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inquiry4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methyl morpholinium chloride CAS 3945-69-5 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediate
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inquiryProduct Description Product Name 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methyl morpholinium chloride CAS No. 3945-69-5 Appea
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inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:DMTMM, a conjugatin
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inquiry4-methyl-morpholine
2-chloro-4,6-dimethoxy-1 ,3,5-triazine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.5h; Alkylation; | 100% |
In tetrahydrofuran at 20℃; for 0.5h; Substitution; | 100% |
In tetrahydrofuran at 0℃; for 0.5h; | 100% |
2-chloro-4,6-dimethoxy-1 ,3,5-triazine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
With 4-methyl-morpholine In tetrahydrofuran; methanol | 97.4% |
With 4-methyl-morpholine In tetrahydrofuran; methanol | 96.9% |
With 4-methyl-morpholine In ethyl acetate | 94.6% |
4-methyl-morpholine
2-chloro-4,6-dimethoxy-1 ,3,5-triazine
B
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 17h; Substitution; | A 95% B 2% |
In dichloromethane at 20℃; for 0.5h; Substitution; | A 21% B 78% |
4-methyl-morpholine
2-chloro-4,6-dimethoxy-1 ,3,5-triazine
butyric acid
A
C9H13N3O4
B
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In [D3]acetonitrile for 1h; |
4-methyl-morpholine
methanol
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
at 0 - 20℃; for 0.00416667h; |
2-Methylbutanoic acid
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
1-(tert-butoxycarbonyl)-L-proline
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
t-Boc-L-valine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
2-tert-butoxycarbonylamino-3-methyl-butyric acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
N-tert-butoxycarbonyl-L-leucine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
L-N-Boc-Ala
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
nonadecanoic acid
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
(E)-3-phenylacrylic acid
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
(E)-3-Phenyl-acrylic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
Monomethyl phthalate
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
N-tert-butyloxy-isoleucine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
2-tert-butoxycarbonylamino-3-methyl-pentanoic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
BOC-L-aspartic acid 4-benzyl ester
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
N-tert-butoxycarbonyl-L-phenylalanine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
benzoic acid
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
2-(benzyloxy)-4,6-dimethoxy-1,3,5-triazin
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
With 4-methyl-morpholine In water; acetone at 20℃; for 0.25h; | |
With 4-methyl-morpholine In 1,4-dioxane; water at 20℃; for 0.25h; |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
3-Phenylpropionic acid
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane at 0℃; for 3h; Condensation; | 100% |
With 4-methyl-morpholine In 1,4-dioxane; water at 20℃; for 0.25h; |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
C30H28N4O8
Conditions | Yield |
---|---|
In chloroform at 0 - 5℃; for 12h; | 100% |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3h; demethylation; | 96% |
In dichloromethane at 20℃; for 3h; Decomposition; | 96% |
In dichloromethane at 20℃; for 3h; | 96% |
In ethyl acetate at 23 - 29℃; for 0.5h; Conversion of starting material; |
2-(tert-butoxycarbonylamino)-3-phenylpropionic acid
methyl (2S)-2-amino-3-phenylpropanoate
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
(S)-methyl 2-((S)-2-(tert-butoxycarbonylamino)-3-phenylpropanamido)-3-phenylpropanoate
Conditions | Yield |
---|---|
In dichloromethane; water | 95% |
(2S)-2-[(2S)-2-[[(tert-butoxy)carbonyl](methyl)amino]propanamido]-2-cyclohexylacetic acid
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In ethyl acetate at -20 - 20℃; | A n/a B n/a C 95% |
N-tert-butoxycarbonyl-L-phenylalanine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
(S)-2-tert-butoxycarbonylamino-3-phenyl-propionic acid methyl ester
Conditions | Yield |
---|---|
With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide In methanol; diethyl ether; water | 93% |
With 4-methyl-morpholine; hydrogenchloride In methanol; dichloromethane; water |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 0 - 20℃; for 8h; Inert atmosphere; | 93% |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
4-nitro-benzoic acid
4-Nitro-benzoic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; | 92% |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
(RP)-5'-O-DMT-thymidine-3'-O-((4,6-dimethoxy-1,3,5-triazin-2-yl)methylphosphonothioate)
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | 90% |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
(SP)-5'-O-DMT-thymidine-3'-O-((4,6-dimethoxy-1,3,5-triazin-2-yl)methylphosphonothioate)
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 0.5h; | 88% |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
A
(5S)-5-aminocarbonyl-4,5-dihydro-1H-pyrrole-1-carboxylic acid 1-(1,1-dimethylethyl) ester
Conditions | Yield |
---|---|
With sodium hydroxide; sodium dihydrogenphosphate; ammonium chloride at 20℃; for 4h; pH=6.20; Conversion of starting material; | A 87% B 12% |
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | A 5% B 85% |
N-acetyl-D-glucosamine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
4,6-dimethoxy-1,3,5-triazin-2-yl α-N-acetylglucosaminide
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In water at 20℃; for 24h; regioselective reaction; | 84% |
(2S)-2-[(2S)-2-[[(tert-butoxy)carbonyl](methyl)amino]propanamido]-2-cyclohexylacetic acid
3-(4-fluoro-phenoxy)-5-(S)-pyrrolidin-2-yl-pyridine
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride
C
C32H43FN4O5
Conditions | Yield |
---|---|
In ethyl acetate at -20 - 20℃; | A n/a B n/a C 82% |
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