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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

2,6-Dichlorophenylacetic acid Manufacturer/High quality/Best price/In stock

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2,6-Dichlorophenylacetic Acid supplier in China

Cas:6575-24-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product description: Product name 2,6-Dichlorophenylacetic acid CAS number 6575-24-2 Assay ≥99% Appearance White solid Capacity 200mt/year Application Organic synthesis inter

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2,6-dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

Type:Trading Company

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The packag

2,6-Dichlorophenylacetic acid CAS:6575-24-2

Cas:6575-24-2

Min.Order:1 Gram

FOB Price: $15.0 / 25.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 6575-24-2 with best price

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzeneaceticacid, 2,6-dichloro- 6575-24-2

Cas:6575-24-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

2,6-Dichlorophenylacetic acid CAS:6575-24-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org

2,6-Dichlorophenylacetic acid CAS:6575-24-2

Cas:6575-24-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benzeneaceticacid, 2,6-dichloro-

Cas:6575-24-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

Benzeneaceticacid, 2,6-dichloro-/ LIDE PHARMA- Factory supply / Best price

Cas:6575-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:6575-24-2

Cas:6575-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Mojin Biotechnology Co.,Ltd

Product quality: Our company have high quality product , and also the product we have good manufacture . First of all, this product is of fine quality. Every finish should be checked by quality inspection system.And every one should be also tried

2, 6-Dichlorophenylacetic Acid CAS 6575-24-2

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $20.0 / 30.0

Type:Trading Company

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $10.0 / 100.0

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2,6-Dichlorophenylacetic Acid

Cas:6575-24-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and quality c

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Benzeneaceticacid, 2,6-dichloro-

Cas:6575-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Newgreat Chemical Co., Ltd

ProName:2,6-Dichlorophenylacetic acid CasNo:6575-24-2 Molecular Formula:C8H6Cl2O2 Appearance:White solid Application:Organic synthesis intermediate DeliveryTime:Immediately PackAge:25kg/drum Port:Shanghai or Qingdao ProductionCapacity:200 M

2,6-Dichlorophenylacetic acid 6575-24-2

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2,6-Dichlorophenylacetic Acid

Cas:6575-24-2

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

2,6-Dichlorophenylacetic acidAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:Steroids, Cosmetics Ingredients, APIs, Intermediates,

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

6575-24-2 2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

2,6-Dichlorophenylacetic acid Basic information Product Name: 2,6-Dichlorophenylacetic acid Synonyms: 2-(2,6-DICHLOROPHENYL)ACETIC ACID;2,6-DICHLORO BENZENEACETIC ACID;2,6-DICHLOROPHENYLACETIC ACID;RARECHEM AL BO 0115;TIMTEC-BB SBB003503;2,6-D

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

2,6-Dichlorophenylacetic acid

Cas:6575-24-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

2,2,6,6-tetrachlorocyclohexanone
3776-30-5

2,2,6,6-tetrachlorocyclohexanone

diethyl malonate
105-53-3

diethyl malonate

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
Stage #1: 2,2,6,6-tetrachlorocyclohexanone; diethyl malonate With 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,2-dichloro-ethane at 60 - 65℃; for 3h;
Stage #2: With sodium hydroxide In 1,2-dichloro-ethane at 20 - 65℃; for 3h; Solvent; Temperature; Reagent/catalyst;
96.6%
ethyl 2-(2,6-dichlorophenyl)acetate
90793-64-9

ethyl 2-(2,6-dichlorophenyl)acetate

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
With water; sodium hydroxide In 1,4-dioxane at 60℃; for 2h; pH=10 - 14;95%
carbon monoxide
201230-82-2

carbon monoxide

1,3-Dichloro-2-chloromethyl-benzene
2014-83-7

1,3-Dichloro-2-chloromethyl-benzene

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; tetraethylammonium chloride; sodium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene at 80℃; under 11251.1 Torr; for 20h; Autoclave; regioselective reaction;93%
2,6-dichlorophenylacetonitrile
3215-64-3

2,6-dichlorophenylacetonitrile

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
Stage #1: 2,6-dichlorophenylacetonitrile With potassium hydroxide; water In ethanol at 80℃; for 20h;
Stage #2: With hydrogenchloride In ethanol pH=3;
83%
With sodium hydroxide
With potassium hydroxide In ethylene glycol
etheric 2.6-dichloro-benzyl magnesium chloride

etheric 2.6-dichloro-benzyl magnesium chloride

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
Einleiten von Kohlendioxid;
carbon dioxide
124-38-9

carbon dioxide

2,6-dichlorotoluene
118-69-4

2,6-dichlorotoluene

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
Stage #1: 2,6-dichlorotoluene With lithium diisopropyl amide In tetrahydrofuran; cyclohexane at -75℃; for 0.75h;
Stage #2: carbon dioxide In tetrahydrofuran; cyclohexane
carbon dioxide
124-38-9

carbon dioxide

2,6-dichlorotoluene
118-69-4

2,6-dichlorotoluene

A

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

B

3,5-dichloro-4-methylbenzoic acid
39652-34-1

3,5-dichloro-4-methylbenzoic acid

C

2,4-Dichloro-3-methyl-benzoic acid
83277-23-0

2,4-Dichloro-3-methyl-benzoic acid

Conditions
ConditionsYield
Stage #1: 2,6-dichlorotoluene With sec.-butyllithium In tetrahydrofuran; cyclohexane at -75℃; for 0.75h;
Stage #2: carbon dioxide In tetrahydrofuran; cyclohexane Title compound not separated from byproducts;
1,3-Dichloro-2-chloromethyl-benzene
2014-83-7

1,3-Dichloro-2-chloromethyl-benzene

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dimethylsulfoxide / 5 h / 40 - 50 °C
2: 25 percent NaOH / ethanol / Heating
View Scheme
Multi-step reaction with 2 steps
2: aqueous NaOH
View Scheme
Multi-step reaction with 2 steps
2: H2SO4
View Scheme
2,6-dichlorotoluene
118-69-4

2,6-dichlorotoluene

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dichloro[4,5-bis(diphenylphosphino)-9,9’-dimethylxanthene]palladium(II); di-tert-butyl peroxide / 16 h / 120 °C / 7600.51 Torr
2: water; sodium hydroxide / 1,4-dioxane / 2 h / 60 °C / pH 10 - 14
View Scheme
2,6-Dichloroaniline
608-31-1

2,6-Dichloroaniline

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium nitrite; sulfuric acid; copper(I) bromide; tetrabutylammomium bromide / water / 2 h / -5 - 95 °C
2: hydrogenchloride / 10 h / 80 - 95 °C / Inert atmosphere
View Scheme
1-(2,2,2-trichloroethyl)-2,6-dichlorobenzene
30359-34-3

1-(2,2,2-trichloroethyl)-2,6-dichlorobenzene

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

Conditions
ConditionsYield
With hydrogenchloride at 80 - 95℃; for 10h; Inert atmosphere;115.3 g
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2,6-dichlorophenylacetylchloride
61875-53-4

2,6-dichlorophenylacetylchloride

Conditions
ConditionsYield
With thionyl chloride In toluene at 20℃; for 12h;100%
With thionyl chloride at 80℃; for 1h;90%
With thionyl chloride
thionyl chloride
7719-09-7

thionyl chloride

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

1-bromo-3-(2,6-dichlorophenyl)propan-2-one
880089-70-3

1-bromo-3-(2,6-dichlorophenyl)propan-2-one

Conditions
ConditionsYield
Stage #1: thionyl chloride; 2-(2,6-dichlorophenyl)acetic acid With diazomethyl-trimethyl-silane
Stage #2: With hydrogen bromide In water
100%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2-(2,6-dichlorophenyl)(1,1-2H2)ethan-1-ol

2-(2,6-dichlorophenyl)(1,1-2H2)ethan-1-ol

Conditions
ConditionsYield
With borane-d3 In tetrahydrofuran at 0 - 20℃; for 20h;99%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

4-[(1S,3R)-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol

4-[(1S,3R)-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol

1-[(1S,3R)-3-({[tert-butyl(dimethyl)silyl]oxy}methyl)-5-(3-hydroxy-3-methylbutyl)-1-methyl-3,4-dihydroisoquinolin-2(1H)-yl]-2-(2,6-dichlorophenyl)ethanone

1-[(1S,3R)-3-({[tert-butyl(dimethyl)silyl]oxy}methyl)-5-(3-hydroxy-3-methylbutyl)-1-methyl-3,4-dihydroisoquinolin-2(1H)-yl]-2-(2,6-dichlorophenyl)ethanone

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole In tetrahydrofuran98%
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 25℃; for 1h;
Stage #2: 4-[(1S,3R)-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol In tetrahydrofuran at 45℃; for 24h; Reagent/catalyst;
376 g
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 25℃; for 1h;
Stage #2: 4-[(1S,3R)-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol In tetrahydrofuran at 25 - 45℃; for 24h;
376 g
With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole In tetrahydrofuran at 40℃; for 72h; Inert atmosphere;250 mg
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2-(2,6-dichlorophenyl)ethan-1-ol
30595-79-0

2-(2,6-dichlorophenyl)ethan-1-ol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether for 12h; Heating;97%
With lithium aluminium tetrahydride In diethyl ether for 16h; Heating / reflux;85%
With borane In tetrahydrofuran at 0 - 20℃; Inert atmosphere;73%
With lithium aluminium tetrahydride In diethyl ether
With borane In tetrahydrofuran
endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide
21715-90-2

endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2,6-Dichloro-benzoic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl ester

2,6-Dichloro-benzoic acid (1R,2S,6R,7S)-3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide97%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2-(2,6-dichlorophenyl)(2H2)acetic acid

2-(2,6-dichlorophenyl)(2H2)acetic acid

Conditions
ConditionsYield
With deuteriated sodium hydroxide; tetrabutylammomium bromide In water-d2 at 105℃; for 40h;97%
methanol
67-56-1

methanol

2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

methyl 2-(2,6-dichlorophenyl)acetate
54551-83-6

methyl 2-(2,6-dichlorophenyl)acetate

Conditions
ConditionsYield
With sulfuric acid96%
With hydrogenchloride Reflux;92%
With thionyl chloride at 0℃; Reflux;10 g
With sulfuric acid for 8h; Reflux;
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

ethyl 4-(piperazin-1-yl)benzoate
80518-57-6

ethyl 4-(piperazin-1-yl)benzoate

C21H22Cl2N2O3
1092069-59-4

C21H22Cl2N2O3

Conditions
ConditionsYield
With diethyl cyanophosphonate; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃;95%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

(1S,3R)-5-bromo-3-(((tertbutyldiphenylsilyl) oxy)methyl)-1-methyl-1,2,3,4-tetrahydroisoquinoline

(1S,3R)-5-bromo-3-(((tertbutyldiphenylsilyl) oxy)methyl)-1-methyl-1,2,3,4-tetrahydroisoquinoline

1-[(1S,3R)-5-bromo-3-[[tert-butyl(diphenyl)silyl]oxymethyl]-1-methyl-3,4-dihydro-1H-isoquinolin-2-yl]-2-(2,6-dichlorophenyl)ethanone

1-[(1S,3R)-5-bromo-3-[[tert-butyl(diphenyl)silyl]oxymethyl]-1-methyl-3,4-dihydro-1H-isoquinolin-2-yl]-2-(2,6-dichlorophenyl)ethanone

Conditions
ConditionsYield
Stage #1: 2-(2,6-dichlorophenyl)acetic acid; (1S,3R)-5-bromo-3-(((tertbutyldiphenylsilyl) oxy)methyl)-1-methyl-1,2,3,4-tetrahydroisoquinoline With trimethylamine In acetonitrile for 0.0833333h;
Stage #2: With propylphosphonic anhydride In ethyl acetate; acetonitrile at 5 - 20℃; for 1.25h;
93%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2-(2,6-dichlorophenyl)acetohydrazide
129564-34-7

2-(2,6-dichlorophenyl)acetohydrazide

Conditions
ConditionsYield
With 1,1'-carbonyldiimidazole; hydrazine In tetrahydrofuran92%
With 1,1'-carbonyldiimidazole; hydrazine In tetrahydrofuran92%
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran
Stage #2: With hydrazine In tetrahydrofuran Further stages.;
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

2-(2,6-dichlorobenzyl)-1H-benzo[d]imidazole
743451-08-3

2-(2,6-dichlorobenzyl)-1H-benzo[d]imidazole

Conditions
ConditionsYield
With polyphosphoric acid at 175℃; for 4h; Inert atmosphere;92%
With polyphosphoric acid for 4h; Inert atmosphere; Heating;92%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

4-Chloro-1,2-phenylenediamine
95-83-0

4-Chloro-1,2-phenylenediamine

5-chloro-2-(2,6-dichlorobenzyl)-1H-benzo[d]imidazole
1274937-60-8

5-chloro-2-(2,6-dichlorobenzyl)-1H-benzo[d]imidazole

Conditions
ConditionsYield
With polyphosphoric acid for 4h; Inert atmosphere; Heating;92%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2,6-dichlorobenzaldehyde
83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With 1H-imidazole; C17H16ClMnN2O2; tetrabutylammonium periodite In chloroform at 20℃; for 0.666667h;90%
With 1H-imidazole; [bis(acetoxy)iodo]benzene; Co(AAOPD) In acetonitrile at 20℃; for 6.33333h;89%
With mercury(II) fluoride; oxygen In acetonitrile at 25℃; for 24h; Irradiation;76%
With oxygen; mercury(II) oxide In methanol; acetonitrile at 25℃; UV-irradiation;64%
With dihydrogen peroxide In water; acetonitrile at 25℃; for 10h; UV-irradiation;12.5 %Chromat.
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2,6-Dichlorobenzyl bromide
20443-98-5

2,6-Dichlorobenzyl bromide

Conditions
ConditionsYield
With silver triflate-bis(1,10-phenanthroline) complex; dibromoisocyanuric acid In 1,2-dichloro-ethane at 20℃; for 22h; Inert atmosphere; Schlenk technique;88%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

(1S)-5-bromo-1-methyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

(1S)-5-bromo-1-methyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

1-[(1S)-5-bromo-1-methyl-3,4-dihydroisoquinolin-2(1H)-yl]-2-(2,6-dichlorophenyl)ethanone

1-[(1S)-5-bromo-1-methyl-3,4-dihydroisoquinolin-2(1H)-yl]-2-(2,6-dichlorophenyl)ethanone

Conditions
ConditionsYield
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine In dichloromethane at 20℃;86%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

1,3-Dichloro-2-chloromethyl-benzene
2014-83-7

1,3-Dichloro-2-chloromethyl-benzene

Conditions
ConditionsYield
With tert-butylhypochlorite; silver triflate-bis(1,10-phenanthroline) complex In acetonitrile at 20℃; for 26h; Inert atmosphere;85%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

4-[(1S,3R)-3-(hydroxymethyl)-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol

4-[(1S,3R)-3-(hydroxymethyl)-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol

2-(2,6-dichlorophenyl)-1-((1S,3R)-5-(3-hydroxy-3-methylbutyl)-3-(hydroxymethyl)-1-methyl-3,4-dihydroisoquinolin-2(1H)-yl)ethan-1-one

2-(2,6-dichlorophenyl)-1-((1S,3R)-5-(3-hydroxy-3-methylbutyl)-3-(hydroxymethyl)-1-methyl-3,4-dihydroisoquinolin-2(1H)-yl)ethan-1-one

Conditions
ConditionsYield
Stage #1: 4-[(1S,3R)-3-(hydroxymethyl)-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine In acetonitrile at 0℃; for 0.5h;
Stage #2: 2-(2,6-dichlorophenyl)acetic acid In acetonitrile at 0℃; for 1h;
85%
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine In acetonitrile at 0℃; for 1h;
Stage #2: 4-[(1S,3R)-3-(hydroxymethyl)-1-methyl-1,2,3,4-tetrahydroisoquinolin-5-yl]-2-methyl-butan-2-ol With potassium carbonate In water; acetonitrile at 0℃; for 4h; Solvent;
85%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2-fluoro-6-[(4,6-dimethoxy-1,3,5-triazin-2-yl)methyl]benzenamine

2-fluoro-6-[(4,6-dimethoxy-1,3,5-triazin-2-yl)methyl]benzenamine

2-(2,6-dichlorophenyl)-N-{2-fluoro-6-[(4,6-dimethoxy-1,3,5-triazin-2-yl)methyl]phenyl}acetamide

2-(2,6-dichlorophenyl)-N-{2-fluoro-6-[(4,6-dimethoxy-1,3,5-triazin-2-yl)methyl]phenyl}acetamide

Conditions
ConditionsYield
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In tetrahydrofuran; ethyl acetate at 20℃; for 2h; Alkaline conditions;85%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

(1S,3R)-3-(((tert-butyldimethylsilyl)oxy)methyl)-1-methyl-5-(1-(oxetan-3-yl)-1H-pyrazol-4-yl)-1,2,3,4-tetrahydroisoquinoline

(1S,3R)-3-(((tert-butyldimethylsilyl)oxy)methyl)-1-methyl-5-(1-(oxetan-3-yl)-1H-pyrazol-4-yl)-1,2,3,4-tetrahydroisoquinoline

1-((1S,3R)-3-(((tert-butyldimethylsilyl)oxy)methyl)-1-methyl-5-(1-(oxetan-3-yl)-1H-pyrazol-4-yl)-3,4-dihydroisoquinolin-2(1H)-yl)-2-(2,6-dichlorophenyl)ethan-1-one

1-((1S,3R)-3-(((tert-butyldimethylsilyl)oxy)methyl)-1-methyl-5-(1-(oxetan-3-yl)-1H-pyrazol-4-yl)-3,4-dihydroisoquinolin-2(1H)-yl)-2-(2,6-dichlorophenyl)ethan-1-one

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; HATU In dichloromethane for 2h;84%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

(1S,3R)-5-bromo-3-(([tert-butyl(dimethyl)silyl]oxy)methyl)-1-methyl-1,2,3,4-tetrahydroisoquinoline

(1S,3R)-5-bromo-3-(([tert-butyl(dimethyl)silyl]oxy)methyl)-1-methyl-1,2,3,4-tetrahydroisoquinoline

1-[(1S,3R)-5-bromo-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-3,4-dihydro-1H-isoquinolin-2-yl]-2-(2,6-dichlorophenyl)ethan-1-one

1-[(1S,3R)-5-bromo-3-[[tert-butyl(dimethyl)silyl]oxymethyl]-1-methyl-3,4-dihydro-1H-isoquinolin-2-yl]-2-(2,6-dichlorophenyl)ethan-1-one

Conditions
ConditionsYield
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide83%
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;55%
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;4.70 g
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;4.7 g
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

2-(2,6-dichloro-phenyl)-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide
318294-29-0

2-(2,6-dichloro-phenyl)-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 6h; Condensation; Heating;82%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

4-amino-N-(4-methoxycyclohexyl)-1H-pyrazole-3-carboxamide

4-amino-N-(4-methoxycyclohexyl)-1H-pyrazole-3-carboxamide

4-(2-(2,6-dichlorophenyl)acetamido)-N-(4-methoxycyclohexyl)-1H-pyrazole-3-carboxamide

4-(2-(2,6-dichlorophenyl)acetamido)-N-(4-methoxycyclohexyl)-1H-pyrazole-3-carboxamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere;81%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

benzylamine
100-46-9

benzylamine

1-benzyl-4-chloro-1,3-dihydroindol-2-one
849098-26-6

1-benzyl-4-chloro-1,3-dihydroindol-2-one

Conditions
ConditionsYield
Stage #1: 2-(2,6-dichlorophenyl)acetic acid; benzylamine at 150℃; for 0.5h; microwave irradiation;
Stage #2: With sodium hydroxide; XPhos; palladium diacetate In water; toluene at 100℃; for 0.5h; microwave irradiation;
80%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

β-(3-chlorobenzyl)mercaptoethylamine
106670-33-1

β-(3-chlorobenzyl)mercaptoethylamine

N-[2-(3-chlorobenzylsulfanyl)ethyl]-2-(2,6-dichlorophenyl)acetamide
1234381-00-0

N-[2-(3-chlorobenzylsulfanyl)ethyl]-2-(2,6-dichlorophenyl)acetamide

Conditions
ConditionsYield
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With dicyclohexyl-carbodiimide In dichloromethane for 0.5h; Inert atmosphere;
Stage #2: β-(3-chlorobenzyl)mercaptoethylamine With triethylamine In dichloromethane at 20℃; for 1h; Inert atmosphere;
80%
Stage #1: 2-(2,6-dichlorophenyl)acetic acid With dicyclohexyl-carbodiimide In dichloromethane for 0.5h; Inert atmosphere;
Stage #2: β-(3-chlorobenzyl)mercaptoethylamine With triethylamine In dichloromethane at 20℃; for 1h; Inert atmosphere;
80%
2-(2,6-dichlorophenyl)acetic acid
6575-24-2

2-(2,6-dichlorophenyl)acetic acid

4-(4-aminobenzyl)-5-(dibromomethylene)furan-2(5H)-one

4-(4-aminobenzyl)-5-(dibromomethylene)furan-2(5H)-one

N-(4-((2-(dibromomethylene)-5-oxo-2,5-dihydrofuran-3-yl)methyl)phenyl)-2-(2,6-dichlorophenyl)acetamide

N-(4-((2-(dibromomethylene)-5-oxo-2,5-dihydrofuran-3-yl)methyl)phenyl)-2-(2,6-dichlorophenyl)acetamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 0 - 20℃;78%
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