Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Simagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:1008-89-5
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryXi'an Xszo Chem Co., Ltd.
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:1008-89-5
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryChemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:1008-89-5
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryHenan Tianfu Chemical Co., Ltd.
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:1008-89-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHebei Nengqian Chemical Import and Export Co., LTD
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:1008-89-5
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryZhuozhou Wenxi import and Export Co., Ltd
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1008-89-5
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryHenan Sinotech Import&Export Corporation
Product name: 2-Phenylpyridine CAS NO.: 1008-89-5 Appearance: Colorless liquid Content: 99% Molecular formula: C11H9N Molecular weight: 155.20 Appearance:Colorless liquid Storage: Preserve in well-closed, light-resistant and airtight containers.
Cas:1008-89-5
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiryHangzhou Sartort Biopharma Co., Ltd
Appearance:Clear colorless to yellow liquid Storage:Store below +30°C. Package:200kg/Drum Application:2-Phenylpyridine has been studied as a dopamine d3 receptor selective ligand with potential application for treatment of drug addictions, schizop
Cas:1008-89-5
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryHubei Langyou International Trading Co., Ltd
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:liquid Storage:Store in sealed containers at cool & dry pla
Cas:1008-89-5
Min.Order:100 Gram
Negotiable
Type:Other
inquiryShanghai Upbio Tech Co.,Ltd
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:1008-89-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryShanghai Minstar Chemical Co., Ltd
Product Name: 2-Phenylpyridine Synonyms: 2-Azabiphenyl;2-PHENYLPYRIDINE;2-phenyl-pyridin;o-Phenylpyridine;Phenylpyridine,95%;Pyridine, 2-phenyl-;2-PHENYLPYRIDINE 98+%;a-Phenylpyridine CAS: 1008-89-5 MF: C11H9N MW: 155.2 EINECS: 213-
Baoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:1008-89-5
Min.Order:1 Kilogram
FOB Price: $68.0 / 75.0
Type:Trading Company
inquiryQingdao Beluga Import and Export Co., LTD
2-Phenylpyridine CAS: 1008-89-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
Cas:1008-89-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:1008-89-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Xiamen Hisunny Chemical Co.,Ltd
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hubei Jiutian Bio-medical Technology Co., Ltd
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:1008-89-5
Min.Order:0 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:1008-89-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Shaanxi Cuicheng Biomedical Technology Co., Ltd.
Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:1008-89-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHangzhou Lingrui Chemical Co.,Ltd.
2-PhenylpyridineAppearance:Brown liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF
Zibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Suzhou Sinosun Imp.&Exp. Corporation
We supply good quality 2-Phenylpyridine CAS# 1008-89-5 at competitive price. Our 2-Phenylpyridine CAS# 1008-89-5 has been exported to many countries and regions. If you are looking for 2-Phenylpyridine CAS# 1008-89-5 suppliers in China, Sinosun i
EAST CHEMSOURCES LIMITED
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:1008-89-5
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
KAISA GROUP INC
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Hangzhou Zhongqi chem Co.,Ltd.
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Synthetic route
| Conditions | Yield |
|---|---|
| With [Pd(N-(naphthyl)-salicylaldimine(-2H))(triphenylphosphine)]; sodium hydroxide at 120℃; for 24h; Reagent/catalyst; Suzuki Coupling; | 100% |
| With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene for 18h; Inert atmosphere; Reflux; | 100% |
| With potassium phosphate; (PdCl2)(2-pyridyl)-6-isopropyl cis piperidine complex In water; N,N-dimethyl-formamide at 110℃; for 2h; | 99% |
-
-
386253-27-6
N-(phenyl(2-phenylpyridin-1(2H)-yl)methylene)methanamine
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With 2,3-dicyano-5,6-dichloro-p-benzoquinone In tetrahydrofuran at 25℃; | 100% |
| Conditions | Yield |
|---|---|
| With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: phenylmagnesium bromide With indium(III) chloride In tetrahydrofuran at 25℃; Stage #2: 2-iodopyridine; tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane In tetrahydrofuran; water for 5h; Heating; Further stages.; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: 2-fluoropyridine; phenylmagnesium bromide; bis(acetylacetonate)nickel(II); ((2-hydroxymethyl)phenyl)diphenylphosphine In diethyl ether for 0.5h; Stage #2: With methanol In diethyl ether Product distribution / selectivity; | 100% |
| Stage #1: 2-fluoropyridine; phenylmagnesium bromide; 1-[2-(diphenylphosphino)phenyl]ethanol; bis(acetylacetonate)nickel(II) In diethyl ether for 2h; Stage #2: With methanol In diethyl ether Product distribution / selectivity; | 96% |
| Conditions | Yield |
|---|---|
| With 4-di-tert-butylphosphanyl-1,5-diphenyl-1H-[1,2,3]triazole; potassium phosphate; bis(dibenzylideneacetone)-palladium(0) In toluene at 100℃; for 12h; Suzuki-Miyaura coupling; | 99% |
| With 4-di-tert-butylphosphanyl-1,5-diphenyl-1H-[1,2,3]triazole; potassium phosphate; bis(dibenzylideneacetone)-palladium(0) In toluene at 100℃; for 12h; Suzuki-Miyaura coupling; | 99% |
| With potassium phosphate; palladium diacetate In tetrahydrofuran at 100℃; for 24h; Suzuki-Miyaura coupling; | 99% |
| Conditions | Yield |
|---|---|
| With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride | 99% |
| Conditions | Yield |
|---|---|
| With chromium dichloride; cesium fluoride; 4,4'-di-tert-butyl-2,2'-bipyridine In tetrahydrofuran at 40℃; for 12h; Mechanism; Catalytic behavior; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 99% |
| With bis(1,5-cyclooctadiene)nickel(0); (dimethoxy)methylsilane; tricyclohexylphosphine In toluene at 80℃; for 12h; Inert atmosphere; | 96% |
| With bis(1,5-cyclooctadiene)nickel(0); 1,1,3,3-Tetramethyldisiloxane; tricyclohexylphosphine In toluene at 110℃; for 10h; Inert atmosphere; | 86% |
| Conditions | Yield |
|---|---|
| With (2-hydroxyethyl)(methyl)amine; copper(l) iodide; dichloro(1,3-bis(dicyclohexylphosphino)propane)palladium In N,N-dimethyl-formamide at 100℃; for 16h; Reagent/catalyst; Suzuki-Miyaura Coupling; Inert atmosphere; | 99% |
-
-
98061-25-7
1,3-dimethoxy-2-(2-pyridyl)benzene
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With chromium dichloride; cesium fluoride; 4,4'-di-tert-butyl-2,2'-bipyridine In tetrahydrofuran at 40℃; for 12h; Schlenk technique; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 25℃; for 5h; | 98% |
| Pd(dppf)Cl2 In tetrahydrofuran; tert-butyl methyl ether; water | 98.1% |
| With isoquinoline; ferric(III) bromide In tetrahydrofuran; tert-butyl methyl ether at 25℃; for 0.25h; Reagent/catalyst; Inert atmosphere; | 89% |
| Conditions | Yield |
|---|---|
| With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride | 98% |
| With (dcpp)Ni(η2–toluene) In tetrahydrofuran at 60℃; for 2h; Negishi Coupling; Glovebox; Schlenk technique; Inert atmosphere; | 96% |
| Conditions | Yield |
|---|---|
| With [1,3-bis(2,6-diisopropylphenyl)-imidazolium][Ni(PPh3)Cl3] In tetrahydrofuran at 30℃; for 5h; Kumada Cross-Coupling; Schlenk technique; Inert atmosphere; | 98% |
| With CpPd(SIMes)Cl; lithium chloride In tetrahydrofuran; 1,2-dimethoxyethane at 20℃; for 36h; Kumada-Tamao-Corriu cross-coupling reaction; Inert atmosphere; | 87% |
| With (IPr)Ni(π-allyl)Cl In tetrahydrofuran at 20℃; for 1h; Kumada Cross-Coupling; Inert atmosphere; | 86% |
-
-
109-04-6
2-bromo-pyridine
-
-
1352708-09-8
trimethyl((5-methyl-2-phenyl-1,3,2-dioxaborinan-5-yl)methoxy)silane
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol at 100℃; for 18h; Reagent/catalyst; Solvent; Suzuki Coupling; Inert atmosphere; | 98% |
| Conditions | Yield |
|---|---|
| With hydrogenchloride; iodine; oxygen In dimethyl sulfoxide at 80℃; for 4h; Catalytic behavior; Reagent/catalyst; Time; Temperature; | 98% |
| With oxygen; palladium diacetate; toluene-4-sulfonic acid In tetrahydrofuran for 10h; Catalytic behavior; Reagent/catalyst; Reflux; | 89% |
| With oxygen In ethanol at 100℃; under 760.051 Torr; for 24h; Solvent; | 75% |
| Conditions | Yield |
|---|---|
| With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; hydrazine hydrate In dimethyl sulfoxide at 20℃; for 11h; Reagent/catalyst; Inert atmosphere; Irradiation; chemoselective reaction; | 97% |
| With palladium on activated charcoal; tetrabutylammomium bromide; water; sodium hydroxide; silicon at 100℃; for 6h; | 95% |
| With titanium In tetrahydrofuran for 0.25h; Ambient temperature; | 89% |
| Conditions | Yield |
|---|---|
| 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 25℃; for 5h; | 97% |
| With reduced graphene oxide supported Ni nanoparticles (~40 wtpercent) In tetrahydrofuran at 25℃; for 10h; Kumada Cross-Coupling; Inert atmosphere; | 91% |
| With ferric(III) bromide In tetrahydrofuran; tert-butyl methyl ether at 20℃; for 1.16667h; Inert atmosphere; Schlenk technique; | 83% |
| With C25H16CuN4O6 In diethyl ether; N,N-dimethyl-formamide at 20℃; for 0.5h; Catalytic behavior; Kumada Cross-Coupling; | 78% |
| With [Ni(9,10-phenanthrenequinone-N''-methylthiosemicarbazone)2] In diethyl ether at 20℃; for 4h; Reagent/catalyst; Kumada Cross-Coupling; | 70% |
| Conditions | Yield |
|---|---|
| With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium carbonate In ethanol; water at 35℃; for 3h; Suzuki Coupling; chemoselective reaction; | 97% |
| Conditions | Yield |
|---|---|
| bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran; 1,2-dimethoxyethane at 0 - 20℃; for 0.5h; | 96% |
| Conditions | Yield |
|---|---|
| With [Pd(N-(3-chloro-2-quinoxalinyl)-N'-(2,6-diisopropylphenyl)imidazolium)(PPh3)Cl2]; potassium carbonate In water at 70℃; for 3h; Catalytic behavior; Suzuki-Miyaura Coupling; | 96% |
| With palladium diacetate; potassium carbonate In ethanol; water at 80℃; for 2h; Suzuki-Miyaura Coupling; | 91% |
| With palladium diacetate; sodium carbonate In ethanol; water at 80℃; for 4h; Suzuki-Miyaura Coupling; | 89% |
-
-
853955-69-8
[2-(hydroxymethyl)phenyl](dimethyl)phenylsilane
-
-
5029-67-4
2-iodopyridine
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With N-cyclohexyl-1-[2-(diphenylphosphanyl)phenyl]methanimine; potassium carbonate; palladium dichloride In water; dimethyl sulfoxide at 50℃; for 13h; | 96% |
| With potassium carbonate; N-cyclohexyl-1-[2-(diphenylphosphanyl)phenyl]methanimine; palladium dichloride In water; dimethyl sulfoxide at 50℃; for 13h; | 92% |
| Conditions | Yield |
|---|---|
| With 1-[2-(diphenylphosphino)phenyl]ethanol; bis(acetylacetonate)nickel(II) In diethyl ether at 20℃; for 2h; | 96% |
| Conditions | Yield |
|---|---|
| With potassium acetate In ethanol; dimethyl sulfoxide at 100℃; for 10h; Suzuki-Miyaura Coupling; Schlenk technique; Inert atmosphere; | 96% |
| With potassium carbonate In water at 90℃; for 0.333333h; Suzuki Coupling; | 96% |
| With potassium phosphate In 1,4-dioxane at 80℃; for 1.5h; Suzuki-Miyaura Coupling; | 95% |
| Conditions | Yield |
|---|---|
| With potassium phosphate; tetrabutylammomium bromide In water at 90℃; for 6h; Suzuki-Miyaura Coupling; Green chemistry; | 96% |
| Stage #1: 3-Chloropyridine; phenylboronic acid With palladium diacetate; (R)-6-dicyclohexylphoshino-6'-diphenylphosphino-3,3'-dimethoxy-2,2',4,4'-tetramethyl-1,1'-biphenyl In dodecane; butan-1-ol at 25℃; for 0.166667h; Suzuki-Miyaura Coupling; Inert atmosphere; Glovebox; Stage #2: With cesiumhydroxide monohydrate In dodecane; water; butan-1-ol at 25℃; Suzuki-Miyaura Coupling; Inert atmosphere; Glovebox; | 96% |
| Conditions | Yield |
|---|---|
| Stage #1: iodobenzene With TurboGrignard In tetrahydrofuran at -40℃; for 1h; Inert atmosphere; Stage #2: With tbepc In tetrahydrofuran at -40 - 0℃; for 2h; Inert atmosphere; Stage #3: pyridine-2-yl magnesium chloride Further stages; | 96% |
| Conditions | Yield |
|---|---|
| With potassium tert-butylate; vasicine at 20 - 110℃; for 72h; Schlenk technique; Inert atmosphere; | 95% |
| With bathophenanthroline; potassium tert-butylate; iron(II) acetate at 20 - 80℃; Inert atmosphere; | 85% |
| With potassium tert-butylate at 110℃; for 3h; | 85% |
-
-
27012-25-5
5-bromo-2-phenylpyridine
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With hydrogen; triethylamine; palladium on activated charcoal In ethanol | 95% |
| Conditions | Yield |
|---|---|
| With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride | 95% |
-
-
109-04-6
2-bromo-pyridine
-
-
913621-71-3
[2-(hydroxymethyl)phenyl](diisopropyl)phenylsilane
-
A
-
1008-89-5
2-phenylpyridine
-
B
-
913621-73-5
1,1-diisopropyl-1,3-dihydrobenzo[c][1,2]oxasilole
| Conditions | Yield |
|---|---|
| With potassium carbonate; copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); ruphos In tetrahydrofuran; N,N-dimethyl-formamide at 75℃; for 23h; Product distribution / selectivity; | A 95% B 95% |
| Conditions | Yield |
|---|---|
| With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; cesium fluoride; 3-tert-butyl-5-methyl-1-(2-(diphenylphosphino)phenyl)-1H-pyrazole In toluene at 60℃; for 10h; Stille coupling; Inert atmosphere; | 95% |
| With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 6h; Catalytic behavior; Stille Cross Coupling; | 86% |
| With 2C13H19N2(1+)*Cl6Pd2(2+); cesium fluoride In N,N-dimethyl-formamide at 120℃; for 0.166667h; Stille Cross Coupling; Microwave irradiation; | 82% |
| With cesium fluoride In water; N,N-dimethyl-formamide at 40℃; for 8h; Stille coupling; | 78% |
| Conditions | Yield |
|---|---|
| With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; Inert atmosphere; | 100% |
| With 3,3-dimethyldioxirane In acetone at 23℃; Kinetics; | 98% |
| With phosphomolybdic acid; dihydrogen peroxide In water; acetonitrile at 50℃; for 12h; Mechanism; | 78% |
| Conditions | Yield |
|---|---|
| In hexane at -78℃; | 100% |
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With potassium tert-butylate; deuterium In tetrahydrofuran at 55℃; under 1500.15 Torr; for 24h; Reagent/catalyst; regioselective reaction; | 100% |
| With copper(l) iodide; tris(triphenylphosphine)ruthenium(II) chloride; potassium deuterohydroxide; water-d2; zinc In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 99% |
| With deuterium In tetrahydrofuran at 55℃; under 750.075 Torr; for 36h; Glovebox; Inert atmosphere; regioselective reaction; | 84% |
| With Crabtree's catalyst; water-d2; deuterium In dichloromethane at 20℃; | |
| With [(2)H6]acetone; C54H50NOP2Rh(1+)*F6P(1-) at 100℃; for 8h; regioselective reaction; |
-
-
1008-89-5
2-phenylpyridine
-
-
13382-54-2
2-chloro-6-phenyl-pyridine
| Conditions | Yield |
|---|---|
| Stage #1: 2-phenylpyridine With n-butyllithium; 2-(N,N-dimethylamino)ethanol In hexane at 0℃; for 1h; Stage #2: With hexachloroethane In hexane at -78 - 20℃; | 100% |
| Stage #1: 2-phenylpyridine With n-butyllithium; 2-(N,N-dimethylamino)ethanol In hexane at 0℃; for 1h; Stage #2: With hexachloroethane In hexane at -78 - 20℃; Further stages.; | 81% |
| Stage #1: 2-phenylpyridine With n-butyllithium; 2-(N,N-dimethylamino)ethanol In tetrahydrofuran at -78℃; Stage #2: With hexachloroethane In tetrahydrofuran at -78 - 20℃; | 72% |
-
-
1008-89-5
2-phenylpyridine
-
-
39774-26-0
2-bromo-6-phenylpyridine
| Conditions | Yield |
|---|---|
| Stage #1: 2-phenylpyridine With n-butyllithium; 2-(N,N-dimethylamino)ethanol In hexane at 0℃; for 1h; Stage #2: With carbon tetrabromide In hexane at -78 - 20℃; | 100% |
| Stage #1: 2-phenylpyridine With n-butyllithium; 2-(N,N-dimethylamino)ethanol In hexane at 0℃; for 1h; Stage #2: With carbon tetrabromide In hexane at -78 - 20℃; Further stages.; | 89% |
| Stage #1: 2-phenylpyridine With n-butyllithium; 2-(N,N-dimethylamino)ethanol In hexane at -10℃; for 1h; Stage #2: With ethylene dibromide In tetrahydrofuran; hexane at -40 - 20℃; | 69% |
-
-
1008-89-5
2-phenylpyridine
-
-
10025-99-7
potassium tetrachloroplatinate(II)
-
-
155475-93-7
phenylpyridinebridgedichloro platinum
| Conditions | Yield |
|---|---|
| In 2-ethoxy-ethanol; water at 80℃; for 23h; Inert atmosphere; | 100% |
| In 2-ethoxy-ethanol; water aq. degassed soln. of K2PtCl4 (1.2 mmol) added under N2 to soln. of 2-phenylpyridine (1.2 mmol) in 2-ethoxyethanol (stirring); heated (80°C, 48 h); cooled in ice bath; H2O added; ppt. filtered; washed with EtOH; dried (vac.); | 95% |
| In 2-ethoxy-ethanol; water at 70℃; for 2h; | 77.2% |
| Conditions | Yield |
|---|---|
| With dichloro[1-(3-methylbenzyl)-3-(n-butyl)benzimidazol-2-ylidene]ruthenium(II); potassium acetate In water at 100℃; for 1h; Reagent/catalyst; | 100% |
| With rhodium(III) chloride hydrate; sodium carbonate; triphenylphosphine In 1-methyl-pyrrolidin-2-one at 140℃; for 22h; Inert atmosphere; | 99% |
| With C36H35Cl2PRu; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 24h; regioselective reaction; | 87% |
| Conditions | Yield |
|---|---|
| With dichloro[1-(3-methylbenzyl)-3-(n-butyl)benzimidazol-2-ylidene]ruthenium(II); potassium acetate In water at 100℃; for 5h; Reagent/catalyst; | 100% |
| With C36H35Cl2PRu; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 24h; regioselective reaction; | 86% |
-
-
1008-89-5
2-phenylpyridine
-
-
708268-52-4
((2,6-iPr2C6H3)NCH2CH2N(2,6-iPr2C6H3))Y(CH2SiMe3)(THF)2
| Conditions | Yield |
|---|---|
| In benzene at 20℃; | 100% |
| Conditions | Yield |
|---|---|
| In neat (no solvent) at 25℃; for 0.05h; Sonication; | 100% |
| Conditions | Yield |
|---|---|
| In neat (no solvent) at 25℃; for 0.05h; Sonication; | 100% |
| Conditions | Yield |
|---|---|
| With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium acetate at 60℃; for 17h; Catalytic behavior; Concentration; Schlenk technique; Sealed tube; | 100% |
-
-
96-43-5
2-thienyl chloride
-
-
1008-89-5
2-phenylpyridine
-
-
1041085-74-8
2-(2-(thiophene-2-yl)phenyl)pyridine
| Conditions | Yield |
|---|---|
| With dichloro[1-(3-methylbenzyl)-3-(n-butyl)benzimidazol-2-ylidene]ruthenium(II); potassium acetate In water at 100℃; for 20h; Reagent/catalyst; | 100% |
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With potassium carbonate for 0.1h; Time; Inert atmosphere; Microwave irradiation; Reflux; | 99.1% |
-
-
1008-89-5
2-phenylpyridine
-
-
344426-19-3, 693794-98-8, 911406-78-5, 94928-86-6, 955950-26-2
fac-tris[2-phenylpyridinato-C2,N]iridium(III)
| Conditions | Yield |
|---|---|
| In water at 205℃; for 48h; Temperature; Inert atmosphere; | 99.1% |
-
-
1008-89-5
2-phenylpyridine
-
-
142207-36-1
2-(2,6-dideuterophenyl)pyridine
| Conditions | Yield |
|---|---|
| With η4-cycloocta-1,5-diene(1,3-dimesitylimidazoline-2-ylidene)(triphenylphosphine)iridium(I) hexafluorophosphate; deuterium In dichloromethane at 20℃; for 72h; Sealed tube; | 99% |
| With copper(l) iodide; tris(triphenylphosphine)ruthenium(II) chloride; water-d2; zinc In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 99% |
| With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; tetradeuterioacetic acid at 60℃; for 24h; Inert atmosphere; Darkness; | 98% |
| Conditions | Yield |
|---|---|
| With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; 1,3-bis-(2,6-(i-Pr)2-C6H4)-[1,3,2]diazaphospholidine 2-oxide; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 8h; | 99% |
| With [RhCl2(p-cymene)]2; potassium pivalate; potassium carbonate In Diethyl carbonate at 120℃; for 2h; Inert atmosphere; | 96% |
| With potassium carbonate; bis(1-adamantyl)phosphine oxide; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In 1-methyl-pyrrolidin-2-one at 120℃; for 24h; | 95% |
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With oxygen; copper diacetate; lithium carbonate; benzoyl chloride In toluene at 145℃; for 60h; chemoselective reaction; | 99% |
| With N-chloro-succinimide; benzoic acid; copper(l) chloride at 100℃; for 24h; Inert atmosphere; Schlenk technique; | 96% |
| With hydrogenchloride; platinum; palladium dichloride In water; N,N-dimethyl-formamide at 90℃; Electrochemical reaction; regioselective reaction; | 94% |
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| With N-iodo-succinimide; toluene-4-sulfonic acid In 1,2-dichloro-ethane at 80℃; for 16h; Solvent; Reagent/catalyst; Sealed tube; | 99% |
| With N-iodo-succinimide; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; Trimethylacetic acid In 1,2-dichloro-ethane at 60℃; for 16h; Inert atmosphere; regioselective reaction; | 88% |
| With N-iodo-succinimide; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer for 3h; Time; Milling; | 84% |
| With N-iodo-succinimide; acetic acid; palladium diacetate at 100℃; for 12h; | 41% |
| With N-iodo-succinimide; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer In 1,2-dichloro-ethane at 85℃; for 0.5h; |
| Conditions | Yield |
|---|---|
| In 2-ethoxy-ethanol; water Reflux; Inert atmosphere; | 99% |
| In 2-ethoxy-ethanol for 24h; Reflux; | 90% |
| In 2-ethoxy-ethanol; water for 24h; Reflux; | 90% |
-
-
1008-89-5
2-phenylpyridine
-
-
10025-99-7
potassium tetrachloroplatinate(II)
| Conditions | Yield |
|---|---|
| In 2-ethoxy-ethanol; water other Radiation; 2-phenylpyridine (2.2 mmol) treated with K2PtCl4 (1 mmol) in degassed soln. (N2) of 2-ethoxyethanol/H2O (3:1, v/v); irradiated with microwave radiation (250 W, 1 min, max. temp. 110°C); cooled; filtered off; recrystd. from CH2Cl2/EtOH; elem. anal.; | 99% |
| In 2-ethoxy-ethanol; water aq. degassed soln. of K2PtCl4 (1.2 mmol) (3 ml) added to degassed soln. of 2-phenylpyridine (2.4 mmol) in 2-ethoxyethanol (9 ml) under N2 (stirring); heated (80°C) overnight; cooled in ice bath; distd. H2O added; ppt. filtered off; washed with cold EtOH; dried (vac.); crystd. from CH2Cl2/EtOH; | 95% |
| In acetic acid suspn. ligand and K2(PtCl4) in AcOH was heated at 75°C for 15 h; soln. was cooled to room temp., evapd., residue was dissolved in CH2Cl2,washed with 2.5 M HCl, water, dried over MgSO4, soln. was concd., Et2O was added, ppt. was collected by filtration; elem. anal.; | 82% |
-
-
1008-89-5
2-phenylpyridine
| Conditions | Yield |
|---|---|
| In dichloromethane under inert atm. or in vac.; stirred (23°C, 15 min, then 3.0 h, room temp.); pptd. by adding hexane; filtered, washed (hexane); dried in vacuo; recrystd. (CH2Cl2/hexane); | 99% |
| In dichloromethane byproducts: CH4; inert atmosphere; stirring (23°C, 2.5 h); pptn. with hexane, collection (filtration), washing (hexane), drying (vac.), recrystn. (CH2Cl2/hexane); elem. anal.; | 92% |
-
-
872-31-1
3-Bromothiophene
-
-
1008-89-5
2-phenylpyridine
-
-
1042718-94-4
2-di[2-(3-thiophenyl)]phenylpyridine
| Conditions | Yield |
|---|---|
| With potassium carbonate; triphenylphosphine; RuCl2(η6-C6H6) In 1-methyl-pyrrolidin-2-one at 120℃; for 20h; | 99% |
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