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Cas:6575-24-2
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Cas:6575-24-2
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inquiryProduct description: Product name 2,6-Dichlorophenylacetic acid CAS number 6575-24-2 Assay ≥99% Appearance White solid Capacity 200mt/year Application Organic synthesis inter
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Min.Order:10 Gram
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inquiry2,6-Dichlorophenylacetic acid CAS:6575-24-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org
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Min.Order:1 Gram
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Negotiable
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inquiryProName:2,6-Dichlorophenylacetic acid CasNo:6575-24-2 Molecular Formula:C8H6Cl2O2 Appearance:White solid Application:Organic synthesis intermediate DeliveryTime:Immediately PackAge:25kg/drum Port:Shanghai or Qingdao ProductionCapacity:200 M
Cas:6575-24-2
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
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Cas:6575-24-2
Min.Order:10 Gram
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inquiry2,6-Dichlorophenylacetic acid Basic information Product Name: 2,6-Dichlorophenylacetic acid Synonyms: 2-(2,6-DICHLOROPHENYL)ACETIC ACID;2,6-DICHLORO BENZENEACETIC ACID;2,6-DICHLOROPHENYLACETIC ACID;RARECHEM AL BO 0115;TIMTEC-BB SBB003503;2,6-D
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Type:Trading Company
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Cas:6575-24-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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2,2,6,6-tetrachlorocyclohexanone
diethyl malonate
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
Stage #1: 2,2,6,6-tetrachlorocyclohexanone; diethyl malonate With 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,2-dichloro-ethane at 60 - 65℃; for 3h; Stage #2: With sodium hydroxide In 1,2-dichloro-ethane at 20 - 65℃; for 3h; Solvent; Temperature; Reagent/catalyst; | 96.6% |
ethyl 2-(2,6-dichlorophenyl)acetate
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With water; sodium hydroxide In 1,4-dioxane at 60℃; for 2h; pH=10 - 14; | 95% |
carbon monoxide
1,3-Dichloro-2-chloromethyl-benzene
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; tetraethylammonium chloride; sodium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene at 80℃; under 11251.1 Torr; for 20h; Autoclave; regioselective reaction; | 93% |
Conditions | Yield |
---|---|
Stage #1: 2,6-dichlorophenylacetonitrile With potassium hydroxide; water In ethanol at 80℃; for 20h; Stage #2: With hydrogenchloride In ethanol pH=3; | 83% |
With sodium hydroxide | |
With potassium hydroxide In ethylene glycol |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
Einleiten von Kohlendioxid; |
Conditions | Yield |
---|---|
Stage #1: 2,6-dichlorotoluene With lithium diisopropyl amide In tetrahydrofuran; cyclohexane at -75℃; for 0.75h; Stage #2: carbon dioxide In tetrahydrofuran; cyclohexane |
carbon dioxide
2,6-dichlorotoluene
A
2-(2,6-dichlorophenyl)acetic acid
B
3,5-dichloro-4-methylbenzoic acid
C
2,4-Dichloro-3-methyl-benzoic acid
Conditions | Yield |
---|---|
Stage #1: 2,6-dichlorotoluene With sec.-butyllithium In tetrahydrofuran; cyclohexane at -75℃; for 0.75h; Stage #2: carbon dioxide In tetrahydrofuran; cyclohexane Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylsulfoxide / 5 h / 40 - 50 °C 2: 25 percent NaOH / ethanol / Heating View Scheme | |
Multi-step reaction with 2 steps 2: aqueous NaOH View Scheme | |
Multi-step reaction with 2 steps 2: H2SO4 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloro[4,5-bis(diphenylphosphino)-9,9’-dimethylxanthene]palladium(II); di-tert-butyl peroxide / 16 h / 120 °C / 7600.51 Torr 2: water; sodium hydroxide / 1,4-dioxane / 2 h / 60 °C / pH 10 - 14 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium nitrite; sulfuric acid; copper(I) bromide; tetrabutylammomium bromide / water / 2 h / -5 - 95 °C 2: hydrogenchloride / 10 h / 80 - 95 °C / Inert atmosphere View Scheme |
1-(2,2,2-trichloroethyl)-2,6-dichlorobenzene
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride at 80 - 95℃; for 10h; Inert atmosphere; | 115.3 g |
2-(2,6-dichlorophenyl)acetic acid
2,6-dichlorophenylacetylchloride
Conditions | Yield |
---|---|
With thionyl chloride In toluene at 20℃; for 12h; | 100% |
With thionyl chloride at 80℃; for 1h; | 90% |
With thionyl chloride |
thionyl chloride
2-(2,6-dichlorophenyl)acetic acid
1-bromo-3-(2,6-dichlorophenyl)propan-2-one
Conditions | Yield |
---|---|
Stage #1: thionyl chloride; 2-(2,6-dichlorophenyl)acetic acid With diazomethyl-trimethyl-silane Stage #2: With hydrogen bromide In water | 100% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With borane-d3 In tetrahydrofuran at 0 - 20℃; for 20h; | 99% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole In tetrahydrofuran | 98% |
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 25℃; for 1h; Stage #2: 4-[(1S,3R)-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol In tetrahydrofuran at 45℃; for 24h; Reagent/catalyst; | 376 g |
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 25℃; for 1h; Stage #2: 4-[(1S,3R)-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol In tetrahydrofuran at 25 - 45℃; for 24h; | 376 g |
With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole In tetrahydrofuran at 40℃; for 72h; Inert atmosphere; | 250 mg |
2-(2,6-dichlorophenyl)acetic acid
2-(2,6-dichlorophenyl)ethan-1-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 12h; Heating; | 97% |
With lithium aluminium tetrahydride In diethyl ether for 16h; Heating / reflux; | 85% |
With borane In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 73% |
With lithium aluminium tetrahydride In diethyl ether | |
With borane In tetrahydrofuran |
endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide | 97% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With deuteriated sodium hydroxide; tetrabutylammomium bromide In water-d2 at 105℃; for 40h; | 97% |
methanol
2-(2,6-dichlorophenyl)acetic acid
methyl 2-(2,6-dichlorophenyl)acetate
Conditions | Yield |
---|---|
With sulfuric acid | 96% |
With hydrogenchloride Reflux; | 92% |
With thionyl chloride at 0℃; Reflux; | 10 g |
With sulfuric acid for 8h; Reflux; |
2-(2,6-dichlorophenyl)acetic acid
ethyl 4-(piperazin-1-yl)benzoate
C21H22Cl2N2O3
Conditions | Yield |
---|---|
With diethyl cyanophosphonate; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; | 95% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
Stage #1: 2-(2,6-dichlorophenyl)acetic acid; (1S,3R)-5-bromo-3-(((tertbutyldiphenylsilyl) oxy)methyl)-1-methyl-1,2,3,4-tetrahydroisoquinoline With trimethylamine In acetonitrile for 0.0833333h; Stage #2: With propylphosphonic anhydride In ethyl acetate; acetonitrile at 5 - 20℃; for 1.25h; | 93% |
2-(2,6-dichlorophenyl)acetic acid
2-(2,6-dichlorophenyl)acetohydrazide
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole; hydrazine In tetrahydrofuran | 92% |
With 1,1'-carbonyldiimidazole; hydrazine In tetrahydrofuran | 92% |
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran Stage #2: With hydrazine In tetrahydrofuran Further stages.; |
2-(2,6-dichlorophenyl)acetic acid
1,2-diamino-benzene
2-(2,6-dichlorobenzyl)-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
With polyphosphoric acid at 175℃; for 4h; Inert atmosphere; | 92% |
With polyphosphoric acid for 4h; Inert atmosphere; Heating; | 92% |
2-(2,6-dichlorophenyl)acetic acid
4-Chloro-1,2-phenylenediamine
5-chloro-2-(2,6-dichlorobenzyl)-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
With polyphosphoric acid for 4h; Inert atmosphere; Heating; | 92% |
Conditions | Yield |
---|---|
With 1H-imidazole; C17H16ClMnN2O2; tetrabutylammonium periodite In chloroform at 20℃; for 0.666667h; | 90% |
With 1H-imidazole; [bis(acetoxy)iodo]benzene; Co(AAOPD) In acetonitrile at 20℃; for 6.33333h; | 89% |
With mercury(II) fluoride; oxygen In acetonitrile at 25℃; for 24h; Irradiation; | 76% |
With oxygen; mercury(II) oxide In methanol; acetonitrile at 25℃; UV-irradiation; | 64% |
With dihydrogen peroxide In water; acetonitrile at 25℃; for 10h; UV-irradiation; | 12.5 %Chromat. |
2-(2,6-dichlorophenyl)acetic acid
2,6-Dichlorobenzyl bromide
Conditions | Yield |
---|---|
With silver triflate-bis(1,10-phenanthroline) complex; dibromoisocyanuric acid In 1,2-dichloro-ethane at 20℃; for 22h; Inert atmosphere; Schlenk technique; | 88% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine In dichloromethane at 20℃; | 86% |
Conditions | Yield |
---|---|
With tert-butylhypochlorite; silver triflate-bis(1,10-phenanthroline) complex In acetonitrile at 20℃; for 26h; Inert atmosphere; | 85% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
Stage #1: 4-[(1S,3R)-3-(hydroxymethyl)-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine In acetonitrile at 0℃; for 0.5h; Stage #2: 2-(2,6-dichlorophenyl)acetic acid In acetonitrile at 0℃; for 1h; | 85% |
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine In acetonitrile at 0℃; for 1h; Stage #2: 4-[(1S,3R)-3-(hydroxymethyl)-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol With potassium carbonate In water; acetonitrile at 0℃; for 4h; Solvent; | 85% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In tetrahydrofuran; ethyl acetate at 20℃; for 2h; Alkaline conditions; | 85% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In dichloromethane for 2h; | 84% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide | 83% |
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; | 55% |
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; | 4.70 g |
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; | 4.7 g |
2-(2,6-dichlorophenyl)acetic acid
2-(3,4-dimethoxyphenyl)-ethylamine
2-(2,6-dichloro-phenyl)-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 6h; Condensation; Heating; | 82% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere; | 81% |
2-(2,6-dichlorophenyl)acetic acid
benzylamine
1-benzyl-4-chloro-1,3-dihydroindol-2-one
Conditions | Yield |
---|---|
Stage #1: 2-(2,6-dichlorophenyl)acetic acid; benzylamine at 150℃; for 0.5h; microwave irradiation; Stage #2: With sodium hydroxide; XPhos; palladium diacetate In water; toluene at 100℃; for 0.5h; microwave irradiation; | 80% |
2-(2,6-dichlorophenyl)acetic acid
β-(3-chlorobenzyl)mercaptoethylamine
N-[2-(3-chlorobenzylsulfanyl)ethyl]-2-(2,6-dichlorophenyl)acetamide
Conditions | Yield |
---|---|
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With dicyclohexyl-carbodiimide In dichloromethane for 0.5h; Inert atmosphere; Stage #2: β-(3-chlorobenzyl)mercaptoethylamine With triethylamine In dichloromethane at 20℃; for 1h; Inert atmosphere; | 80% |
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With dicyclohexyl-carbodiimide In dichloromethane for 0.5h; Inert atmosphere; Stage #2: β-(3-chlorobenzyl)mercaptoethylamine With triethylamine In dichloromethane at 20℃; for 1h; Inert atmosphere; | 80% |
2-(2,6-dichlorophenyl)acetic acid
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; | 78% |
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