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inquiryName:3-Chloro-4-fluoroaniline CAS:367-21-5 Grade:For chemical industry, scientific research and export Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security without vulnerab
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3-Chloro-4-fluoroaniline CAS 367-21-5 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to asse
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inquiry3-Chloro-4-fluoroaniline CAS 367-21-5 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality c
Cas:367-21-5
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inquiryConditions | Yield |
---|---|
With hydrogen In ethanol; water at 25℃; under 760.051 Torr; for 3h; Autoclave; | 99.9% |
With sodium tetrahydroborate; cyclohexanediamine-Pd-β-cyclodextrin In water at 20℃; for 3h; Sealed tube; | 96% |
With hydrazine hydrate In ethanol at 100℃; under 760.051 Torr; for 8h; Time; Sealed tube; chemoselective reaction; | 94.7% |
3-chloro-4-fluorophenylamine
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate at 20℃; for 0.25h; chemoselective reaction; | 86% |
(3-chloro-4-fluoro-phenyl)-carbamic acid tert-butyl ester
3-chloro-4-fluorophenylamine
Conditions | Yield |
---|---|
With methanol; oxalyl dichloride at 20℃; for 2h; | 80% |
Conditions | Yield |
---|---|
With Piperonyl butoxide; hydrogen fluoride Yields of byproduct given; | A 34% B n/a |
3-chloro-4-fluorophenylamine
Conditions | Yield |
---|---|
(i) PCl5, (ii) aq. HCl; Multistep reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: iron-powder / Einleiten von Chlor 2: titanium (III)-chloride; water View Scheme | |
Multi-step reaction with 2 steps 1: Cl2, FeCl3 2: Fe, aq. NH4Cl View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogenchloride; sodium nitrite / water / 0.5 h 2: trifluoromethan; fluorosulfonyl fluoride / 70 °C 3: hydrogenchloride / water / 2 h / 50 °C View Scheme |
3-chloro-4-fluorophenylamine
Conditions | Yield |
---|---|
With hydrogenchloride In water at 50℃; for 2h; |
3-chloro-4-fluorophenylamine
diethyl 2-ethoxymethylenemalonate
diethyl 2-[(3-chloro-4-fluorophenylamino)methylene]malonate
Conditions | Yield |
---|---|
at 120 - 130℃; for 2h; | 100% |
for 0.0333333h; Gould-Jacob reaction; Irradiation; | 99% |
at 110℃; for 1h; Microwave irradiation; | 99% |
3-chloro-4-fluorophenylamine
di-tert-butyl dicarbonate
(3-chloro-4-fluoro-phenyl)-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: 3-chloro-4-fluorophenylamine With triethylamine In tetrahydrofuran; water at 20℃; for 0.0833333h; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran; water at 0 - 20℃; for 6h; | 100% |
With 1-butyl-3-methylimidazolium trifluoromethanesulfonimide at 30 - 35℃; for 0.25h; neat (no solvent); chemoselective reaction; | 95% |
In water at 30 - 35℃; for 6h; | 92% |
3-chloro-4-fluorophenylamine
4-chloro-7-fluoro-6-nitroquinazoline
N-(3-chloro-4-fluorophenyl)-7-fluoro-6-nitroquinazolin-4-amine
Conditions | Yield |
---|---|
In isopropyl alcohol for 4h; Product distribution / selectivity; Reflux; | 100% |
With triethylamine In isopropyl alcohol for 1.5h; | 100% |
In isopropyl alcohol at 20℃; for 24h; Inert atmosphere; | 99% |
3-chloro-4-fluorophenylamine
4-chloro-6-nitro-7-trifluoromethoxyquinoline-3-carbonitrile
4-(3-chloro-4-fluorophenylamino)-6-nitro-7-trifluoromethoxyquinoline-3-carbonitrile
Conditions | Yield |
---|---|
In isopropyl alcohol for 3.5h; Heating; | 100% |
In ethanol for 12h; Heating; |
3-chloro-4-fluorophenylamine
6-bromo-4-chloro-3-quinolinecarbonitrile
6-bromo-N-(3-chloro-4-fluoro-phenyl)-quinoline-3-carbnitrile-4-amine
Conditions | Yield |
---|---|
In 1,4-dioxane at 90℃; for 2h; | 100% |
In 1,4-dioxane at 90℃; for 2h; | 100% |
In 2-ethoxy-ethanol at 135℃; for 2.5h; Heating / reflux; | 56% |
With aniline In isopropyl alcohol at 80℃; for 24h; | 38.8% |
In ethanol for 12h; Heating; |
3-chloro-4-fluorophenylamine
2-chloro-5-methoxyquinoline
Conditions | Yield |
---|---|
In neat (no solvent) at 160℃; | 100% |
1-methyl-piperazine
3-chloro-4-fluorophenylamine
bis(trichloromethyl) carbonate
Conditions | Yield |
---|---|
Stage #1: 3-chloro-4-fluorophenylamine; bis(trichloromethyl) carbonate With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; Stage #2: 1-methyl-piperazine In dichloromethane at 20℃; for 3h; | 100% |
3-chloro-4-fluorophenylamine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In iso-butanol Reflux; Inert atmosphere; | 100% |
3-chloro-4-fluorophenylamine
chloroacetyl chloride
N-(2-chloroacetyl)-3-chloro-4-fluoroaniline
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 25℃; | 99.3% |
With triethylamine In dichloromethane at 0 - 25℃; | 99.3% |
With pyridine In benzene for 1h; Ambient temperature; | 90% |
3-chloro-4-fluorophenylamine
6-acetoxy-4-chloro-7-methoxyquinazoline
4-((3-chloro-4-fluorophenyl)amino)-7-methoxyquinazolin-6-yl acetate
Conditions | Yield |
---|---|
In isopropyl alcohol for 2h; Inert atmosphere; Reflux; | 99% |
With gold(I) chloride In methanol at 65℃; Reagent/catalyst; Temperature; Concentration; | 93.4% |
In isopropyl alcohol for 2h; Reflux; | 92.5% |
3-chloro-4-fluorophenylamine
4-chloro-7-methoxy-6-(3-morpholinopropoxy)quinazoline
gefitinib
Conditions | Yield |
---|---|
With potassium hydroxide In isopropyl alcohol at 20℃; | 99% |
In isopropyl alcohol at 80℃; for 0.533333h; Microwave irradiation; | 92% |
With N,N,N,N,-tetramethylethylenediamine; nickel dichloride In tetrahydrofuran at 50℃; for 0.333333h; Concentration; Temperature; Reagent/catalyst; | 92.5% |
Conditions | Yield |
---|---|
In ethanol | 99% |
3-chloro-4-fluorophenylamine
4-chloro-7-methoxy-6-nitro-quinoline-3-carbonitrile
4-(3-Chloro-4-fluoro-phenylamino)-7-methoxy-6-nitro-quinoline-3-carbonitrile
Conditions | Yield |
---|---|
Stage #1: 3-chloro-4-fluorophenylamine; 4-chloro-7-methoxy-6-nitro-quinoline-3-carbonitrile In isopropyl alcohol at 20℃; for 22h; Heating / reflux; Stage #2: With sodium hydrogencarbonate In water; ethyl acetate | 99% |
In methanol; 2-methoxy-ethanol; ethyl acetate | |
In methanol; 2-methoxy-ethanol; ethyl acetate |
4-chloro-7-ethoxy-6-nitroquinazoline
3-chloro-4-fluorophenylamine
N-(3-chloro-4-fluorophenyl)-7-ethoxy-6-nitroquinazoline-4-amine
Conditions | Yield |
---|---|
With hydrogenchloride In water; isopropyl alcohol Reflux; | 99% |
In dichloromethane; isopropyl alcohol at 20℃; | 93% |
In dichloromethane; isopropyl alcohol at 20℃; | 93% |
In isopropyl alcohol for 1h; Reflux; | 89% |
With toluene-4-sulfonic acid In isopropyl alcohol at 75℃; for 5h; | 76% |
4-chloroquinazoline
3-chloro-4-fluorophenylamine
N-(3-chloro-4-fluorophenyl)quinazolin-4-amine
Conditions | Yield |
---|---|
In isopropyl alcohol for 2h; Reflux; | 99% |
In isopropyl alcohol for 6h; Reflux; | 91.6% |
Conditions | Yield |
---|---|
Stage #1: 3-chloro-4-fluorophenylamine; C15H13O4Pol With acetic acid In dichloromethane at 20℃; for 2h; not specified; Schlenk technique; Molecular sieve; Stage #2: With sodium tris(acetoxy)borohydride at 20℃; for 17h; not specified; Schlenk technique; | 99% |
3-chloro-4-fluorophenylamine
4-chloro-7-(3-chloropropoxy)-6-nitroquinoline-3-carbonitrile
4-(3-chloro-4-fluoro-phenylamino)-7-(3-chloro-propoxy)-6-nitro-quinoline-3-carbonitrile
Conditions | Yield |
---|---|
In isopropyl alcohol Heating; | 98% |
3-chloro-4-fluorophenylamine
4-chloro-1H-pyrrolo[2,3-d]pyrimidine
(3-chloro-4-fluoro-phenyl)-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)-amine
Conditions | Yield |
---|---|
With silver trifluoromethanesulfonate In N,N-dimethyl-formamide at 90℃; | 98% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 98% |
5-amino-4,6-dichloro-2-methylpyrimidine
3-chloro-4-fluorophenylamine
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water at 20℃; for 16h; Reflux; | 98% |
3-chloro-4-fluorophenylamine
7-chloro-6-nitro-4(3H)-quinazolinone
4-((3-chloro-4-fluorophenyl)amino)-6-nitro-7-chloroquinazoline
Conditions | Yield |
---|---|
Stage #1: 7-chloro-6-nitro-4(3H)-quinazolinone With thionyl chloride In N,N-dimethyl-formamide for 3h; Reflux; Stage #2: 3-chloro-4-fluorophenylamine In 1,4-dioxane; N,N-dimethyl-formamide at 90℃; for 1h; | 98% |
Stage #1: 7-chloro-6-nitro-4(3H)-quinazolinone With trichlorophosphate In acetonitrile at 80℃; for 5h; Stage #2: 3-chloro-4-fluorophenylamine In 1,4-dioxane; acetonitrile for 1h; | 70% |
3-chloro-4-fluorophenylamine
N,N-dimethyl-formamide
N-(3-chloro-4-fluoro-phenyl)-formamide
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 80℃; for 5.5h; Concentration; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 5℃; for 1h; | 98% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at -20 - 20℃; for 12h; |
formic acid
3-chloro-4-fluorophenylamine
N-(3-chloro-4-fluoro-phenyl)-formamide
Conditions | Yield |
---|---|
at 80℃; for 3.5h; | 97.7% |
for 16h; Reflux; | 93% |
With zinc(II) chloride at 70℃; for 1.33333h; neat (no solvent); | 92% |
Conditions | Yield |
---|---|
With acetic anhydride In toluene at 105 - 110℃; for 3h; Time; Reagent/catalyst; | 97.4% |
3-chloro-4-fluorophenylamine
isopropyl α-methyl α-diazoacetate
(R)-isopropyl 2-(3-chloro-4-fluorophenylamino)propionate
Conditions | Yield |
---|---|
With tetrakis(actonitrile)copper(I) hexafluorophosphate; C35H30N2O2; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In dichloromethane at 25℃; for 2h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 97% |
3-chloro-4-fluorophenylamine
N,N-dimethyl-formamide dimethyl acetal
4-(3-chloro-4-fluorophenylamino)-6-hydroxy-7-methoxyquinazoline
Conditions | Yield |
---|---|
With acetic acid In toluene at 65℃; for 7h; Solvent; Temperature; Concentration; Reagent/catalyst; Inert atmosphere; | 97% |
3-chloro-4-fluorophenylamine
benzyl alcohol
N-(3-chloro-4-fluorophenyl)-benzenemethanamine
Conditions | Yield |
---|---|
With palladium nanoparticles embedded in the solid matrix of tetrabutylammonium bromide synthetized in supercritical carbon dioxide at 140℃; Sealed tube; Inert atmosphere; Green chemistry; | 97% |
4-chloro-6-iodoquinazoline
3-chloro-4-fluorophenylamine
4-((3-chloro-4-fluorophenyl)amino)-6-iodoquinazoline
Conditions | Yield |
---|---|
In isopropyl alcohol at 80℃; for 2h; | 96% |
In isopropyl alcohol at 80℃; for 2h; | 96.3% |
With triethylamine In isopropyl alcohol at 20℃; for 9h; Reflux; | 95% |
In tetrahydrofuran for 1h; Reflux; | 60% |
In isopropyl alcohol |
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