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chlorine
A
trithiazyl trichloride
B
sulfur dichloride
Conditions | Yield |
---|---|
A 88% B n/a |
sulfur
diselenium dichloride
A
disulfur dichloride
B
sulfur selenium dichloride
C
sulfur dichloride
D
selenium tetrachloride
Conditions | Yield |
---|---|
In neat (no solvent) heating of equimolar amount in closed tube to 200°C for 6 h;; fractional distillation;; | A n/a B 30% C n/a D n/a |
In neat (no solvent) heating of equimolar amount in closed tube to 200°C for 6 h;; fractional distillation;; | A n/a B 30% C n/a D n/a |
In neat (no solvent) heating of equimolar amount in closed tube to 100, 150, 200 or 250°C for 6 h;; fractional distillation;; | |
In neat (no solvent) heating of equimolar amount in closed tube to 100, 150, 200 or 250°C for 6 h;; fractional distillation;; |
disulfur dichloride
selenium
B
sulfur dichloride
C
selenium tetrachloride
Conditions | Yield |
---|---|
In neat (no solvent) heating in closed tube to 200°C for 4 h;; fractional distillation;; | A 13.2% B n/a C n/a |
In neat (no solvent) heating in closed tube to 200°C for 4 h;; fractional distillation;; | A 13.2% B n/a C n/a |
In neat (no solvent) heating in closed tube at 100, 150, 200 or 250°C for 4 h;; fractional distillation;; | |
In neat (no solvent) heating in closed tube at 100, 150, 200 or 250°C for 4 h;; fractional distillation;; |
carbon disulfide
A
dichloromethanebis(sulphenyl chloride)
B
sulfur dichloride
C
chlorothio-trichloro-methane
Conditions | Yield |
---|---|
With chlorine at -20 - -5℃; for 2.5h; Irradiation; Yields of byproduct given; | A 1.58% B n/a C n/a |
With chlorine at -20 - -5℃; for 2.5h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
C
sulfur dichloride
D
chloride
Conditions | Yield |
---|---|
In not given molar ratio of Ba(OCl)2:Na2S2O3=2:1, warmed; |
Conditions | Yield |
---|---|
In neat (no solvent) at ambient temp. and 4000 Torr;; | A n/a B >99 |
Conditions | Yield |
---|---|
below 200°C;; almost pure;; | A n/a B n/a C >99 |
disulfur dichloride
sulfur trioxide
chlorine
A
thionyl chloride
B
sulfur dichloride
Conditions | Yield |
---|---|
In neat (no solvent) 100-110°C; iron reactor, presence of SbCl3;; distillation over S (formation of educt S2Cl2 from SCl2);; |
Conditions | Yield |
---|---|
Formation of spectroscopic detectable amounts of SO.; |
chlorine
sulfur
A
disulfur dichloride
B
sulfur dichloride
C
vanadiumtetrachloride
D
vanadium(V) oxychloride
Conditions | Yield |
---|---|
In neat (no solvent) heating;; |
thionyl chloride
A
disulfur dichloride
B
sulfur dichloride
C
sulfur dioxide
D
chlorine
Conditions | Yield |
---|---|
In gas passing through glass tube (red heat); discoloration;; | |
In neat (no solvent, gas phase) passing through glass tube (red heat); discoloration;; |
Conditions | Yield |
---|---|
In neat (no solvent) thermal dissociation (reversible);; | |
In neat (no solvent) thermal dissociation (reversible);; |
disulfur dichloride
sulfuryl dichloride
A
sulfur dichloride
B
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) on heating, without AlCl3;; | A 0% B 0% |
In neat (no solvent) on heating, in presence of AlCl3;; | |
In neat (no solvent) on heating, without AlCl3;; | A 0% B 0% |
In neat (no solvent) on heating, in presence of AlCl3;; |
sulfuryl dichloride
hydrogen sulfide
A
disulfur dichloride
B
sulfur dichloride
C
sulfur dioxide
D
sulfur
Conditions | Yield |
---|---|
byproducts: HCl, H2O, H2SO4; room temp., excess of SO2Cl2 (8:1); | |
byproducts: HCl, H2O, H2SO4; room temp., excess of SO2Cl2 (8:1); |
antimonypentachloride
antimony(III) chloride
A
disulfur dichloride
B
sulfur dichloride
Conditions | Yield |
---|---|
by distn. at normal pressure; | |
by distn. at normal pressure; |
trichlorothiophosphine
chlorine
A
phosphorus pentachloride
B
sulfur dichloride
Conditions | Yield |
---|---|
In not given react. of PSCl3 with Cl2;; | |
In not given react. of PSCl3 with Cl2;; |
Conditions | Yield |
---|---|
With chlorine In neat (no solvent) Kinetics; at ambient temp. and 350 - 483 Torr;; |
Conditions | Yield |
---|---|
With anthracite In neat (no solvent) passing Cl2 through heated (750°C) mixture;; |
Conditions | Yield |
---|---|
In neat (no solvent) heating;; | |
In neat (no solvent) heating;; |
Conditions | Yield |
---|---|
With chlorine with dry Cl2 gas; by fractionated distn.; | |
With Cl2 with dry Cl2 gas; by fractionated distn.; |
sulphur monochloride
sulfur dichloride
Conditions | Yield |
---|---|
With chlorine In gaseous matrix Kinetics; byproducts: Cl; equilibrium , Pyrex discharge-flow system , T=295K , He carrier gas; detection of free radicals and molecular species by molecular-beam-sampling quadrupole MS; |
sulphur monochloride
A
disulfur
B
S2Cl
C
sulfur dichloride
D
sulfur
Conditions | Yield |
---|---|
With C2H4S In gaseous matrix byproducts: C2H4; disproportionation , Pyrex discharge-flow system , T=295K , excess of C2H4S , He carrier gas; detection of free radicals and molecular species by molecular-beam-sampling quadrupole MS; | |
With chlorine In gaseous matrix Kinetics; byproducts: Cl , Cl2; disproportionation , Pyrex discharge-flow system , T=295K , He carrier gas , excess of Cl atoms; detection of free radicals and molecular species by molecular-beam-sampling quadrupole MS; |
dichlorofluoromethanesulphenyl chloride
A
disulfur dichloride
B
chlorotrifluoromethane
C
Bis(trifluoromethyl)disulfid
D
sulfur dichloride
Conditions | Yield |
---|---|
byproducts: S; Irradiation (UV/VIS); 14 d in quartz bomb; | |
byproducts: S; Irradiation (UV/VIS); 14 d in quartz bomb; |
fluorochloroisothiocyanatomethansulphenyl chloride
A
Dichloro-fluoro-isothiocyanato-methane
B
sulfur dichloride
Conditions | Yield |
---|---|
With chlorine 40°C; | |
With chlorine 40°C; |
fluoro-trifluoromethyldithiomethylene-trifluoromethylmercaptoamine
A
Trifluoromethylsulfenyl chloride
B
chlorofluoromethylene-trifluoromethylmercaptoamine
C
sulfur dichloride
Conditions | Yield |
---|---|
With chlorine | |
With Cl2 |
Conditions | Yield |
---|---|
With chlorine dry Cl2 stream; | |
With Cl2 dry Cl2 stream; |
sulfur dichloride
sulfur trioxide
A
thionyl chloride
B
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) below -10°C or under pressure;; | A 100% B n/a |
sulfur dichloride
B
diferroceno[1,2-c:1'',2''-g][1,2,5,6]tetrathiocin
Conditions | Yield |
---|---|
In dichloromethane (N2); treating iron compd. with 1.1 equiv. of sulphur dichloride in CH2Cl2 at 0°C; | A 99% B 30% |
In tetrahydrofuran (N2); addn. of 1.1 equiv. of sulphur dichloride to soln. of iron compd. in THF at 0°C, stirring for 10 min; addn. to ice water, extn. (CHCl3), drying over MgSO4, evapn., chromy. (silica gel, chloroform/hexane (1:1)); | A 95% B 37% |
In tetrahydrofuran (N2); treating iron compd. with excess of sulphur dichloride in THF at 0°C; | A 50% B 0% |
sulfur dichloride
molybdenum hexacarbonyl
Conditions | Yield |
---|---|
In tetrachloromethane byproducts: CO, S; 80°C, 0.5 h; | 98% |
In chloroform byproducts: CO, S; 80°C, 2 h; | 95% |
In hexane byproducts: CO, S; 25°C, 12 h (pptn.); filtration, washing (CHCl3), drying (vac., 150°C); elem. anal.; | 95% |
In chloroform byproducts: CO, S; 25°C, 2 h; | 93% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: S2Cl2; (Ar); heating (80-90°C, 4-6 h); pptn. on cooling, recrystn. (SCl2), drying (Cl2 flow); elem. anal.; | 98% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: SO2; (Ar);; pptn. on cooling, recrystn. (SCl2), drying (Cl2 flow); elem. anal.; | 98% |
sulfur dichloride
Conditions | Yield |
---|---|
In tetrahydrofuran soln. SCl2 in THF was added dropwise at -10°C to stirred soln. Cocomplex in THF, mixt. was stirred for 40 min; solvent was evapd. in vac., residue was washed with hexane; elem. anal.; | 98% |
Conditions | Yield |
---|---|
In tetrachloromethane mole ratio 1:2 at -5-(-8)°C; 5 h; | 96% |
In neat (no solvent) mole ratio 1:2 at -5-(-8)°C; 5 h; | 88% |
trithiazyl trichloride
silver(I) hexafluoroarsenate
sulfur dichloride
dichlorodithionitronium hexafluoroarsenate
Conditions | Yield |
---|---|
In sulfur dioxide byproducts: AgCl; (N2); stirring (NSCl)3 and AgAsF6 in SO2, addn. of SCl2, stirring, 18 h; filtering off ppt. (AgCl), washing with SO2, evapg. solvent, pumping to dryness; elem. anal.; | 96% |
sulfur dichloride
tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III)
Conditions | Yield |
---|---|
In tetrahydrofuran soln. SCl2 in THF was added dropwise at -10°C to stirred soln. complex in THF, mixt. was stirred for 40 min; solvent was evapd. in vac.; elem. anal.; | 94% |
tungsten hexacarbonyl
sulfur dichloride
tungsten(VI) sulfide tetrachloride
Conditions | Yield |
---|---|
In hexane byproducts: CO, S; 70°C, 0.5 h (pptn.); filtration, drying, sublimation (120°C, 0.1 Torr); elem. anal.; | 93% |
In tetrachloromethane byproducts: CO, S; 80°C, 0.5 h; | 80% |
sulfur dichloride
Conditions | Yield |
---|---|
In tetrahydrofuran soln. SCl2 in THF was added dropwise at -10°C to stirred soln. Alcomplex in THF, mixt. was stirred for 40 min; solvent was evapd. in vac., residue was washed with hexane; elem. anal.; | 93% |
Conditions | Yield |
---|---|
excess SCl2; | 92% |
Conditions | Yield |
---|---|
excess SCl2; | 92% |
chromium(pivaloylacetonate)3
sulfur dichloride
tris(3-chlorosulfenyl-5,5-dimethyl-2,4-hexanedionato)chromium(III)
Conditions | Yield |
---|---|
In hexane SCl2 was added dropwise to stirred suspn. Cr complex in hexane, mixt. was stirred for 15 min; ppt. was filtered off, washed with hexane and vac.-dried; elem. anal.; | 92% |
sulfur dichloride
tris(2-chlorosulfenyl-2,4-pentanedionato)rhodium(III)
Conditions | Yield |
---|---|
In hexane SCl2 was added dropwise to stirred suspn. Rh complex in hexane, mixt. was stirred for 10 min; ppt. was filtered off, washed with hexane and vac.-dried; elem. anal.; | 92% |
sulfur dichloride
bis(indenyl)zirconium(IV) dichloride
Conditions | Yield |
---|---|
In toluene (N2); a soln. of SCl2 in toluene added to a suspn. of Zr complex in toluene, stirred for 45 min at room temp.; evapd. (vac.); | 91.4% |
In dichloromethane (N2); a soln. of SCl2 in CH2Cl2 added to a suspn. of Zr complex in CH2Cl2, stirred for 3 h at room temp., addnl. SCl2 added, stirred for 1 h; evapd. (vac.), obtained impure; |
Conditions | Yield |
---|---|
With antimony pentafluoride 60°C, 1 h; | 90% |
With SbF5 60°C, 1 h; | 90% |
Conditions | Yield |
---|---|
great excess of SCl2; -10°C-0°C; | 90% |
great excess of SCl2; -80°C; | 90% |
In tetrachloromethane -20°C; | >99 |
sulfur dichloride
Conditions | Yield |
---|---|
With sodium carbonate In dichloromethane under Ar; to a mixt. of the Cr complex and Na2CO3 in CH2Cl2 was added SCl2 in CH2Cl2, stirred for 2 d at 0°C; filtered, solvent was removed under reduced pressure, fractionated withEt2O; elem. anal.; | 90% |
sulfur dichloride
Conditions | Yield |
---|---|
In hexane SCl2 was added dropwise to stirred suspn. Cr complex in hexane, mixt. was stirred for 10 min; ppt. was filtered off, washed with hexane and vac.-dried; elem. anal.; | 90% |
tris(2,4-pentanedionato)ruthenium(III)
sulfur dichloride
tris(2-chlorosulfenyl-2,4-pentanedionato)ruthenium(III)
Conditions | Yield |
---|---|
In hexane SCl2 was added dropwise to stirred suspn. Ru complex in hexane, mixt. was stirred for 10 min; ppt. was filtered off, washed with hexane and vac.-dried; elem. anal.; | 89% |
Conditions | Yield |
---|---|
In dichloromethane under argon, Se(N(SiMe3)2)2in CH2Cl2 was cooled at -196°C, SCl2 was condensed to the solution, warmed up under stirring to 22°C, stirring 1 h at 22°C,; after 24 h decanted and washed with CH2Cl2, drying under vacuo,elem. anal.; | 86% |
sulfur dichloride
triphenylantimony
triphenylantimony dichloride
Conditions | Yield |
---|---|
In diethyl ether room temp., 0.5 h; | 85% |
In diethyl ether room temp., 0.5 h; | 85% |
Conditions | Yield |
---|---|
With 2,4,6-trimethylpyridine In benzene elem. anal.; | 85% |
trithiazyl trichloride
sulfur dichloride
selenium tetrachloride
Conditions | Yield |
---|---|
In thionyl chloride (N2); stirring (NSCl)3 and SeCl4 in SOCl2, addn. of SCl2, heating to reflux, 6 h; allowing to cool, filtering off ppt., washing with ice-cold SOCl2; elem. anal.; | 84% |
sulfur dichloride
lithium perfluoro isopropylideneamide
bis(hexafluoroisopropylidene amino) sulfane
Conditions | Yield |
---|---|
83% | |
83% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: chlorotrimethylsilane; -80°C, stirring for 5 min; crystd., sepd., dried at 20°C (7mm); elem.anal.; | 82% |
In neat (no solvent) byproducts: (CH3)3SiCl; SCl2 and (CH3)3SiCN are stirred at 0°C for 2 h; sublimation (vac.); | 80% |
sulfur dichloride
sulfur trioxide
A
thionyl chloride
B
pyrosulfuryl chloride
C
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) SO3 is distilled (from 65 % oleum) into cooled (ice/water) vessel containing SCl2; evolution of SO2;; multiple fractionation (at last in presence of sulfur);; | A 80% B n/a C n/a |
4-(perfluoro tolyl) magnesiumbromide
sulfur dichloride
bis(2,3,5,6-tetrafluoro-4-trifluoromethylphenyl) sulfide
Conditions | Yield |
---|---|
80% | |
80% |
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