proportion of extract according to the demand. Appearance:White fine
Cas:2627-69-2
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FOB Price: $25.0 / 37.7
Type:Manufacturers
inquiryHebei yanxi chemical co., LTD is a professional research, development and production Cyromazine、lead diacetate trihydrate /Lead acetate trihydrateC、 2-phenylacetamide 、 4-Aminophenyl-1-phenethylpiperidine 、Citric acid monohydrate 、 Citric acid/c
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:2627-69-2
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:2627-69-2
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:2627-69-2
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:2627-69-2
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:2627-69-2
Min.Order:1 Kilogram
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inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
Name:Acadesine Molecular Weight:258.23 EINECS:220-097-5 CAS No.:2627-69-2 Melting Point:214-215 °C … Appearance:white powder Storage:dry and cool place Package:1g/pack Application:Only for research applications, not for human consumption
Cas:2627-69-2
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryBeluga chemical professional supply Acadesine CAS 2627-69-2 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in China and exported to man
Cas:2627-69-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWe have overseas warehouses in California, Nuevo Laredo, Mexico, Vancouver, Canada, Amsterdam, The Netherlands and Melbourne, Australia. Overseas warehouses can provide some of the best selling products. We look forward to cooperating with strong loc
1.High Quality: Quality is life. Quality is the most important element for all goods. We have a lab doing research in Wuhan China and produce sarms in bulk quantity. We have 8 years experience making all kinds of sarms. And all our old customers
Cas:2627-69-2
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
AICAR CAS: 2627-69-2 Specification item specification result appearance white powder complies related substance (hplc) total impurity ≤0.
Service: 1. Any inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. OEM/ODM Available. 5. Reasonable & competitiv
Cas:2627-69-2
Min.Order:1 Gram
FOB Price: $55.0 / 60.0
Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryOur company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
Cas:2627-69-2
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Type:Lab/Research institutions
inquiryQ1: Are you a manufacturer?Answer: Yes, we are factory founded on 2002. Q2: How to contact with us?Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours. Q3:Which kind of payment terms do yo
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Type:Trading Company
inquiryCompany Profile SHENGZHIKAI TECHNOLOGY INDUSTRY CO., LTD is a high-tech enterprise dedicated to the fields of fine chemical products.The scope of products covers pharmaceutical intermediates, plant extracts, chemical reagent, animal p
Cas:2627-69-2
Min.Order:1 Kilogram
FOB Price: $58.0 / 69.0
Type:Trading Company
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:2627-69-2
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:2627-69-2
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiry5-amino-1-(5′-O-tert-butyldimethylsilyl-2′,3′-O-isopropylidene-β-D-ribofuranosyl)imidazole-4-carboxamide
AICA riboside
Conditions | Yield |
---|---|
With trifluoroacetic acid In acetonitrile at 0 - 20℃; for 17h; | 78% |
9-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1-(2-methoxy-ethoxymethyl)-1,9-dihydro-purin-6-one
AICA riboside
Conditions | Yield |
---|---|
With sodium hydroxide for 1h; Heating; | 73% |
Stage #1: 9-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1-(2-methoxy-ethoxymethyl)-1,9-dihydro-purin-6-one With sodium hydroxide; water for 1h; Heating / reflux; Stage #2: With hydrogenchloride In water at 20℃; | 70% |
5-amino-1-β-D-ribofuranosyl-1H-imidazole-4-carbonitrile
AICA riboside
Conditions | Yield |
---|---|
With sodium hydroxide at 100℃; for 2.5h; | 72% |
5-azido-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamide
AICA riboside
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In acetic acid under 760 Torr; for 1.5h; Ambient temperature; | 42% |
With hydrogen; palladium on activated charcoal In water; acetic acid at 23℃; under 760 Torr; for 1h; | 42% |
5-Amino-1-(β-D-ribofuranosyl)imidazole-4-carboxylic Acid Hydrazide
AICA riboside
Conditions | Yield |
---|---|
With ethanol; water; nickel |
5-nitro-1-β-D-ribofuranosyl-1H-imidazole-4-carboxylic acid amide
AICA riboside
Conditions | Yield |
---|---|
With water; platinum Hydrogenation; |
5-amino-1-(β-D-ribofuranosyl)imidazole-4-(N-benzyl)carboxamide
AICA riboside
Conditions | Yield |
---|---|
With ammonia; sodium amide |
Conditions | Yield |
---|---|
With ethyl acetate; platinum Hydrogenation.Behandeln mit -cyan-essigsaeure-amid und metanol. Natriummethylat; |
9-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1-methoxymethyl-1,9-dihydro-purin-6-one
AICA riboside
Conditions | Yield |
---|---|
With sodium hydroxide Heating; |
AICA riboside
Conditions | Yield |
---|---|
With sodium hydroxide Heating; |
AICA riboside
Conditions | Yield |
---|---|
With sodium hydroxide Heating; |
AICA riboside
Conditions | Yield |
---|---|
With sodium hydroxide Heating; |
1-(2,4-dinitrophenyl)inosine
AICA riboside
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dinitrophenyl)inosine With dmap In pyridine at 20℃; for 24h; Stage #2: With ethylenediamine In N,N-dimethyl-formamide at 50℃; for 8h; Stage #3: With trifluoroacetic acid In dichloromethane Further stages.; | |
Stage #1: 1-(2,4-dinitrophenyl)inosine With pyridine; dmap at 20℃; for 24h; Stage #2: With ethylenediamine In N,N-dimethyl-formamide at 50℃; for 8h; Further stages.; |
1-(2,4-dinitrophenyl)-2',3'-O-isopropylideneinosine
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 90 percent / aq. HCOOH / 4 h / 20 °C 2.1: MMTCl polystyrene resin; 4-(N,N-dimethylamino)pyridine / pyridine / 24 h / 20 °C 2.2: ethylenediamine / dimethylformamide / 8 h / 50 °C 2.3: TFA / CH2Cl2 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 99 percent / pyridine 2: 77 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 3: aq. NH3 / methanol / 20 °C 4: aq. NaOH / Heating View Scheme | |
Multi-step reaction with 4 steps 1: 99 percent / pyridine 2: 49 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 3: aq. NH3 / methanol / 20 °C 4: aq. NaOH / Heating View Scheme | |
Multi-step reaction with 4 steps 1: 99 percent / pyridine 2: 86 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 3: 91 percent / aq. NH3 / methanol / 1 h / 20 °C 4: 73 percent / aq. NaOH / 1 h / Heating View Scheme | |
Multi-step reaction with 4 steps 1: 99 percent / pyridine 2: 53 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 3: aq. NH3 / methanol / 20 °C 4: aq. NaOH / Heating View Scheme | |
Multi-step reaction with 4 steps 1: 99 percent / pyridine 2: 85 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 3: aq. NH3 / methanol / 20 °C 4: aq. NaOH / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 77 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 2: aq. NH3 / methanol / 20 °C 3: aq. NaOH / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 49 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 2: aq. NH3 / methanol / 20 °C 3: aq. NaOH / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 86 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 2: 91 percent / aq. NH3 / methanol / 1 h / 20 °C 3: 73 percent / aq. NaOH / 1 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 53 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 2: aq. NH3 / methanol / 20 °C 3: aq. NaOH / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 85 percent / i-Pr2NEt / CH2Cl2 / 1.08 h / 0 °C 2: aq. NH3 / methanol / 20 °C 3: aq. NaOH / Heating View Scheme |
2',3',5'-tri-O-acetyl-1-[(methoxy)methyl]inosine
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NH3 / methanol / 20 °C 2: aq. NaOH / Heating View Scheme |
2',3',5'-tri-O-acetyl-1-[(ethoxy)methyl]inosine
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NH3 / methanol / 20 °C 2: aq. NaOH / Heating View Scheme |
2',3',5'-tri-O-acetyl-1-[(2-methoxyethoxy)methyl]inosine
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / aq. NH3 / methanol / 1 h / 20 °C 2: 73 percent / aq. NaOH / 1 h / Heating View Scheme |
2',3',5'-tri-O-acetyl-1-[(benzyloxy)methyl]inosine
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NH3 / methanol / 20 °C 2: aq. NaOH / Heating View Scheme |
2',3',5'-tri-O-acetyl-1-[(2-trimethylsilylethoxy)methyl]inosine
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NH3 / methanol / 20 °C 2: aq. NaOH / Heating View Scheme |
5-azido-1-β-D-ribofuranosyl-1H-imidazole-4-carbonitrile
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / conc. aq. NH3, 30percent aq. H2O2 / 1.5 h / 1 °C 2: 42 percent / H2 / 10percent Pd/C / acetic acid; H2O / 1 h / 23 °C / 760 Torr View Scheme |
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) 1N aq. HCl, NaNO2, 2.) conc. aq. NH3 / 1.) 2 deg C, 200 min, 2.) 2 deg C, 40 min 2: 85 percent / conc. aq. NH3, 30percent aq. H2O2 / 1.5 h / 1 °C 3: 42 percent / H2 / 10percent Pd/C / acetic acid; H2O / 1 h / 23 °C / 760 Torr View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: trimethylsilyl trifluoromethanesulfonate / CH2Cl2 / 2.5 h 2: 2.) sodium methoxide / 1.) anisole, 90 deg C, 1.5 h, 2.) 140 deg C, 35 min 3: 55 percent / NaOMe / 2 h 4: 55 percent / sodium hypochlorite, 1.5 N NaOH / 2.5 h / 75 °C 5: 72 percent / 1.5 N NaOH / 2.5 h / 100 °C View Scheme | |
Multi-step reaction with 5 steps 1: trimethylsilyl trifluoromethanesulfonate / CH2Cl2 / 2.5 h / Ambient temperature 2: 63 percent / acetic acid / benzene / 10 h / Heating 3: 55 percent / NaOMe / 2 h 4: 55 percent / sodium hypochlorite, 1.5 N NaOH / 2.5 h / 75 °C 5: 72 percent / 1.5 N NaOH / 2.5 h / 100 °C View Scheme |
2,3,5-tri-O-benzoyl-β-D-ribofuranosyl bromide
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 44 percent / dioxane / 24 h / Ambient temperature 2: 2.) sodium methoxide / 1.) anisole, 90 deg C, 1.5 h, 2.) 140 deg C, 35 min 3: 55 percent / NaOMe / 2 h 4: 55 percent / sodium hypochlorite, 1.5 N NaOH / 2.5 h / 75 °C 5: 72 percent / 1.5 N NaOH / 2.5 h / 100 °C View Scheme |
N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)diaminomaleonoitrile
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 2.) sodium methoxide / 1.) anisole, 90 deg C, 1.5 h, 2.) 140 deg C, 35 min 2: 55 percent / NaOMe / 2 h 3: 55 percent / sodium hypochlorite, 1.5 N NaOH / 2.5 h / 75 °C 4: 72 percent / 1.5 N NaOH / 2.5 h / 100 °C View Scheme |
methyl 4-cyano-1-(β-D-ribofuranosyl)imidazole-5-carboximidate
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 55 percent / sodium hypochlorite, 1.5 N NaOH / 2.5 h / 75 °C 2: 72 percent / 1.5 N NaOH / 2.5 h / 100 °C View Scheme |
1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-dicyanoimidazole
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 55 percent / NaOMe / 2 h 2: 55 percent / sodium hypochlorite, 1.5 N NaOH / 2.5 h / 75 °C 3: 72 percent / 1.5 N NaOH / 2.5 h / 100 °C View Scheme |
N-formyl-N'-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)diaminomaleonitrile
AICA riboside
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 63 percent / acetic acid / benzene / 10 h / Heating 2: 55 percent / NaOMe / 2 h 3: 55 percent / sodium hypochlorite, 1.5 N NaOH / 2.5 h / 75 °C 4: 72 percent / 1.5 N NaOH / 2.5 h / 100 °C View Scheme |
AICA riboside
tert-butyldimethylsilyl chloride
5-amino-1-[2',3',5'-O-tris(tert-butyldimethylsilyl)-β-D-ribofuranosyl]imidazole-4-carboxamide
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 72h; Ambient temperature; | 98% |
With 1H-imidazole In N,N-dimethyl-formamide at 50℃; for 21h; | 96% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 48h; | 94% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 48h; | 66.6% |
AICA riboside
acetic anhydride
5-Amino-4-carbamoyl-1β-(2',3',5'-tri-O-acetyl-D-ribofuranosyl)imidazole
Conditions | Yield |
---|---|
With pyridine at 20℃; for 15h; | 95% |
In pyridine for 2h; Ambient temperature; | 94% |
In pyridine |
AICA riboside
ethyl methoxymethyleneoxyacetate
9-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-2-methoxymethoxymethyl-1,9-dihydro-purin-6-one
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 36h; Heating; | 93% |
methyl 9,10-dihydro-9,10-ethanoanthracene-11-carboxylate
AICA riboside
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 23h; Heating; | 91% |
AICA riboside
propionic acid anhydride
5-amino-1-(2,3,5-tri-O-propionyl-β-D-ribofuranosyl)-imidazole-4-carboxamide
Conditions | Yield |
---|---|
In pyridine for 16h; Ambient temperature; | 83% |
ethyl 2-hydroxyacetate
AICA riboside
9-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-2-hydroxymethyl-1,9-dihydro-purin-6-one
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 36h; Heating; | 81% |
AICA riboside
acetone
5-Amino-1-((3aR,4R,6R,6aR)-6-hydroxymethyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-1H-imidazole-4-carboxylic acid amide
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; orthoformic acid triethyl ester for 2h; Ambient temperature; | 78% |
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 36h; Heating; | 76% |
AICA riboside
methyl thioisocyanate
5-<1-(3-methylthioureido)>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 60℃; for 36h; | 75% |
In N,N-dimethyl-formamide at 80℃; for 12h; |
Conditions | Yield |
---|---|
With sodium hydroxide In methanol at 30 - 180℃; for 3h; Product distribution / selectivity; | 75% |
Conditions | Yield |
---|---|
With sodium hydroxide In methanol at 180℃; under 16501.3 Torr; for 3h; | 74% |
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 36h; Heating; | 72% |
AICA riboside
A
aminomalonic monoamide
B
2-amino-N-(β-D-ribofuranosyl)malondiamide
Conditions | Yield |
---|---|
With hydrogenchloride In water for 6h; Irradiation; | A 68% B n/a |
With hydrogenchloride In water for 6h; Ambient temperature; Yields of byproduct given; |
AICA riboside
1-benzyl-3-(ethoxycarbonyl)-carbodiimide
5-(3-benzyl-3'-(ethoxycarbonyl)-1-guanidino)-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide Ambient temperature; | 64% |
AICA riboside
1-(ethoxycarbonyl)-3-(4'-methoxybenzyl)carbodiimide
5-<3-(ethoxycarbonyl)-3'-(4'-methoxybenzyl)-1-guanidino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide Ambient temperature; | 64% |
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 36h; Heating; | 61% |
AICA riboside
5-azido-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamide
Conditions | Yield |
---|---|
Stage #1: AICA riboside With cis-nitrous acid Stage #2: With sodium azide | 60% |
Stage #1: AICA riboside With sodium nitrite In hydrogenchloride at -20℃; Stage #2: With sodium azide In hydrogenchloride at -20℃; for 2h; | 38% |
AICA riboside
isothiocyanatocyclohexane
5-<1-(3-cyclohexylthioureido)>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
Conditions | Yield |
---|---|
In pyridine Heating; | 58% |
AICA riboside
sodium 5-amino-1-(β-D-ribofuranosyl)imidazole-4-carboxylate
Conditions | Yield |
---|---|
With sodium hydroxide In water for 4h; Heating; | 55% |
AICA riboside
1-(benzyloxycarbonyl)-3-(4'-methoxybenzyl)carbodiimide
5-<3-(benzyloxycarbonyl)-3'-(4'-methoxybenzyl)-1-guanidino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide Ambient temperature; | 54% |
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane
AICA riboside
3',5'-O-tetraisopropyldisiloxanyl-5-amino-1-(β-D-2'-deoxyribofuranosyl) imidazole-4-carboxamide
Conditions | Yield |
---|---|
With pyridine In N,N-dimethyl-formamide for 4h; | 47% |
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 78℃; for 4h; Cyclization; | 43% |
AICA riboside
Benzyl isothiocyanate
A
5-<1-(3-benzylthioureido)>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
B
5-<1-<3-(benzylthiocarbamoyl)-3-benzylthioureido>>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
Conditions | Yield |
---|---|
In pyridine at 45 - 55℃; for 48h; | A 41% B 7% |
AICA riboside
2-Chloroethyl isothiocyanate
3-(β-D-ribofuranosyl)-6,7-dihydrothiazolo<3,2-a>purin-9-one
Conditions | Yield |
---|---|
In pyridine at 50℃; for 72h; | 22% |
Conditions | Yield |
---|---|
With enzyme-extracts from pigeon's liver; ATP | |
With brewer's yeast-autolysate; ATP |
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