Specification: CAS Number 608-31-1 Product Name 2,6-dichloroaniline Synonyms 2,6-dichlorobenzenamine; 2,6-dichlorobenzenamine Molecular Formula
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:608-31-1
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:608-31-1
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inquiryProduct description: Product name 2,6-Dichloroaniline CAS number 608-31-1 Assay ≥99% Appearance White crystal Capacity 200mt/year Application Pharmaceutical/pesticide/dye int
Cas:608-31-1
Min.Order:100 Gram
FOB Price: $12.0
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:608-31-1
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:608-31-1
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inquiry2,6-Dichloroaniline Basic information Product Name: 2,6-Dichloroaniline Synonyms: 2,6-dichloro;2,6-DICHLOROANILINE;2,6-Dichlorobenzenamine;2,6 DICHLORANILINE;AURORA KA-687;2,5-DICHLOROBE
Cas:608-31-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryCAS Number 608-31-1 Product Name 2,6-dichloroaniline Synonyms 2,6-dichlorobenzenamine; 2,6-dichlorobenzenamine
2,6-Dichloroaniline CAS: 608-31-1 Specification Product name 2,6-Dichloroaniline CAS number 608-31-1 Assay ≥99% Appearance White crystal Capacity 200mt/year Application Phar
Product Detail Minimum Order Qty. 10 Gram
Cas:608-31-1
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryProduct Name: 2,6-Dichloroaniline Synonyms: 1-aMino-2,6-dichlorobenzene;Clonidine IMpurity-C(BP);2,6- twochloro aniline;2.6-Dichloroan;Clonidine Impurity C (2,6-Dichloroaniline);6-Dichlorobenzenamine;2,6-dichloro;2,6-DICHLOROANILINE CAS: 608-3
Cas:608-31-1
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:608-31-1
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:608-31-1
Min.Order:1 Gram
FOB Price: $1.0
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:608-31-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white or light yellow powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:608-31-1
Min.Order:1 Metric Ton
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inquiryHANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in
Cas:608-31-1
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inquiryCapability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:608-31-1
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers456.Safe and fa
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:608-31-1
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:608-31-1
Min.Order:0
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Type:Lab/Research institutions
inquiry4-amino-3,5-dichloro-benzenesulfonamide
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With sulfuric acid at 180℃; | 96.2% |
Conditions | Yield |
---|---|
With ammonium formate at 20℃; for 0.75h; Reduction; | 91% |
With hydrogenchloride; tin | |
With hydrogen; silver; silica gel In ethanol at 140℃; under 15001.2 Torr; for 3h; | 100 % Chromat. |
Conditions | Yield |
---|---|
With methanol; gold; hydrogen; caesium carbonate at 100℃; under 3800.26 Torr; for 72h; | 91% |
With hydrogen bromide; acetic acid; aniline for 24h; Heating; | 86% |
With hydrogen bromide; acetic acid; aniline Reflux; | 80% |
4-amino-3,5-dichlorobenzoic acid
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With copper(I) oxide In quinoline at 220℃; for 6h; Autoclave; | 85% |
In water | 80% |
N-(2,6-dichlorophenyl)benzamide
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With sulfuric acid for 3h; Heating; | 68% |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide; Chloroacetamide In N,N-dimethyl-formamide at 90 - 150℃; for 4h; Reagent/catalyst; Smiles Aromatic Rearrangement; | 65% |
Conditions | Yield |
---|---|
With chlorine In chlorobenzene at 15℃; for 6h; Solvent; Reagent/catalyst; Temperature; | A 60% B 35% |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium permanganate In acetonitrile at 60℃; | A 19% B 29% |
Conditions | Yield |
---|---|
With carbon dioxide; water; chlorine Behandeln des Reaktionsprodukts mit 98 prozentiger Schwefelsaeure und Dampf bei 180grad; |
tert-butyl (2,6-dichlorophenyl)carbamate
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol |
N,N-diacetyl-2,6-dichloroaniline
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With hydrogenchloride In acetic acid for 1h; Heating; |
5-(2,6-dichlorophenyl)-1-phenyl-1H-1,2,5-triazapentadiene
A
5-chloro-quinoxaline
B
2,6-Dichloroaniline
Conditions | Yield |
---|---|
at 600℃; under 0.01 Torr; for 0.416667h; Title compound not separated from byproducts; | A 13 % Chromat. B 37 % Chromat. |
aniline
A
2,4-Dichloroaniline
B
4-chloro-aniline
C
2-Chloroaniline
D
2,6-Dichloroaniline
E
2,4,6-trichloroaniline
Conditions | Yield |
---|---|
With hydrogenchloride; calcium hypochlorite; ammonia In water pH=1.3; other concentration of chlorinating agent; other pH; |
2,4,6-trichloroaniline
A
2,4-Dichloroaniline
B
4-chloro-aniline
C
aniline
D
2-Chloroaniline
E
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With ammonium formate; palladium on activated charcoal In acetonitrile at 80℃; for 2h; Product distribution; other haloanilines; other H-donors; var. solvents, temperatures, reaction times; |
2-chloro-N-hydroxybenzenamine
A
4-amino-3-chlorophenol
B
2,4-Dichloroaniline
C
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With perchloric acid; sodium perchlorate; sodium chloride In water; acetonitrile at 25℃; Rate constant; |
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 100℃; for 5h; Dehydrochlorination; | 2.32 g |
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With sulfuric acid Darstellung; Destillation mit Dampf; |
Conditions | Yield |
---|---|
Behandeln mit Kalilauge; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaClO3; HCl 2: 86 percent / HBr; AcOH; aniline / 24 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 5.74 g / NH3; TiCl4 / toluene / 2 h / -1 - 10 °C 2: 2.32 g / (CH3CH2)3N / dimethylformamide / 5 h / 100 °C View Scheme |
2,4,6-trichloro-diacetanilide
2,6-Dichloroaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 65 percent / sodium formate / 5percent Pd/C / acetonitrile / 24 h / Heating 2: conc. HCl / acetic acid / 1 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: HCl(gas), Cl2 / CCl4; ethanol / ice-bath 2: 96 percent / CH3SO3H / Heating 3: 65 percent / sodium formate / 5percent Pd/C / acetonitrile / 24 h / Heating 4: conc. HCl / acetic acid / 1 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 96 percent / CH3SO3H / Heating 2: 65 percent / sodium formate / 5percent Pd/C / acetonitrile / 24 h / Heating 3: conc. HCl / acetic acid / 1 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 96 percent / conc.HCl, perhydrol / H2O 2: 96.2 percent / 70 percent H2SO4 / 180 °C View Scheme |
2-chloro-N-hydroxybenzenamine
2,6-Dichloroaniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaHCO3 / diethyl ether; H2O / 1 h / T < 5 deg C; or in benzene 2: 77 percent / SOCl2 / diethyl ether / 1 h / T < 5 deg C 3: 68 percent / 70percent H2SO4 / 3 h / Heating View Scheme |
N-(o-chlorophenyl)benzohydroxamic acid
2,6-Dichloroaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 77 percent / SOCl2 / diethyl ether / 1 h / T < 5 deg C 2: 68 percent / 70percent H2SO4 / 3 h / Heating View Scheme |
2,4-dichloro-3-nitroaniline
2,6-Dichloroaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: tin; hydrochloric acid View Scheme |
trimethylacetic formic anhydride
2,6-Dichloroaniline
N-(2,6-dichlorophenyl)-formamide
Conditions | Yield |
---|---|
In chloroform at 25℃; | 100% |
acetic acid
acetyl chloride
2,6-Dichloroaniline
2,6-dichloroacetanilide
Conditions | Yield |
---|---|
at 90℃; for 0.333333h; | 100% |
2,6-Dichloroaniline
Conditions | Yield |
---|---|
In dichlorometane at 45℃; | 99.9% |
Benzoyl isothiocyanate
2,6-Dichloroaniline
N-(2,6-dichlorophenyl)-N'-benzoyl thiourea
Conditions | Yield |
---|---|
In acetone for 0.5h; Heating; | 99% |
In tetrahydrofuran at 60 - 65℃; for 0.166667h; Microwave irradiation; | 89% |
In benzene | 82% |
In ethyl acetate for 2h; Reflux; | |
In acetone at 60℃; for 0.5h; |
potassium isopropylxanthate
2,6-Dichloroaniline
4-chloro-2-mercaptobenzothiazole
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide at 150℃; for 0.0833333h; Solvent; Temperature; Microwave irradiation; | 99% |
acetic anhydride
2,6-Dichloroaniline
1-(4-amino-3,5-dichlorophenyl)-1-ethanone
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; | 98.9% |
Conditions | Yield |
---|---|
With pyridine; calcium chloride for 4h; Reagent/catalyst; Reflux; Cooling with ice; | 98.3% |
With pyridine for 4h; Reagent/catalyst; Cooling with ice; Reflux; | 98.3% |
2-Iodo-N,N-dimethylbenzamide
2,6-Dichloroaniline
2-(2,6-dichloro-phenylamino)-N,N-dimethyl-benzamide
Conditions | Yield |
---|---|
With copper(l) iodide; copper; potassium carbonate In xylene Condensation; Heating; | 98% |
2,6-Dichloroaniline
4-methyl-3-nitrobenzoyl chloride
Conditions | Yield |
---|---|
at 130℃; for 0.25h; Inert atmosphere; Microwave irradiation; | 98% |
Ethoxycarbonyl isothiocyanate
2,6-Dichloroaniline
ethyl 3-(2,6-dichlorophenyl)thioureidocarboxylate
Conditions | Yield |
---|---|
In acetone at 20 - 40℃; for 12.33h; | 98% |
Conditions | Yield |
---|---|
With supported L-pyrrolidine-2-carboxylic acid-4-hydrogen sulfate on Silica Gel at 20℃; for 1.2h; Green chemistry; | 97% |
With acetic acid; zinc for 0.5h; Ambient temperature; | 50% |
With dmap In dichloromethane at 0 - 40℃; | 47.64% |
With pyridine for 2h; Heating; | |
With sulfuric acid |
2,6-Dichloroaniline
1-azido-2,6-dichlorobenzene
Conditions | Yield |
---|---|
Stage #1: 2,6-Dichloroaniline With trifluoroacetic acid; sodium nitrite In water at 0℃; for 0.5h; Stage #2: With sodium azide In water at 0 - 20℃; for 2.16667h; | 97% |
Stage #1: 2,6-Dichloroaniline With trifluoroacetic acid; sodium nitrite In water at 0℃; for 0.5h; Stage #2: With sodium azide In water at 0℃; for 2.16667h; | 97% |
With sodium azide; trifluoroacetic acid; sodium nitrite In water at 0 - 20℃; for 2.16667h; | 97% |
2,6-Dichloroaniline
Conditions | Yield |
---|---|
With phosphorus pentachloride In chloroform for 22h; Heating; | 97% |
With phosphorus pentachloride In tetrachloromethane Substitution; Heating; |
2,6-Dichloroaniline
2,6-dichloro-N-trimethylsilylaniline
Conditions | Yield |
---|---|
With trimethylsilyl bromide; triethylamine In benzene | 97% |
methyl (2-iodophenyl)acetate
2,6-Dichloroaniline
2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester
Conditions | Yield |
---|---|
With copper(l) iodide; (+)-D-glucosamine hydrochloride; caesium carbonate In water; dimethyl sulfoxide at 110℃; for 8h; Temperature; | 96.1% |
Conditions | Yield |
---|---|
In acetic acid | 96% |
In acetic acid at 70℃; for 0.5h; | 78% |
With acetic acid | |
With acetic acid at 100℃; |
Conditions | Yield |
---|---|
In toluene ligand was added to toluene soln. of V(NMe2)4 at room temp., Me3SiCl wasadded at room temp. under Ar, heated at 100°C for 20 h; volatiles were pumped off, washed with pentane, dried under vac.; elem. anal.; | 96% |
Conditions | Yield |
---|---|
Stage #1: 2,6-Dichloroaniline With n-butyllithium In tetrahydrofuran; hexane at -78 - -40℃; Stage #2: methyl iodide In tetrahydrofuran; hexane Cooling; | 96% |
Stage #1: 2,6-Dichloroaniline With n-butyllithium In tetrahydrofuran; hexane at -78 - -40℃; Stage #2: methyl iodide In tetrahydrofuran; hexane at -78 - 20℃; Stage #3: With ammonium chloride In tetrahydrofuran; hexane; water at 20℃; | 96% |
Conditions | Yield |
---|---|
With C24H50N5Si2Y In toluene at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 96% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium bromide; HZSM-5 In acetic acid at 20℃; for 4h; Bromination; | 95% |
With tetrabutylammomium bromide; copper(ll) bromide In ethanol at 25℃; regioselective reaction; | 93% |
With sodium tungstate; sodium perborate; sulfuric acid; acetic anhydride; potassium bromide In acetic acid for 1h; Ambient temperature; | 70% |
Conditions | Yield |
---|---|
With isopentyl nitrite In acetic acid for 0.0833333h; | 95% |
Conditions | Yield |
---|---|
With sodium azide In neat (no solvent) at 100℃; for 0.75h; | 95% |
Conditions | Yield |
---|---|
at 130℃; for 0.25h; Temperature; Solvent; Reagent/catalyst; Inert atmosphere; Microwave irradiation; | 95% |
Conditions | Yield |
---|---|
at 130℃; for 0.25h; Inert atmosphere; Microwave irradiation; | 95% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | 95% |
Conditions | Yield |
---|---|
With copper(II) oxide In 1,4-dioxane at 130℃; for 20h; Reagent/catalyst; Solvent; | 95% |
Conditions | Yield |
---|---|
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; 4-phenyl-N-methylpyridinium iodide; 4,4'-di-tert-butyl-2,2'-bipyridine; zinc In dimethyl sulfoxide at 80℃; for 8h; Reagent/catalyst; Inert atmosphere; | 95% |
methanesulfonyl isocyanate
2,6-Dichloroaniline
1-(2,6-dichlorophenyl)-3-methanesulfonylurea
Conditions | Yield |
---|---|
In benzene | 94.6% |
Conditions | Yield |
---|---|
With johnphos; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In toluene for 1h; Heating; | 94% |
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