Thionyl chloride CAS:7719-09-7 Specification Welcome to contact us to get complete COA. Shanghai Lonwin Chemical Co.,Ltd is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceutic
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
low price and good quality Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and D
sulfur dichloride
sulfur trioxide
A
thionyl chloride
B
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) below -10°C or under pressure;; | A 100% B n/a |
hydrogenchloride
N-phenylsulfinylamine
A
thionyl chloride
B
aniline hydrochloride
Conditions | Yield |
---|---|
In Petroleum ether decompn. of thioaniline dissolved in dild. petroleum (b.p. 200-250°C) on introduction of dry HCl (shaking) at -10°C;; filtration (anilinium chloride); fractionation;; | A 94% B n/a |
sulfur dichloride
sulfur trioxide
A
thionyl chloride
B
pyrosulfuryl chloride
C
sulfur dioxide
Conditions | Yield |
---|---|
In neat (no solvent) SO3 is distilled (from 65 % oleum) into cooled (ice/water) vessel containing SCl2; evolution of SO2;; multiple fractionation (at last in presence of sulfur);; | A 80% B n/a C n/a |
Conditions | Yield |
---|---|
With sulfur dioxide In neat (no solvent) reaction of CCl4 with SO2 on heating to 200°C;; | A n/a B 72% |
Ethanesulfonyl chloride
A
thionyl chloride
B
chloroethane
C
phosphorus pentachloride
D
trichlorophosphate
phosphorus pentachloride
benzenesulfonyl chloride
A
thionyl chloride
B
chlorobenzene
C
trichlorophosphate
Conditions | Yield |
---|---|
at 200 - 210℃; |
Conditions | Yield |
---|---|
at 200℃; unter Druck; |
Conditions | Yield |
---|---|
at 200 - 400℃; |
Trichloromethanesulfonyl chloride
A
tetrachloromethane
B
phosgene
C
thionyl chloride
Conditions | Yield |
---|---|
at 200℃; |
Conditions | Yield |
---|---|
at 150℃; |
diethyl sulphite
phosphorus pentachloride
A
thionyl chloride
B
ethyl chlorosulfite
C
chloroethane
Conditions | Yield |
---|---|
bei niedrigerer Temperatur; |
dipropyl sulfite
phosphorus pentachloride
A
thionyl chloride
B
1-Chloropropane
Conditions | Yield |
---|---|
beim Erwaermen; |
sulfurous acid dibutyl ester
phosphorus pentachloride
A
thionyl chloride
B
n-Butyl chloride
Conditions | Yield |
---|---|
bei schwachem Erwaermen; |
aluminium trichloride
sulfuryl dichloride
1,2,4,5-tetrachlorobenzene
A
tetrachloromethane
B
thionyl chloride
C
pentachlorobenzene
D
hexachlorobenzene
ethyl chlorosulfite
phosphorus pentachloride
A
thionyl chloride
B
chloroethane
C
trichlorophosphate
Conditions | Yield |
---|---|
at 25℃; |
p-hydoroxybenzenesulfonic acid
phosphorus pentachloride
A
thionyl chloride
B
para-dichlorobenzene
C
4-chlorophenylphosphorodichloridate
D
trichlorophosphate
Conditions | Yield |
---|---|
Reaktion des Kaliumsalzes; |
diethyl sulphite
phosphorus pentachloride
A
thionyl chloride
B
chloroethane
phosphorus pentachloride
4,4'-sulfonyl-bis-benzenesulfonyl chloride
A
thionyl chloride
B
para-dichlorobenzene
C
trichlorophosphate
D
phosphorus trichloride
phosphorus pentachloride
1-Naphthalenesulfonyl chloride
A
thionyl chloride
B
trichlorophosphate
C
1-Chloronaphthalene
Conditions | Yield |
---|---|
at 150 - 160℃; |
phenyltetrachlorophosphorane
A
P,P-dichlorophenylphosphine oxide
B
thionyl chloride
Conditions | Yield |
---|---|
at 70℃; Einleiten von HCl; |
phenyl chlorosulphinate
trichlorophosphate
A
thionyl chloride
B
phosphoric acid triphenyl ester
2-benzoylamino-[1]naphthoic acid
A
thionyl chloride
phosphorus pentachloride
A
thionyl chloride
B
1,2-dichloro-benzene
Conditions | Yield |
---|---|
at 200 - 210℃; |
A
thionyl chloride
B
N,N-dipropylphosphoramidic dichloride
C
trichlorophosphate
phosphorus pentachloride
A
thionyl chloride
B
benzyl chloride
C
trichlorophosphate
A
thionyl chloride
Conditions | Yield |
---|---|
In acetone |
carbon disulfide
hypochlorous anhydride
A
phosgene
B
thionyl chloride
Conditions | Yield |
---|---|
In tetrachloromethane CS2 dild. in CCl4 (to diminuish vehemence of reaction);; | |
In tetrachloromethane |
thionyl chloride
methyl (S)-4,5,6,7-tetrahydro-3H-imidazo[4,5-c]pyridine-6-carboxylate hydrochloric acid salt
Conditions | Yield |
---|---|
In methanol for 3.5h; Heating / reflux; | 100% |
thionyl chloride
Conditions | Yield |
---|---|
In thionyl chloride (argon); stirring (ca. 16 h); pptn. with Et2O, washing (Et2O), drying (vac.); | 100% |
thionyl chloride
Conditions | Yield |
---|---|
In thionyl chloride (argon); stirring (ca. 16 h); pptn. with Et2O, washing (Et2O), drying (vac.); | 100% |
thionyl chloride
(5,7,12,14-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecinate(2-))VCl2
Conditions | Yield |
---|---|
In dichloromethane (Ar); react. (0°C), warming (room temp.), stirring (6 h), solventevapn.; washing (diethyl ether, pentane), drying (high vacuum, 50°C, 8 h); | 100% |
Conditions | Yield |
---|---|
In thionyl chloride vac., 150°C, 3 d; | 100% |
thionyl chloride
2-(2,6-dichlorophenyl)acetic acid
1-bromo-3-(2,6-dichlorophenyl)propan-2-one
Conditions | Yield |
---|---|
Stage #1: thionyl chloride; 2-(2,6-dichlorophenyl)acetic acid With diazomethyl-trimethyl-silane Stage #2: With hydrogen bromide In water | 100% |
Conditions | Yield |
---|---|
100% |
thionyl chloride
4-[1-(trifluoroacetyl)piperidin-4-yl]benzoic acid
4-(1-(2,2,2-trifluoroacetyl)piperidin-4-yl)benzoyl chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 70℃; for 5h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate at 35℃; for 4h; Inert atmosphere; | 100% |
thionyl chloride
Conditions | Yield |
---|---|
at 80℃; for 12h; | 100% |
methanol
thionyl chloride
4-nitro-1H-pyrazole-3-carboxylic acid
methyl 4-nitro-1H-pyrazole-3-carboxylate
Conditions | Yield |
---|---|
at 0 - 25℃; for 16 - 48h; Product distribution / selectivity; | 99.5% |
Conditions | Yield |
---|---|
In diethyl ether byproducts: SO2; to finely ground dry Ag salt in anhyd. Et2O cooled to 0°C added dropwise with vigorous stirring equimolar amt. of thionyl chloride; suspn. stirred for 15 min; soln. was decanted from AgCl; AgCl dried; soln. washed (Et2O); all extracts combined; cooled to 0°C; | A n/a B 99% |
Conditions | Yield |
---|---|
In diethyl ether byproducts: SO2, SO3; to finely ground dry Ag salt in anhyd. Et2O cooled to 0°C added dropwise with vigorous stirring equimolar amt. of thionyl chloride; suspn. stirred for 15 min; soln. was decanted from AgCl; AgCl dried; soln. washed (Et2O); all extracts combined; cooled to 0°C; | A n/a B n/a C 99% |
thionyl chloride
Conditions | Yield |
---|---|
In dichloromethane (N2); stirring (4 h, reflux); solvent removal (reduced pressure), drying (vac., 60-70 degree.C, 1 h); elem. anal.; | 99% |
thionyl chloride
Conditions | Yield |
---|---|
In dichloromethane SOCl2 added to CH2Cl2 soln. of B compd. (molar ratio 1:3, 1:4); concd. slowly; ppt. purified by column chromy. (silica gel, CH2Cl2); | 99% |
In neat (no solvent) excess of SOCl2 added to B compd.; purified by column chromy. (silica gel, CH2Cl2); | 99% |
In dichloromethane SOCl2 added to CH2Cl2 soln. of B compd. (molar ratio 2:1, 1:1, 1:2); concd. slowly; mixt. of the starting B compd. and title compd. pptd.; purified by column chromy. (silica gel, CH2Cl2); | 15% |
thionyl chloride
[(C5(CH3)5)TiCl(C5H4C(CH3)2CH2CO2)]
[(C5(CH3)5)TiCl2(C5H4C(CH3)2CH2COCl)]
Conditions | Yield |
---|---|
In not given | 99% |
thionyl chloride
chloro(cyclopentadienyl)(cyclopentadienyl-3-methyl-3-butanoate)titanium(IV)
Cp(CpCMe2CH2COCl)titanium(IV)dichloride
Conditions | Yield |
---|---|
In not given | 99% |
In neat (no solvent) at 20℃; for 1h; Inert atmosphere; Schlenk technique; Glovebox; |
thionyl chloride
[(C5H5)TiCl(C5H4C(CH2)5CH2CO2)]
[(C5H5)TiCl2(C5H4C(CH2)5CH2COCl)]
Conditions | Yield |
---|---|
In not given | 99% |
thionyl chloride
chloro(cyclopentadienyl)(cyclopentadienyl-3-methyl-3-butanoate)titanium(IV)
cholesterol
Conditions | Yield |
---|---|
With sodium hydride In dichloromethane mixt. of Ti complex and SOCl2 was stirred for 3 h; evapd. (vac., 80°C); dissolved in CH2Cl2; added to mixt. of NaH and cholesterol; stirred for 16 h; filtered; solvent removed (vac.); crystd. (CH2Cl2); | 99% |
Conditions | Yield |
---|---|
With sodium hydride In dichloromethane mixt. of Ti complex and SOCl2 was stirred for 3 h; evapd. (vac., 80°C); dissolved in CH2Cl2; added to mixt. of NaH and cholesterol; stirred for 16 h; filtered; solvent removed (vac.); crystd. (CH2Cl2); | 99% |
thionyl chloride
(4R,5S)-5-phenylthio-4-octanol
((4S,5R)-5-chlorooctan-4-yl)(phenyl)sulfane
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide In dichloromethane at 0℃; for 0.5h; Inert atmosphere; optical yield given as %ee; | 99% |
thionyl chloride
1,7-dihydroxycarbonyl-1,7-dicarba-closo-dodecaborane
m-carborane-1,7-dicarboxylic acid dichloride
Conditions | Yield |
---|---|
In thionyl chloride B compd. and SOCl2 placed into a flask under N2, refluxed for 24 h; evapd. (vac.); obtained as an oil; | 99% |
thionyl chloride
tris(8-carboxyl-2,2,6,6-tetramethylbenzo[1,2-d;4,5-d′]bis[1,3]dithiol-4-yl)methyl radical sodium salt
C40H36Cl3O3S12
Conditions | Yield |
---|---|
Stage #1: tris(8-carboxyl-2,2,6,6-tetramethylbenzo[1,2-d;4,5-d′]bis[1,3]dithiol-4-yl)methyl radical sodium salt With triethylamine In chloroform at 20℃; for 0.5h; Stage #2: thionyl chloride In chloroform at 20 - 50℃; | 99% |
Conditions | Yield |
---|---|
In acetonitrile TlCl suspd. in CH3CN; Cl2 added under vigorous stirring; stirred for 30 min; soln. filtered; solvent evapd. in vacuum; SOCl2 added; evapd. after 10 min; | 98.5% |
thionyl chloride
tetrabenzyltin
A
phenylmethanesulfinyl chloride
B
dibenzyltin(IV) dichloride
Conditions | Yield |
---|---|
In not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.; | A n/a B 98% |
thionyl chloride
(29H,31H-2,9,16,23-tetracarboxyphthalocyaninato-N(29),N(30),N(31),N(32))cobalt(II)
cobalt tetra-4-(chlorocarbonyl)phthalocyanine
Conditions | Yield |
---|---|
In benzene a mixt. in dry benzene was refluxed for 7 h; filtered, washed with dry benzene, dried in a vac. at room temp.; | 98% |
With pyridine In benzene at 80℃; | 96% |
thionyl chloride
2-chloro-4-(trifluoromethyl)-5-thiazolecarboxylic acid
2-chloro-4-(trifluoromethyl)-5-thiazolecarbonyl chloride
Conditions | Yield |
---|---|
6 h refluxing with excess SOCl2; | 98% |
thionyl chloride
(m-carborane-9,10-diyl)diacetic acids
(m-carboranyl-9,10-diyl)di(acetyl chlorides)
Conditions | Yield |
---|---|
In benzene byproducts: SO2, HCl; addn. of SOCl2 to soln. of (CH2COOH)2C2B10H10 in dry benzene at 20°C; heating for 2 h; cooling, removal of solvent and excess SOCl2 in vac.; | 98% |
thionyl chloride
C6H3F2N2(1+)*Cl(1-)
2,3-difluorobenzenesulphonyl chloride
Conditions | Yield |
---|---|
Stage #1: thionyl chloride With copper(l) chloride In water at -5 - 20℃; Stage #2: C6H3F2N2(1+)*Cl(1-) In water at -5℃; for 0.5h; | 98% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View