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inquiryProduct Name: 3-Chloro-4-fluorobenzaldehyde CAS: 34328-61-5 MF: C7H4ClFO MW: 158.56 EINECS: 608-972-3 Mol File: 34328-61-5.mol 3-Chloro-4-fluorobenzaldehyde Structure 3-Chloro-4-fluorobenzaldehyde Chemical Properties Melting point
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inquiryProduct name: 3-Chloro-4-Fluorobenzaldehyde CAS No.:34328-61-5 Molecule Formula:C7H4ClFO Molecule Weight:158.56 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TE
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inquiryMelting point 28-30 ° C (lit.) Boiling point 66 ° C Density 1.3310 (estimate) Refractive index 1.544-1.546 Flash point > 230 ° f Storage condition: insert atmosphere, 2-8 ° C Liquid after melting Color clear light yellow App
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inquiry3-Chloro-4-fluorobenzaldehyde cas 34328-61-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquirypotassium (2-fluoro-5-formyl)phenyltrifluoroborate
3-Chloro-4-fluorobenzaldehyde
Conditions | Yield |
---|---|
With trichloroisocyanuric acid In water; ethyl acetate at 20℃; for 0.666667h; Open flask; | 80% |
3,4-dichlorobenzaldehyde
3-Chloro-4-fluorobenzaldehyde
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether; tetraphenylphosphonium bromide at 230℃; for 2h; | 66% |
With potassium fluoride | 66% |
With potassium fluoride In sulfolane at 220℃; for 12h; | 98 % Turnov. |
Conditions | Yield |
---|---|
(i) NaNO2, HCl, NaOAc, (ii) /BRN= 1697325/, CuSO4, Na2SO3, (iii) aq. HCl; Multistep reaction; |
3-Chloro-4-fluorobenzaldehyde
p-aminoethylbenzoate
4-[(3-chloro-4-fluoro-benzylidene)-amino]-benzoic acid ethyl ester
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 12h; Reflux; | 100% |
toluene-4-sulfonic acid In toluene for 12h; Reflux; | 100% |
Conditions | Yield |
---|---|
With C23H3BF16N2O In toluene at 25℃; for 3h; Green chemistry; | 100% |
3-Chloro-4-fluorobenzaldehyde
dimethyl amine
3-chloro-4-(dimethylamino)benzaldehyde
Conditions | Yield |
---|---|
In tetrahydrofuran at 90℃; for 36h; | 99% |
3-Chloro-4-fluorobenzaldehyde
ethyl acetoacetate
dimedone
ethyl 4-(3-chloro-4-fluorophenyl)-1,4,5,6,7,8-hexahydro-2,7,7-trimethyl-5-oxoquinoline-3-carboxylate
Conditions | Yield |
---|---|
With ammonium acetate In acetonitrile at 20℃; for 0.0333333h; Hantzsch pyridine synthesis; | 98% |
Conditions | Yield |
---|---|
Stage #1: 3-Chloro-4-fluorobenzaldehyde; 5-(aminomethyl)-2-chloropyridine In methanol at 20℃; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 0.333333h; | 96.7% |
malonic acid
3-Chloro-4-fluorobenzaldehyde
(E)-3-(3-chloro-4-fluorophenyl)acrylic acid
Conditions | Yield |
---|---|
With piperidine for 4h; Reagent/catalyst; Temperature; Knoevenagel Condensation; Reflux; diastereoselective reaction; | 96% |
With piperidine; pyridine at 70℃; Knoevenagel reaction; |
Methyl 3-mercaptopropionate
3-Chloro-4-fluorobenzaldehyde
3-(2-chloro-4-formyl-phenylsulfanyl)-propionic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 2h; | 95% |
D-Sorbose
3-Chloro-4-fluorobenzaldehyde
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol; cyclohexane; water | 95% |
3-Chloro-4-fluorobenzaldehyde
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 1h; Inert atmosphere; | 95% |
1H-imidazole
3-Chloro-4-fluorobenzaldehyde
3-chloro-4-(1H-imidazol-1-yl)benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate; copper(II) oxide In N,N-dimethyl-formamide at 120℃; for 2h; | 94% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; |
3-Chloro-4-fluorobenzaldehyde
2-hydroxy-5-methyl-3-nitroacetophenone
A
N-(3-{(E)-3-[4-(benzyloxy)-3-bromophenyl]-2-propenoyl}-2-hydroxy-5-methylphenyl)acetamide
B
(E)-3-(3-chloro-4-fluorophenyl)-1-(2-hydroxy-5-methyl-3-nitrophenyl)-2-propen-1-one
Conditions | Yield |
---|---|
A 94% B n/a |
3-Chloro-4-fluorobenzaldehyde
ethyl (triphenylphosphoranylidene)acetate
ethyl (2E)-3-(3-chloro-4-fluorophenyl)acrylate
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 94% |
3-Chloro-4-fluorobenzaldehyde
5-amino-2-cyanopyridine
5-[(3-chloro-4-fluoro-benzylidene)-amino]-pyridine-2-carbonitrile
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 12h; Reflux; | 93.6% |
With toluene-4-sulfonic acid In toluene for 12h; Reflux; | 93.6% |
Conditions | Yield |
---|---|
With C23H3BF16N2O In toluene at 25℃; for 3h; Green chemistry; | 93% |
3-Chloro-4-fluorobenzaldehyde
1-methyl-4-nitrobenzene
triethyl phosphite
Conditions | Yield |
---|---|
With hydrogenchloride; indium In water at 20℃; for 0.833333h; | 92% |
3-Chloro-4-fluorobenzaldehyde
4-(2,4-dichlorophenyl)-1,3-thiazol-2-amine
triethyl phosphite
Conditions | Yield |
---|---|
With nano-BF3/SiO2 In neat (no solvent) at 20℃; for 0.233333h; Temperature; Kabachnik-Fields Reaction; Sonication; Green chemistry; | 92% |
3-Chloro-4-fluorobenzaldehyde
(R)-2-methylpropane-2-sulfinamide
Conditions | Yield |
---|---|
With titanium(IV) tetraethanolate In dichloromethane for 20h; | 92% |
3-Chloro-4-fluorobenzaldehyde
3-chloro-4-fluorobenzonitrile
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; zinc(II) oxide for 0.0166667h; Microwave irradiation; neat (no solvent); | 91% |
With hydroxylamine hydrochloride; toluene-4-sulfonic acid for 0.0111111h; Microwave irradiation; | 85% |
4-Amino-2,6-dihydroxypyrimidine
3-Chloro-4-fluorobenzaldehyde
3-methyl-2-pyrazoline-5-one
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 70℃; | 91% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 18h; | 90% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 18h; Inert atmosphere; | 90% |
3-Chloro-4-fluorobenzaldehyde
hydroxy-2-propanone
Conditions | Yield |
---|---|
With (1S,2S)-N'-methyl-N'-((S)-1-phenylethyl)cyclohexane-1,2-diamine; trifluoroacetic acid In water; N,N-dimethyl-formamide at 20℃; aldol reaction; optical yield given as %ee; enantioselective reaction; | 89% |
3-Chloro-4-fluorobenzaldehyde
thiophenol
3-chloro-4-(phenylthio)benzaldehyde
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 100℃; | 89% |
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In dichloromethane at 20℃; for 0.123333h; Flow reactor; | 89% |
2-methylfuran
3-Chloro-4-fluorobenzaldehyde
Conditions | Yield |
---|---|
With aminosulfonic acid at 70℃; for 6h; | 89% |
3-aminohept-2-enoic acid ethyl ester
2H-pyran-3,5(4H,6H)-dione
3-Chloro-4-fluorobenzaldehyde
2-butyl-4-(3-chloro-4-fluoro-phenyl)-5-oxo-4,5,6,8-tetrahydro-1H-pyrano[3,4-b]pyridine-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
In ethanol at 80℃; for 16h; | 88% |
4-Amino-2,6-dihydroxypyrimidine
3-Chloro-4-fluorobenzaldehyde
malononitrile
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 70℃; | 88% |
3-Chloro-4-fluorobenzaldehyde
Conditions | Yield |
---|---|
With piperidine In ethanol for 8h; Reflux; | 88% |
3-Chloro-4-fluorobenzaldehyde
2,3-diamino-1,4-naphthoquinone
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 70℃; | 87% |
3-Chloro-4-fluorobenzaldehyde
1-(3-chloro-4-fluorophenyl)-1H-1,2,3,4-tetrazole
Conditions | Yield |
---|---|
With sodium azide In methanol at 20℃; for 5h; Irradiation; regioselective reaction; | 87% |
3-Chloro-4-fluorobenzaldehyde
sodium methansulfinate
3-chloro-4-(methylsulfonyl)benzaldehyde
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 80℃; | 86% |
In dimethyl sulfoxide at 90℃; for 6h; | |
In dimethyl sulfoxide at 70℃; |
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