Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:15307-79-6
Min.Order:10 Kilogram
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Type:Trading Company
inquiryAppearance:White or slightly yellow powder Storage:R.T Package:25kg/drum Application:Anti-inflammatory and analgesic Transportation:Express/Sea/Air Port:Any port in China
Cas:15307-79-6
Min.Order:25 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:Diclofenac sodium CAS No:15307-79-6 Sy
Specifications CAS No.: 15307-79-6 Other Names: diclofenac sodium, diclofenac sodium MF: 15307-79-6 EINECS No.: 15307-79-6
Why is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) W
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $825.0 / 1100.0
Type:Trading Company
inquiry1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Onchem specialized in APIs, chemical intermediate
Cas:15307-79-6
Min.Order:25 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $9.5 / 9.8
Type:Trading Company
inquiryStrict quality control: good raw materials, good quality, Zenuo Biology has always regarded quality as the life of the enterprise. Zenuo Biology has an independent quality control department and long-term cooperation with the third-party detection
Cas:15307-79-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryBest quality! Competitive Price!! Long-term stable Supply!!! Experienced shipment Service!!!! Excellent after-sales Service!!!!! JOSUN INTERNATIONAL LIMITED is a pharmaceutical company which is integrated with manufacturing, marketing, RD in C
Items Standard Result Appearance A white or or slightly yellowish crystalline powder White crystalline powder
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $12.0 / 15.0
Type:Manufacturers
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:15307-79-6
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryUnique advantages for Diclofenac sodium Cas 15307-79-6 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Cream colour powder with characteristic odour Storage:-20°C Freezer Pac
Cas:15307-79-6
Min.Order:25 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryXi’an Quanao Biotech Co., Ltd. with 18 years experience in plant extract filed. Product grade: Medicine, Health care product, Cosmetics, Food, Beverage, Feed. Hot selling market: Europe, North America, South America, Middle East, Asia Pacifi
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $8.0 / 12.0
Type:Manufacturers
inquiryGood quality Competitive price On time delivery Our Advantages: Full experience of large numbers containers loading in main Chinese seaports Packing with pallet as buyer's special request Best service after shipment with e-mail
Cas:15307-79-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:15307-79-6
Min.Order:1
Negotiable
Type:Other
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:15307-79-6
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryADVANTAGE: 1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day 2. The products are provided with COA, HPLC, NMR, quality assurance,
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Cas:15307-79-6
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Diclofenac sodium Manufacturer Factory CAS 15307-79-6 Diclofenac sodium Manufacturer High quality Best price In stock factory CAS 15307-79-6 Diclofenac sodium COA TDS price MSDS Diclofenac sodium Chemical Properties Melting point 288-290&de
Cas:15307-79-6
Min.Order:5 Kiloliter
FOB Price: $3.5 / 5.0
Type:Manufacturers
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryName:Diclofenac Sodium Name:Diclofenac Sodium CAS no:15307-79-6 Grade:Medical chemical industry Molecular formula:C14H10Cl2NNaO2 Molecular weight: 318.14 Product Quality 12 years of chemical raw materials Mature operation of the indu
Cas:15307-79-6
Min.Order:25 Kilogram
FOB Price: $1.0 / 2.0
Type:Other
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:15307-79-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:15307-79-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:15307-79-6
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:15307-79-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: Diclofenac Sodium CAS No: 15307-79-6 EC No: 239-346-4 Molecular Formula: C14H10CL2NNaO2 Molecular Weight: 318.13 Appearance: White Powder Storage:Store in cool and dry place, away from sun light. Package: 25 KG/Wov
Our Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
Cas:15307-79-6
Min.Order:10 Gram
Negotiable
Type:Other
inquiry2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester
diclofenac sodium
Conditions | Yield |
---|---|
With sodium hydroxide In water; N,N-dimethyl-formamide at 80℃; for 24h; | 96.1% |
1-(2,6-dichlorophenyl)indolin-2-one
diclofenac sodium
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water for 4h; Heating; | 93% |
With sodium dithionite; water; sodium hydroxide for 6h; Reflux; | 92.3% |
With sodium hydroxide In ethanol for 3h; Heating; | 85% |
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In toluene for 10h; Reflux; | 83.6% |
With sodium hydroxide for 2h; Temperature; Reflux; | 4.035 g |
diclofenac sodium
Conditions | Yield |
---|---|
With water; sodium hydroxide In methanol for 6h; Solvent; Reflux; | 86% |
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; copper; potassium carbonate at 120℃; for 22h; | 56% |
2'-chloro-benzeneacetic acid
2,6-Dichloroaniline
butan-1-ol
diclofenac sodium
Conditions | Yield |
---|---|
With sodium hydroxide; potassium iodide; copper(I) iodide; potassium carbonate In N,N-dimethyl-formamide | 42.9% |
Conditions | Yield |
---|---|
Stage #1: 2'-chloro-benzeneacetic acid; 2,6-Dichloroaniline With copper(l) iodide; iodine; potassium carbonate; potassium iodide In N,N-dimethyl-formamide for 12h; Inert atmosphere; Schlenk technique; Reflux; Stage #2: With sodium hydroxide In water for 4h; Reflux; | 31% |
2-(2-((2,6-dichlorophenyl)amino)phenyl)-2-oxoacetic acid
diclofenac sodium
Conditions | Yield |
---|---|
With sodium methylate; hydrazine hydrate In 2-methoxy-ethanol 1.) from 60 deg C to 150 deg C, 2.) 150 deg C, 1 h; Yield given; |
N-phenyl-2,6-dichloroaniline
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: benzene / 6 h / Heating 2: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature 3: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating 4: 97 percent / Zn / acetic acid / 4 h / Heating 5: 85 percent / 20percent NaOH / ethanol / 3 h / Heating View Scheme | |
Multi-step reaction with 5 steps 1: benzene / 6 h / Heating 2: N-chlorosuccinimide / CCl4 / 1 h / Ambient temperature 3: SnCl4 / CCl4 / 0.83 h / Ambient temperature 4: 97 percent / Zn / acetic acid / 4 h / Heating 5: 85 percent / 20percent NaOH / ethanol / 3 h / Heating View Scheme | |
Multi-step reaction with 4 steps 1: benzene / 2 h / Ambient temperature 2: AlCl3 / various solvent(s) / 20 h / Ambient temperature 3: 1 N NaOH / ethanol; H2O / 0.17 h / Heating 4: hydrazine hydrate, NaOCH3 / 2-methoxy-ethanol / 1.) from 60 deg C to 150 deg C, 2.) 150 deg C, 1 h View Scheme | |
Multi-step reaction with 3 steps 1: 66 percent / 16 h / Heating 2: 75.4 percent / AlCl3 / 2 h / 160 °C 3: 93 percent / 2 N NaOH / ethanol; H2O / 4 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: toluene / 3 h / 120 °C 2: triethylamine hydrochloride-aluminum trichloride / 4.5 h / 20 - 60 °C 3: sodium hydroxide / 2 h / Reflux View Scheme |
N-(2,6-dichlorophenyl)-α-(methylthio)acetanilide
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature 2: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating 3: 97 percent / Zn / acetic acid / 4 h / Heating 4: 85 percent / 20percent NaOH / ethanol / 3 h / Heating View Scheme | |
Multi-step reaction with 4 steps 1: N-chlorosuccinimide / CCl4 / 1 h / Ambient temperature 2: SnCl4 / CCl4 / 0.83 h / Ambient temperature 3: 97 percent / Zn / acetic acid / 4 h / Heating 4: 85 percent / 20percent NaOH / ethanol / 3 h / Heating View Scheme |
1-(2,6-dichlorophenyl)-3-(methylthio)oxindole
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 97 percent / Zn / acetic acid / 4 h / Heating 2: 85 percent / 20percent NaOH / ethanol / 3 h / Heating View Scheme |
N-(2,6-dichlorophenyl)-α-(methylsulfinyl)acetanilide
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating 2: 97 percent / Zn / acetic acid / 4 h / Heating 3: 85 percent / 20percent NaOH / ethanol / 3 h / Heating View Scheme |
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SnCl4 / CCl4 / 0.83 h / Ambient temperature 2: 97 percent / Zn / acetic acid / 4 h / Heating 3: 85 percent / 20percent NaOH / ethanol / 3 h / Heating View Scheme |
1-(2,6-Dichlorphenyl)-2,3-indoldion
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1 N NaOH / ethanol; H2O / 0.17 h / Heating 2: hydrazine hydrate, NaOCH3 / 2-methoxy-ethanol / 1.) from 60 deg C to 150 deg C, 2.) 150 deg C, 1 h View Scheme |
[(2,6-Dichloro-phenyl)-phenyl-amino]-oxo-acetyl chloride
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: AlCl3 / various solvent(s) / 20 h / Ambient temperature 2: 1 N NaOH / ethanol; H2O / 0.17 h / Heating 3: hydrazine hydrate, NaOCH3 / 2-methoxy-ethanol / 1.) from 60 deg C to 150 deg C, 2.) 150 deg C, 1 h View Scheme |
2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75.4 percent / AlCl3 / 2 h / 160 °C 2: 93 percent / 2 N NaOH / ethanol; H2O / 4 h / Heating View Scheme |
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tert-butylhypochlorite / dichloromethane / 10 h / 25 °C / Cooling with ice 2: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Cooling with ice 3: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / toluene / 10 h / Reflux View Scheme |
2,6-Dichloroaniline
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: calcium chloride; pyridine / 4 h / Reflux; Cooling with ice 2: tert-butylhypochlorite / dichloromethane / 10 h / 25 °C / Cooling with ice 3: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Cooling with ice 4: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / toluene / 10 h / Reflux View Scheme |
phenylacetyl chloride
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: calcium chloride; pyridine / 4 h / Reflux; Cooling with ice 2: tert-butylhypochlorite / dichloromethane / 10 h / 25 °C / Cooling with ice 3: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Cooling with ice 4: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / toluene / 10 h / Reflux View Scheme |
(2-benzoylamino-phenyl)-acetic acid methyl ester
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: thionyl chloride / 3 h / Reflux 1.2: 3 h / Cooling with ice; Reflux 2.1: diphenylether / 3 h / Reflux 3.1: sodium hydroxide; water / methanol / 6 h / Reflux View Scheme |
methyl (2-nitrophenyl)acetate
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: palladium on activated charcoal; hydrogen / toluene / 5 °C / 760.05 Torr 2.1: triethylamine / toluene / 2 h / 0 °C 3.1: thionyl chloride / 3 h / Reflux 3.2: 3 h / Cooling with ice; Reflux 4.1: diphenylether / 3 h / Reflux 5.1: sodium hydroxide; water / methanol / 6 h / Reflux View Scheme |
benzeneacetic acid methyl ester
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: nitric acid / dichloromethane / 24 h / 0 - 20 °C 2.1: palladium on activated charcoal; hydrogen / toluene / 5 °C / 760.05 Torr 3.1: triethylamine / toluene / 2 h / 0 °C 4.1: thionyl chloride / 3 h / Reflux 4.2: 3 h / Cooling with ice; Reflux 5.1: diphenylether / 3 h / Reflux 6.1: sodium hydroxide; water / methanol / 6 h / Reflux View Scheme |
2-aminophenylacetic acid methyl ester
diclofenac sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: triethylamine / toluene / 2 h / 0 °C 2.1: thionyl chloride / 3 h / Reflux 2.2: 3 h / Cooling with ice; Reflux 3.1: diphenylether / 3 h / Reflux 4.1: sodium hydroxide; water / methanol / 6 h / Reflux View Scheme |
didecyldimethylammonium chloride
diclofenac sodium
diclofenac didecyldimethylammonium salt
Conditions | Yield |
---|---|
In water at 20℃; for 0.5h; Product distribution / selectivity; | 100% |
diclofenac sodium
cadmium(II) chloride
{Cd(C6H3Cl2NHC6H4CH2COO)2(H2O)}
Conditions | Yield |
---|---|
With H2O; KOH In water byproducts: NaCl; mixing aq. soln. of the components, adjusting to pH 5.5-7.5 with KOH and stirring at room temp. for 4-6 h; filtn., washing with water, drying over silica gel (vac.) and over P4O10 at 90°C (vac.); | 100% |
diclofenac sodium
zinc(II) chloride
{Zn(C6H3Cl2NHC6H4CH2COO)2(H2O)}
Conditions | Yield |
---|---|
With H2O; KOH In water byproducts: NaCl; mixing aq. soln. of the components, adjusting to pH 5.5-7.5 with KOH and stirring at room temp. for 4-6 h; filtn., washing with water, drying over silica gel (vac.) and over P4O10 at 90°C (vac.); | 100% |
diclofenac sodium
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water; acetone at 20 - 45℃; for 3h; pH=1.4 - 1.6; Solvent; | 99% |
With hydrogenchloride In water Cooling with ice; | 90% |
With hydrogenchloride In water at 0 - 20℃; | 70% |
diclofenac sodium
1-(2,6-dichlorophenyl)-1,3-dihydro-indol-2-one-[3,3,5,7-D4]
Conditions | Yield |
---|---|
With water-d2; hydrogen chloride at 160℃; for 0.333333h; Microwave irradiation; | 96% |
choline chloride
diclofenac sodium
(2-hydroxyethyl)tri-methylammonium [o-(2,6-dichloroanilino)phenyl]acetate
Conditions | Yield |
---|---|
In ethanol at 20℃; for 1h; | 96% |
diclofenac sodium
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide
1-O-<2-<(2,6-dichlorophenyl)amino>phenylacetyl>-2,3,4,6-tetra-O-acetyl-β-D-glucopyranose
Conditions | Yield |
---|---|
citrimide In water; 1,2-dichloro-ethane Ambient temperature; | 95% |
bromoacetic acid tert-butyl ester
diclofenac sodium
2-((2,6-dichlorophenyl)amino)phenylacetoxyacetic acid tert-butyl ester
Conditions | Yield |
---|---|
With potassium iodide In ethanol at 61 - 65℃; for 3h; Temperature; Large scale; | 94.45% |
With potassium iodide In acetonitrile at 30℃; for 0.25h; Microwave irradiation; | 91.6% |
With tetra(n-butyl)ammonium hydrogensulfate; potassium iodide In water; acetone at 60 - 65℃; for 2h; | 17.3 g |
In N,N-dimethyl-formamide at 20 - 45℃; |
4-methyloxetan-2-one
diclofenac sodium
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 20℃; | 94% |
diclofenac sodium
Conditions | Yield |
---|---|
With trifluoroacetic acid-d1 at 110℃; for 16h; Sealed tube; | 94% |
4,4'-bipyridine
diclofenac sodium
Conditions | Yield |
---|---|
In water; acetonitrile at 50℃; | 94% |
diclofenac sodium
3-(bromomethyl)-4-methyl-1,2,5-oxadiazole-2-oxide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20 - 25℃; for 2h; | 93% |
2-(2-Hydroxyethyl)pyridine
diclofenac sodium
copper(II) acetate monohydrate
Conditions | Yield |
---|---|
In methanol at 50℃; | 91% |
diclofenac sodium
N,N-didecyl-N,N-dimethylammonium bromide
diclofenac didecyldimethylammonium salt
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; sodium hydroxide In methanol; water at 20℃; for 0.5h; | 91% |
diclofenac sodium
methyl iodide
2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 90% |
In acetone Heating; |
Conditions | Yield |
---|---|
In water at 20℃; | 90% |
tert-Butyl chloroacetate
diclofenac sodium
2-((2,6-dichlorophenyl)amino)phenylacetoxyacetic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium iodide In acetonitrile at 77 - 78℃; for 2h; | 89.6% |
In acetonitrile for 4h; Reflux; | |
With potassium iodide In N,N-dimethyl-formamide for 2h; Reflux; Large scale; | 25.5 g |
diclofenac sodium
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20 - 25℃; for 2h; | 89% |
diclofenac sodium
5-(bromomethyl)benzofuroxan
given name is incorrect
Conditions | Yield |
---|---|
With N-Bromosuccinimide; dibenzoyl peroxide In N,N-dimethyl-formamide at 25℃; for 2h; | 89% |
2-(2-Hydroxyethyl)pyridine
diclofenac sodium
Conditions | Yield |
---|---|
In methanol at 50℃; | 89% |
methanol
diclofenac sodium
Conditions | Yield |
---|---|
In water at 20℃; | 89% |
1H-imidazole
diclofenac sodium
Conditions | Yield |
---|---|
In methanol; water at 20℃; | 89% |
didecyldimethylammonium acesulfamate
diclofenac sodium
diclofenac didecyldimethylammonium salt
Conditions | Yield |
---|---|
In acetone at 60℃; for 2h; Product distribution / selectivity; | 88% |
Conditions | Yield |
---|---|
In water | 87% |
In methanol at 20℃; for 1h; Darkness; | 85% |
With ammonia In ethanol; water at 20℃; for 0.25h; pH=8; |
isopropyloxycarbonyloxymethyl iodide
diclofenac sodium
1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate
Conditions | Yield |
---|---|
Stage #1: diclofenac sodium With sodium carbonate In N,N-dimethyl acetamide at 30℃; for 0.166667h; Inert atmosphere; Stage #2: isopropyloxycarbonyloxymethyl iodide In N,N-dimethyl acetamide at -10℃; for 0.75h; Inert atmosphere; | 86.4% |
Conditions | Yield |
---|---|
In chloroform byproducts: sodium chloride; under inert atmosphere; 1 equiv. of sodium salt of ligand refluxed withSn compd. in dry CHCl3 for 6-7 h; cooled to room temp.; filtered; solvent removed from filtrate by rotary evaporator; crystd. from CH2Cl2-hexane; elem. anal.; | 86% |
1-(2-aminoethyl)pyrrolidine
diclofenac sodium
[Ni(diclofenac)2(1-(2-aminoethyl)pyrrolidine)2]
Conditions | Yield |
---|---|
Stage #1: nickel(II) chloride hexahydrate; diclofenac sodium In ethanol at 50℃; Stage #2: 1-(2-aminoethyl)pyrrolidine In ethanol at 20℃; | 86% |
Conditions | Yield |
---|---|
In water at 20℃; for 3h; | 86% |
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