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inquiry3-(2-Chlorophenyl)-5-methylisoxazole-4-carbonyl chloride Basic information Product Name: 3-(2-Chlorophenyl)-5-methylisoxazole-4-carbonyl chloride Synonyms: 3-(2-chlorophenyl)-5-methyl-4-
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inquiryProduct Name: 3-(2-Chlorophenyl)-5-methylisoxazole-4-carbonyl chloride Synonyms: 3-(2-chlorophenyl)-5-methyl-4-isoxazolecarbonylchlorid;4-Isoxazolecarbonyl chloride, 3-(2-chlorophenyl)-5-methyl-;4-Isoxazole
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inquiry3-(2-chlorophenyl)-5-methyl-4-isoxazolecarboxylic acid
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride at 45℃; for 1h; | 93% |
With thionyl chloride | |
With thionyl chloride; sodium hydrogencarbonate In ice-water; dichloromethane; water |
2-chloro benzaldehyde oxime
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Cl2 2: (i) Na, MeOH, (ii) /BRN= 2502600/ 3: aq. KOH / ethanol 4: SOCl2 View Scheme | |
Multi-step reaction with 4 steps 1.1: chlorine / methanol / 0 - 5 °C 2.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10 2.2: 2 h / 0 - 20 °C / pH 9 3.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 4.1: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 4 steps 1: N-chloro-succinimide / N,N-dimethyl-formamide / 20 °C 2: triethylamine / dichloromethane / 20 °C 3: potassium hydroxide / water; ethanol / 20 °C 4: thionyl chloride / Reflux View Scheme |
methyl 3-(2'-chlorophenyl)-5-methylisoxazole-4-carboxylate
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. KOH / ethanol 2: SOCl2 View Scheme | |
Multi-step reaction with 2 steps 1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 2: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydroxide / water; methanol / 3 h 2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 40 °C View Scheme |
2-chloro-N-hydroxybenzimidoyl chloride
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) Na, MeOH, (ii) /BRN= 2502600/ 2: aq. KOH / ethanol 3: SOCl2 View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10 1.2: 2 h / 0 - 20 °C / pH 9 2.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 3.1: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane / 20 °C 2: potassium hydroxide / water; ethanol / 20 °C 3: thionyl chloride / Reflux View Scheme |
2-chloro-benzaldehyde
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: hydroxylamine sulfate / methanol / 0.5 h 1.2: 0.5 h / pH 8 - 9 / Reflux 2.1: chlorine / methanol / 0 - 5 °C 3.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10 3.2: 2 h / 0 - 20 °C / pH 9 4.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 5.1: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: hydroxylamine sulfate / methanol / 1 h / 20 - 40 °C 1.2: 24 h / 0 - 20 °C / pH ~ 9.5 / Inert atmosphere 1.3: pH ~ 7 - 7.5 2.1: phosphorus pentachloride / toluene View Scheme | |
Multi-step reaction with 5 steps 1: hydroxylamine hydrochloride; sodium carbonate / 20 °C 2: N-chloro-succinimide / N,N-dimethyl-formamide / 20 °C 3: triethylamine / dichloromethane / 20 °C 4: potassium hydroxide / water; ethanol / 20 °C 5: thionyl chloride / Reflux View Scheme |
ethyl 3-(2-chlorophenyl)-5-methylisoxazole-4-carboxylate
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium hydroxide / water; ethanol / 20 °C 2: thionyl chloride / Reflux View Scheme |
3-amino-naphthalene-1,8-dicarboxylic acid-anhydride
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
C23H13ClN2O5
Conditions | Yield |
---|---|
With pyridine In diethyl ether at 60 - 80℃; | 98% |
anthranilic acid
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 2h; | 94% |
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
3-(2-chlorophenyl)-5-methylisoxazole-4-carboxamide
Conditions | Yield |
---|---|
With ammonia at 100℃; for 1h; Sealed tube; | 93% |
With ammonium hydroxide In acetone |
para-fluorobenzylamine
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 93% |
2-octyn-1-ol
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With zinc In benzene for 0.133333h; Esterification; | 92% |
3-bromo-N-hydroxybenzimidamide
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; | 92% |
4-chloro-aniline
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
C17H12Cl2N2O2
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 92% |
p-toluidine
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 92% |
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
(Z)-N′-hydroxy-3-methoxybenzimidamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran for 20h; | 91% |
pentan-1-ol
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With zinc In benzene for 0.1h; Esterification; | 90% |
(+)-D-glucosamine hydrochloride
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at -5℃; for 4h; | 90% |
4-fluoroaniline
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 90% |
4-(trifluoromethoxy)aniline
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 90% |
1-amino-naphthalene
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 90% |
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
benzyl alcohol
Conditions | Yield |
---|---|
With zinc In benzene for 0.166667h; Esterification; | 89% |
isopropyl alcohol
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With zinc In benzene for 0.15h; Esterification; | 88% |
dimethylenecyclourethane
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In water; acetone at 20℃; | 87.3% |
thiosemicarbazide
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In acetone Cooling with ice; | 87% |
piperidine
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 87% |
trimethylsilylazide
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
at 20 - 100℃; Sealed tube; | 86% |
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With trimethylsilylazide at 100℃; Sealed tube; | 86% |
3-chloro-4-fluorophenylamine
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 86% |
3-methyl-2-buten-1-ol
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With zinc In benzene for 0.133333h; Esterification; | 85% |
morpholine
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 84% |
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 1.5h; | 83% |
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 20h; | 82% |
2-thiazolylamine
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 82% |
3-nitro-aniline
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; | 81% |
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 15h; | 80% |
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