CAS No.13453-32-2,THALLIUM(III) CHLORIDE HYDRATE Suppliers

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Synonyms: thalliumchloride(tlcl3);thallium trichloride;THALLIUM(III)TRICHLORIDE CAS: 13453-32-2 MF: Cl3Tl MW: 310.7423 EINECS: 236-625-2

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Synthetic route

: thallium (III) oxide

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With hydrogenchloride In not given rather concd. HCl, boiling;;	100%
With HCl In not given rather concd. HCl, boiling;;	100%

: 7719-09-7
thionyl chloride

: thallium chloride

: 7782-50-5
chlorine

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In acetonitrile TlCl suspd. in CH3CN; Cl2 added under vigorous stirring; stirred for 30 min; soln. filtered; solvent evapd. in vacuum; SOCl2 added; evapd. after 10 min;	98.5%

...Expand

: thallium(I) nitrate

: 2696-92-6
nitrosylchloride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) at -20°C;;
In neat (no solvent) at -20°C;;

: thallium chloride

: 2696-92-6
nitrosylchloride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) at -20°C;;
In neat (no solvent) at -20°C;;

: thallium chloride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With chlorine In not given heating;;
With chlorine In water aq. suspension of TlCl;;
With KMnO4 or PbO2 or BaO2 In hydrogenchloride

: thallium chloride

: 15906-70-4
chlorochromate(VI) ion

A: chromium (III) ion

B: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With hydrogenchloride In acetic acid Kinetics; prepn. of mixtures (TL(I), Cr(VI)) in 60% aq.CH3COOH (1.23 mol/l); keeping them at 25°C for about 3 h; accelaration of react. on increasing concn. of H(+) and Cl(-); addn. of Tl(III), Cr(III), Mn(II), Ce(III), Th(IV), U(VI) does not affect react.; detn. of Cr(VI) spectrophotometrically; detn. of Tl(III) jodometrically;
With ammonium vanadate In acetic acid Kinetics; prepn. of mixtures of TlCl and CrO3Cl(1-) in 60% aq. acetic acid contg. 1.25 mol/l HCl; keeping them at 25°C for more than 3 h; accelaration of react. by addn. of V(V) until concn. of V(V) exceeds concn. of Tl(I); detn. of Cr(VI) spectrophotometrically, detn. of Tl(III) jodometrically;

...Expand

: thallium (III) oxide

A: thallium chloride

B: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) vigorous reaction (coooling by solid CO2);;
In neat (no solvent) vigorous reaction (coooling by solid CO2);;

: thallium(I) chromate

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With hydrogenchloride In hydrogenchloride byproducts: Cl2; decompn.;;
With HCl In hydrogenchloride byproducts: Cl2; decompn.;;

: 13826-63-6
thallium nitrite

: 2696-92-6
nitrosylchloride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) at -20°C;;
In neat (no solvent) at -20°C;;

: thallium(I) oxide

: 2696-92-6
nitrosylchloride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) at -20°C;;
In neat (no solvent) at -20°C;;

: thallium chloride

: 7782-50-5
chlorine

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
in a sealed tube at 6-7 atm below 150 °C;;
In water aq. suspension;; aq. soln. obtained;;
In neat (no solvent)

: thallium(I) trichromate(VI)

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With hydrogenchloride In hydrogenchloride byproducts: Cl2; decompn. by HCl soln.;;
With HCl In hydrogenchloride byproducts: Cl2; decompn. by HCl soln.;;

: thallium(I) dichromate(VI)

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With hydrogenchloride In hydrogenchloride byproducts: Cl2; decompn.;;
With HCl In hydrogenchloride byproducts: Cl2; decompn.;;

: 19628-33-2
monophenylthallium dichloride

A: 13453-32-2
thallium (III) chloride

B: 100-56-1
phenylmercury(II) chloride

Conditions

Conditions	Yield
With mercury dichloride In water

: thallium

: 7791-25-5
sulfuryl dichloride

A: Tl4Cl6

B: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In acetonitrile addn. of Tl to soln. of SO2Cl2 (3 d); evapn., dissolution of TlCl3 in H2O; elem. anal.;

...Expand

: thallium

: 7782-50-5
chlorine

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In water aq. suspension;; aq. soln. obtained;;
In neat (no solvent)
In neat (no solvent)
In water

: 3 thallium(I) chloride * thallium(III) chloride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With chlorine In water
In water

: thallium(III) chloride dihydrate

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) prolonged heating on air;;
In neat (no solvent) prolonged heating on air;;

: thallium(III) chloride * diethylether

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: ether; in vac.; the educt melts with loss of ether ad solidifies upon cooling;; anhydrous TlCl3 obtained;;
In neat (no solvent) byproducts: ether; in vac.;; anhyd. TlCl3 obtained;;
In neat (no solvent) byproducts: ether; in vac.; the educt melts with loss of ether ad solidifies upon cooling;; anhydrous TlCl3 obtained;;
In neat (no solvent) byproducts: ether; in vac.;; anhyd. TlCl3 obtained;;

: 7647-01-0
hydrogenchloride

: thallium (III) oxide

A: 3 thallium(I) chloride * thallium(III) chloride

B: thallium(I) chloride * thallium(III) chloride

C: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In not given dissolving Tl2O3 in HCl soln.;;
In not given dissolving Tl2O3 in HCl soln.;;
In not given

...Expand

: 7647-01-0
hydrogenchloride

: thallium (III) oxide

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In not given under evolution of heat;;
In not given dissolving Tl2O3 in HCl;; aq. soln. obtained; contains considerable amts. of thallium(I,III) chlorides;;
In not given dissolving Tl2O3 in dil. HCl soln.;; aq. soln. obtained;;
In not given under evolution of heat;;
In not given

: thallium(III) chloride tetrahydrate

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) heating in dry air stream for 1h to 100 °C;; almost anhyd. TlCl3 obtained;;
In neat (no solvent) in presence of KOH in a sealed tube at room temp. in vac. or 1 atm; resp. in a desiccator over P2O5;;
In neat (no solvent) slow dehydration over P2O5 in a desiccator;;

: 7719-09-7
thionyl chloride

: thallium(III) chloride hydrate

A: 7647-01-0
hydrogenchloride

B: thallium chloride

C: 7446-09-5
sulfur dioxide

D: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) dehydratation; room temp.;;	A n/a B >1 C n/a D n/a
In neat (no solvent) dehydratation; room temp.;;	A n/a B >1 C n/a D n/a

...Expand

: 192875-04-0
thallium(III) chloride monohydrate

A: thallium chloride

B: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) prolonged heating to 100 °C;;
In neat (no solvent) prolonged heating to 100 °C;;

: thallium(I) chloride * thallium(III) chloride

A: 3 thallium(I) chloride * thallium(III) chloride

B: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In water H2O or solvents miscible with H2O;;
In water coldness;;
In water

: thallium(I) chloride * thallium(III) chloride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With Cl2 In not given in presence of moisture;; aq. TlCl3 obtained;;
In not given

: thallium(III) oxyfluoride

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With hydrogenchloride In not given
With HCl In not given

: p-Bromophenylthallium dichloride

A: 28969-28-0
4-Bromphenylquecksilberchlorid

B: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With mercury dichloride In water

: 124159-02-0
C6H5N2(1+)*Cl(1-)*TlCl3=C6H5N2Cl*TlCl3

A: thallium chloride

B: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: N2, C6H5Cl, Cl2; heating to 75-80 °C; further byproducts: (C6H5)2, C6H5OH;;
In water byproducts: N2, C6H5Cl, Cl2; heating to 75-80 °C; further byproducts: (C6H5)2, C6H5OH;;

: C6H4BrTl(2+)*2Cl(1-)=C6H4BrTlCl2

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
With mercury dichloride In not given byproducts: p-C6H4BrHgCl;
With HgCl2 In not given byproducts: p-C6H4BrHgCl;

: 603-36-1
triphenylantimony

: 13453-32-2
thallium (III) chloride

: 594-31-0, 34716-91-1, 20265-29-6
triphenylantimony dichloride

Conditions

Conditions	Yield
In ethanol; toluene	100%
In ethanol; toluene	100%

: 13453-32-2
thallium (III) chloride

: thallium (III) oxide

Conditions

Conditions	Yield
With alkali In not given	100%
With chloride In water	100%
With alkali In not given	100%

: 13453-32-2
thallium (III) chloride

: thallium chloride

Conditions

Conditions	Yield
With iron(II) sulfate In not given prolonged boiling with huge excess FeSO4;;	100%
With hydroquinone In not given byproducts: quinone, quinhydrone;
With sulfur dioxide In water

: 13453-32-2
thallium (III) chloride

: 93690-72-3
tri(isopropenyl)bismuthane

A: (CH2C(CH3))TlCl

B: 7787-60-2
bismuth(III) chloride

Conditions

Conditions	Yield
In diethyl ether at -40°C;	A 98% B n/a

...Expand

: 1076-44-4
Li(1+)*C6F5(1-)=Li(C6F5)

: 1100-88-5
benzyltriphenylphosphonium chloride

: 13453-32-2
thallium (III) chloride

: 75579-15-6
(C6H5)3PCH2C6H5(1+)*[Tl(C6F5)4](1-)=((C6H5)3PCH2C6H5)[Tl(C6F5)4]

Conditions

Conditions	Yield
In diethyl ether TlCl3 added to LiC6F5 soln. at -78°C, stirred for 15 min, allowed to warm to room temp., stirred for 3 h under N2, a few drops of H2O added, Ph3BzPCl added; exposed to air for 10 min, filtered, evapd., recrystd. (CH2Cl2/hexane);elem. anal.;	96%

...Expand

: (NBu4)[Pt(C6Cl5)4]

: 13453-32-2
thallium (III) chloride

: (CH3CH2CH2CH2)4N(1+)*Pt(C6Cl5)4(1-)=[N(C4H9)4][Pt(C6Cl5)4]

Conditions

Conditions	Yield
In dichloromethane byproducts: TlCl, [N((CH2)3CH3)4]TlCl4; addn. of soln. of Pt-complex to TlCl3 (Pt : Tl = 2 : 3), stirring (roomtemp., 24 h); centrifugation off of TlCl, evapn. to dryness, washing (MeOH);	92%

: 13453-32-2
thallium (III) chloride

: 1,2-ethylene-3,3'-di-tert-butyl-diimidazole-2,2'-diylidene

: [TlCl3((C3H2N2C(CH3)3)2CH2CH2)]

Conditions

Conditions	Yield
In tetrahydrofuran (Ar or N2); using Schlenk techniques; addn. dropwise of soln. of 1,2-ethylene-3,3'-di-tert-butyl-diimidazole-2,2'-diylidene in THF to soln. of TlCl3 in THF at -50°C over 15 min, warming to room temp., stirringovernight; pptn., filtration, washing with THF, drying in vac.;	92%

: dichlorobis-(π-cyclopentadienyl)tantalum(IV)

: 13453-32-2
thallium (III) chloride

: (η5-cyclopentadienyl)2TaCl(μ-Cl)TlCl3

Conditions

Conditions	Yield
In not given under inert gas; TlCl3 added to suspn. of Cp2TaCl2, stirred at room temp. for 0.5 h; solid filtered off, washed with Et2O, dried in vac.; elem. anal.;	90%

: [(S)-(2-Me2NCH(Me)C6H4)2TlCl]

: 13453-32-2
thallium (III) chloride

: [(S)-(2-Me2-NCH(Me)C6H4)TlCl2]

Conditions

Conditions	Yield
In dichloromethane byproducts: LiCl; Tl-compound and TlCl3 stirred in CH2Cl2 for 10 min; filtered, evapd., washed with pentane, dried in vac. elem.anal.;	90%

: 7440-74-6
indium

: thallium

: 10026-12-7
niobium pentachloride

: 13453-32-2
thallium (III) chloride

: Tl[Nb6Cl15]

Conditions

Conditions	Yield
In neat (no solvent, solid phase) vac.; stoichiometric amts., heating (720.degre.C, 3 d), cooling (room temp.);	90%

...Expand

: 1076-44-4
Li(1+)*C6F5(1-)=Li(C6F5)

: 1643-19-2
tetrabutylammomium bromide

: 13453-32-2
thallium (III) chloride

: {(n-C4H9)4N}-tetrakis(pentafluorophenyl)thalliate(III)

Conditions

Conditions	Yield
In diethyl ether TlCl3 added to LiC6F5 soln. at -78°C, stirred for 15 min, allowed to warm to room temp., stirred for 4 h under N2, (C4H9)4NBr added; exposed to air for 10 min, filtered, evapd., recrystd. (CH2Cl2/hexane);elem. anal.;	89%
In diethyl ether Tl complex (obtained from TlCl3 and (C4H9)4NBr) added to ether soln. ofLi salt; exposed to air for 10 min, filtered, evapd., recrystd. (CH2Cl2/hexane);elem. anal.;	60%

...Expand

: {(n-C4H9)4N}-tetrakis(pentafluorophenyl)thalliate(III)

: 13453-32-2
thallium (III) chloride

A: {(n-C4H9)4N}-tris(pentafluorophenyl)chlorothalliate(III)

B: {(n-C4H9)4N}-chloro-bis{chlorobis(pentafluorophenyl)}dithalliate(III)

Conditions

Conditions	Yield
In diethyl ether stirred for 48 h at room temp.; filtered, evapd., crystd. (Bu2O), recrystd. (CH2Cl2/hexane); elem. anal.;	A 88% B n/a

...Expand

: 24261-90-3
N,N,N'-tris(trimethylsilyl)benzamidine

: 13453-32-2
thallium (III) chloride

: (C6H5C(NHSi(CH3)3)2)(1+)*(C6H5C(NSi(CH3)3)2TlCl3)(1-)=(C6H5C(NHSi(CH3)3)2)(C6H5C(NSi(CH3)3)2TlCl3)

B: 137680-56-9
N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: ClSi(CH3)3; absence of moisture, solution is stirred at room temp. and allowed to stand for 12 h; volume is reduced under vacuum, filtrate is washed with THF and dried under vacuum, elem. anal.;	A 11% B 85%

...Expand

: 13453-32-2
thallium (III) chloride

: 368-49-0
3-(trifluoromethyl)phenyllithium

: Tl(CF3C6H4)2Cl

Conditions

Conditions	Yield
In diethyl ether byproducts: LiCl; TlCl3 added to Li educt (1/2 molar ratio) soln. at -78°C under N2, stirred for 30 min, warmed slowly to room temp.; filtered, hydrolyzed with aq. HCl, org. layer removed, dried (MgSO4), evapd.; elem. anal.;	85%

: 221364-56-3
[CH2(CH2NSi(CH3)3)2](Li(C4H8O))2

: 13453-32-2
thallium (III) chloride

: 221364-76-7
([CH2(CH2NSi(CH3)3)2]2Tl)Li(C4H8O)2

Conditions

Conditions	Yield
In tetrahydrofuran Ar-atmosphere; stirring TlCl3 with 2 equiv. of Li-complex at -78°C, warming to room temp., stirring for 20 h; solvent removal (vac.), extn. into pentane, centrifugation, solvent removal, drying (vac., 6 h), recrystn. (pentane); elem. anal.;	84%

: 1076-44-4
Li(1+)*C6F5(1-)=Li(C6F5)

: 13453-32-2
thallium (III) chloride

: 1813-39-4
chlorobis(pentafluorophenyl)thallium(III)

Conditions

Conditions	Yield
In diethyl ether byproducts: LiCl; TlCl3 added to Li educt (1/2 molar ratio) soln. at -78°C under N2, stirred for 30 min, warmed slowly to room temp.; filtered, hydrolyzed with aq. HCl, org. layer removed, dried (MgSO4), evapd., recrystd. (C6H6); elem. anal.;	83%

: 13453-32-2
thallium (III) chloride

: 1076-44-4
pentafluorophenyl lithium

: bis(pentafluorophenyl)thallium chloride

Conditions

Conditions	Yield
In diethyl ether -78°C, 0.5 h, stirring, anhydr. TlCl3;	83%
In diethyl ether -78°C, 0.5 h, stirring, anhydr. TlCl3;	83%

: 13453-32-2
thallium (III) chloride

: 141556-42-5
[1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene

: C(NC6H2(CH3)3)2CHCHTlCl3

Conditions

Conditions	Yield
In tetrahydrofuran addn. of a soln. of ligand in THF to a soln. of thallium salt in THF at -30°C over 20 min, stirring overnight, warming to room temp.; evapn., recrystn. (THF, -10°C); elem. anal.;	83%

: 1259-34-3
tris(pentafluorophenyl)arsine

: 13453-32-2
thallium (III) chloride

: 18005-76-0
tris(pentafluorophenyl) arsenic(V) dichloride

Conditions

Conditions	Yield
In diethyl ether at room temp. for 12 h;	80%

: 13453-32-2
thallium (III) chloride

: 603-33-8
triphenylbismuthane

: 5153-28-6
diphenylbismuth(III) chloride

Conditions

Conditions	Yield
In diethyl ether byproducts: (C6H5)2TlCl; 20°C;	80%
In diethyl ether byproducts: (C6H5)2TlCl; 20°C;	80%
In chloroform byproducts: BiCl3, C6H6; 5 h reflux;
In chloroform

: 187877-83-4
TlMes3

: 13453-32-2
thallium (III) chloride

: [(Mes2TlCl)(MesTlCl2)]

Conditions

Conditions	Yield
In toluene TlCl3 added to toluene soln. of TlMes3 at 0°C; left standing for 12 h; heated under reflux for 1 h; filtered when hot; cooled to 20°C; warmed and cooled again; elem.anal.;	79%

: 13453-32-2
thallium (III) chloride

: 30123-12-7
silver(I)pentafluorobenzene

: 1813-39-4
chlorobis(pentafluorophenyl)thallium(III)

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: AgCl; TlCl3 added to ether soln. of Ag-compd. (molar ratio 1:2), stirred 2h under N2, pptn. of AgCl; AgCl filtered off, soln. concd., n-hexane added, pptn.;	78%
In diethyl ether byproducts: AgCl; TlCl3 added to ether soln. of Ag-compd. (molar ratio 1:1.5), stirred 3h under N2, pptn. of AgCl; AgCl filtered off, soln. concd., n-hexane added, pptn.;	45%

: 1643-19-2
tetrabutylammomium bromide

: 13453-32-2
thallium (III) chloride

: 6782-80-5
pentachlorophenyllithium

: 75563-64-3
(C4H9)4N(1+)*[Tl(C6Cl5)4](1-)=(C4H9)4N[Tl(C6Cl5)4]

Conditions

Conditions	Yield
In diethyl ether Tl complex (obtained from TlCl3 and (C4H9)4NBr) added to ether soln. ofLi salt; exposed to air for 10 min, filtered, evapd., recrystd. (CH2Cl2/hexane);elem. anal.;	78%

...Expand

: 13453-32-2
thallium (III) chloride

: 3-dimethylaminopropyllithium

: bis(dimethylaminopropyl)thallium chloride

Conditions

Conditions	Yield
In diethyl ether byproducts: LiCl; Ar atm.; molar ratio TlCl3:ligand 1:2, cooling (-50°C), stirring (2 h, room temp.); filtn., extraction (Et2O), sublimation (1E-3 torr, 130°C); elem. anal.;	78%

: 13453-32-2
thallium (III) chloride

: 53732-49-3
lithium-2,4,6-trifluorophenyl

: 74625-70-0
thallium(III)Cl(2.4.6-C6F3H2)2

Conditions

Conditions	Yield
In diethyl ether byproducts: LiCl; TlCl3 added to Li educt (1/2 molar ratio) soln. at -78°C under N2, stirred for 30 min, warmed slowly to room temp.; filtered, hydrolyzed with aq. HCl, org. layer removed, dried (MgSO4), evapd., recrystd. (CH2Cl2/hexane); elem. anal.;	75%

: 13453-32-2
thallium (III) chloride

: C6F4H(1-)*Li(1+)=C6F4HLi

: 84356-31-0
Tl(C6F4H)2Cl

Conditions

Conditions	Yield
In diethyl ether byproducts: LiCl; TlCl3 added to Li educt (1/2 molar ratio) soln. at -78°C under N2, stirred for 30 min, warmed slowly to room temp.; filtered, hydrolyzed with aq. HCl, org. layer removed, dried (MgSO4), evapd., recrystd. (CH2Cl2/hexane); elem. anal.;	75%

: chlorodi-η5-cyclopentadienyltantalum

: 13453-32-2
thallium (III) chloride

: 86721-88-2
(η5-cyclopentadienyl)2Ta(μ-Cl)2TlCl2

Conditions

Conditions	Yield
In tetrahydrofuran; diethyl ether under inert gas; soln. of TlCl3 in Et2O added to soln. of Cp2TaCl in THF; solid filtered, washed with Et2O, dried in vac.; elem. anal.;	75%

: 879-05-0
2,3,4,5,6-pentafluorophenylmagnesium bromide

: 13453-32-2
thallium (III) chloride

: bis(pentafluorophenyl)thallium bromide

Conditions

Conditions	Yield
In diethyl ether molar ratio of C6F5MgBr and TlCl3 = 8:3;	74%
In diethyl ether molar ratio of C6F5MgBr and TlCl3 = 8:3;	74%

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RIDADR	1707
HazardClass	6.1(a)
PackingGroup	II

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