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Cas:4756-13-2
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Type:Lab/Research institutions
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Min.Order:1 Metric Ton
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Type:Trading Company
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1,2,3-Propanetrithiol Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
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Conditions | Yield |
---|---|
at 60 - 70℃; for 0.5h; Reduction; oxidation; | A 5.4% B 98.6% |
at 100 - 120℃; for 5h; Reduction; oxidation; | A 92.5% B 95.6% |
1,2,3-propanetrithiol
Conditions | Yield |
---|---|
With sodium hydroxide; hydrazine hydrate at 80 - 90℃; for 1h; | 59% |
polymer, product of thiylation with 0.19 g/mol of sulfur, where content of sulfur moieties 6.0 in repeating units; monomer(s): 1,2,3-trichloropropane, charged content 0.06 g/mol
1,2,3-propanetrithiol
Conditions | Yield |
---|---|
With potassium hydroxide; hydrazine hydrate at 80 - 85℃; for 2h; | 30% |
1,2,3-propanetrithiol
Conditions | Yield |
---|---|
With potassium hydroxide; hydrazine hydrate at 80 - 85℃; | 26% |
Conditions | Yield |
---|---|
With ethanol; potassium hydrosulfide | |
With sodium hydrogensulfide; tetrabutyl-ammonium chloride at 90℃; for 4h; Temperature; Reagent/catalyst; | 137.2 g |
Conditions | Yield |
---|---|
With ammonium sulfide; ethanol at 60℃; | |
With sodium tetrasulfide; ethanol Behandeln des Reaktionsprodukts mit Natrium und fluessigem Ammoniak; | |
With sodium hydrogensulfide; ethanol at 60 - 90℃; |
1,2,3-tris-acetylsulfanyl-propane
1,2,3-propanetrithiol
Conditions | Yield |
---|---|
With sodium hydroxide | |
With sodium hydroxide In methanol |
1,2,3-propanetrithiol
Conditions | Yield |
---|---|
With hydrogen sulfide; ammonia In methanol at 90℃; for 16h; |
1,2,3-propanetrithiol
Conditions | Yield |
---|---|
With ethanol; potassium hydrosulfide |
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
at 70 - 80℃; |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; toluene 1.) -20 - -30 deg C, 1 h, 2.) -20 - -30 deg C to room temperature, 1 h, 3.) room temperature, 30 min; | 66% |
1,2,3-propanetrithiol
2,4-bis(mercaptomethyl)-1,3-dithiolane
Conditions | Yield |
---|---|
With sodium hydroxide; trifluoroborane diethyl ether In methanol; dichloromethane | 65% |
tris[triphenylphosphinegold(I)]oxonium tetrafluoroborate
1,2,3-propanetrithiol
(propane-1,2,3-trithiolato)tetrakis[(triphenylphosphine)gold(I)] tetrafluoroborate
Conditions | Yield |
---|---|
In dichloromethane byproducts: water; N2-atmosphere; stirring at room temp. for 1 h; layering with Et2O (pptn. and oil formation during 12 h), decantation; elem. anal.; | 65% |
1,2,3-propanetrithiol
dimethyl sulfate
A
1,2,3-tris-methylsulfanyl-propane
B
3-Methylsulfanyl-propane-1,2-dithiol
C
2-methylthio-1,3-propanedithiol
D
2,3-Bis-methylsulfanyl-propane-1-thiol
Conditions | Yield |
---|---|
With potassium carbonate In various solvent(s) for 2h; Yield given. Further byproducts given; | A n/a B 12% C 40% D n/a |
1,2,3-propanetrithiol
dimethyl sulfate
A
3-Methylsulfanyl-propane-1,2-dithiol
B
2-methylthio-1,3-propanedithiol
C
2,3-Bis-methylsulfanyl-propane-1-thiol
D
1,3-bismethylthio-2-propanethiol
Conditions | Yield |
---|---|
With potassium carbonate In various solvent(s) for 2h; Further byproducts given; | A 12% B 40% C n/a D n/a |
With potassium carbonate In various solvent(s) for 2h; Further byproducts given. Title compound not separated from byproducts; | A 12% B 40% C n/a D n/a |
With potassium carbonate In various solvent(s) for 2h; Yield given. Further byproducts given; | A 12% B 40% C n/a D n/a |
Conditions | Yield |
---|---|
With Na; EtOH; air In ethanol addn. of trithiol to soln. of Na in EtOH (under N2), addn. of Et3NCH2PhBr and MnCl2, stirring and controlled exposing to air (dissoln., then pptn.); N2-atmosphere; collection (filtration), washing (EtOH), drying (vac.), dissoln. in MeCN, filtration, Et2O addn., crystn. (-20°C, overnight), collection (filtration), washing (Et2O), drying (vac.); elem. anal.; | 35% |
Conditions | Yield |
---|---|
Stage #1: 9-fluorenone; 1,2,3-propanetrithiol With iodine In chloroform at 20℃; for 18h; Stage #2: 2-chloropropionyl chloride In toluene at 20 - 50℃; for 30.5h; Inert atmosphere; Stage #3: With sodium hydrogencarbonate In water for 0.5h; | 34% |
Conditions | Yield |
---|---|
at 140℃; |
Conditions | Yield |
---|---|
With ethanol; sodium ethanolate anschliessendes Behandeln mit Acetanhydrid in Pyridin; |
1,2,3-propanetrithiol
orthoformic acid triethyl ester
2,6,7-trithia-norbornane
Conditions | Yield |
---|---|
Erhitzen des Reaktionsgemisches unter vermindertem Druck; |
Conditions | Yield |
---|---|
With potassium hydroxide |
1,2,3-propanetrithiol
dimethyl sulfate
1,2,3-tris-methylsulfanyl-propane
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With methanol; sodium methylate Erwaermen des Reaktionsprodukts mit Acetanhydrid und Natriumacetat; |
Conditions | Yield |
---|---|
With sodium hydroxide |
1,2,3-propanetrithiol
n-hexadecanoyl chloride
1,2,3-tris-palmitoylmercapto-propane
Conditions | Yield |
---|---|
With pyridine; chloroform |
1,2,3-propanetrithiol
propylene sulphide
3-[(2-sulfanylpropyl)sulfanyl]propane-1,2-dithiol
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol |
1,2,3-propanetrithiol
propylene sulphide
1,3-bis-(2-mercapto-propylsulfanyl)-propane-2-thiol
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol |
1,2,3-propanetrithiol
acetic anhydride
methyloxirane
2-Acetoxypropyl-2,3-diacetylthiopropyl-sulfid
Conditions | Yield |
---|---|
(i) Na, EtOH, (ii) /BRN= 385737/, NaOAc; Multistep reaction; |
1,2,3-propanetrithiol
methyl iodide
A
1,2,3-tris-methylsulfanyl-propane
B
3-Methylsulfanyl-propane-1,2-dithiol
C
2,3-Bis-methylsulfanyl-propane-1-thiol
D
1,3-bismethylthio-2-propanethiol
Conditions | Yield |
---|---|
With n-butyllithium 1.) hexane/tetrahydrofuran, -78 deg C, 2.) THF, 0 deg C, then room temperature, 30 min; Yield given. Multistep reaction. Yields of byproduct given; |
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