Indium chloride Chemical Properties Melting point 262 °C (dec.)(lit.) Boiling point 300°C density 3.46 g/mL at 25 °C(lit.) Fp 300°C subl. storage temp. Inert atmosphere,Room Temperature form powder color Wh
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Indium chloride Melting point 262 °C (dec.) (lit.) Boiling point 300°C Density 3.46 g/mL at 25 °C (lit.) Flash point 300°C subl. Morphology Color White to off-white Water soluble reacts Sensitivity Hygroscopic Merc
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Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; heating from 550 to 750°C; | |
In neat (no solvent) on In2O3 surface; not isolated, detd. by thermal desorption (20-650°C) and mass spectroscopy; |
Conditions | Yield |
---|---|
In neat (no solvent) 300°C;; | |
In neat (no solvent) 300°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) 300°C;; | |
In neat (no solvent) 300°C;; |
tetrachlorosilane
A
silica gel
B
indium(III) chloride
Conditions | Yield |
---|---|
780-800°C in vac.; Two-fold vacuum sublimation with prior distilling off SiCl4.; |
Conditions | Yield |
---|---|
450°C;; | |
In neat (no solvent) chlorination of In2O3 with CCl4 at ca 450°C; | |
In not given react. of In2O3 with CCl4; |
Conditions | Yield |
---|---|
In gas Kinetics; flow method (600 - 800°C, 5 - 50 vol.% SnCl4, 20 - 120 min); |
Conditions | Yield |
---|---|
With tin(IV) chloride In neat (no solvent) byproducts: O2; chlorination of equimolar mixt. of In2O3 by Cl2/SnCl4 mixt. (4 vol % SnCl4, const. temp. in range 550-700°C, 60 min); chem. anal.; |
Conditions | Yield |
---|---|
With pyrographite heating in dry flow of Cl2; | |
In neat (no solvent) Kinetics; byproducts: O2; heating to 700°C; |
Conditions | Yield |
---|---|
Cl2/Ar mixt. flowing over In2O3 (const. temp. in range 500-700°C,gas flow rate 2ml/min, complete satn. of carrier gas by vapours of gase ous products, duration 3 h); monitoring by gravimetric and chem. anal.; |
chlorine
A
In2Cl6
B
indium(III) chloride
C
tin(IV) chloride
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; byproducts: O2; chlorination of equimolar mixt. of In2O3/SnO2 at const. temp. in range 500-700°C (Cl2 flow 100 ml/min); chem. anal.; | |
With sulfur dioxide In neat (no solvent) Kinetics; byproducts: O2, SO3, In2(SO4)3; chlorination of equimolar mixt. of In2O3/SnO2 at const. temp. in range 500-700°C (Cl2/SO2 flow 100 ml/min); chem. anal.; |
Conditions | Yield |
---|---|
reaction with nascent Cl; | |
reaction with nascent Cl; |
Conditions | Yield |
---|---|
With water starting with slightly wettened In without heating, then at 120 to 140°C, by adding more water; | |
byproducts: H2; wet HCl gas; | |
In hydrogenchloride prepn. by dissolving In in HCl according to S. V. Bleshinskii, V. F. Abramova, Chemistry of Indium (Akad. Nauk Kirg. SSR, Frunze, 1958); |
Conditions | Yield |
---|---|
in dry Cl2-flow; | |
Glowing to red heat, yellow-green flame.; | |
air removed by N2-flow, then reaction at 600°C in N2/Cl2-flow; |
InCl2(1+)
indium(III) chloride
Conditions | Yield |
---|---|
With lithium chloride In N,N-dimethyl-formamide Ar atmosphere, 25°C, ionic strength 1 M (LiClO4); not isolated; potentiometric monitoring (3 mass-% indium amalgam indicator electrode), estimation of stability const. of InCl3 in DMF; |
Conditions | Yield |
---|---|
In water In(OH)3 was dissolved in conc. HCl; evapd.; | |
In water drying (HCl(g) stream, 250°C), sublimation (500°C); |
indium(III) chloride
Conditions | Yield |
---|---|
With thionyl chloride In neat (no solvent) refluxing educt with dry SOCl2 for about 6 h; dried in vac. for about 2 h; |
indium(III) chloride
Conditions | Yield |
---|---|
With lithium chloride In N,N-dimethyl-formamide Ar atmosphere, 25°C, ionic strength 1 M (LiClO4); not isolated; potentiometric monitoring (3 mass-% indium amalgam indicator electrode), estimation of stability const. of InCl3 in DMF; |
Conditions | Yield |
---|---|
mild heating; sublimation in CO2-flow; | |
at 300-350°C in CO2-containing Cl2-flow, in few hours; | |
mild heating; sublimation in CO2-flow; |
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; byproducts: SO3; heating to from 550 to 750°C; |
indium(III) chloride
Conditions | Yield |
---|---|
With sulfur dioxide; chlorine Kinetics; byproducts: SO2; | |
With chlorine In solid Kinetics; byproducts: SO2, O2; at 128-800°C; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: O2; heating to above 800°C; |
water
C
indium(III) chloride
Conditions | Yield |
---|---|
In water reaction of an excess of InCl with aq. LiNO3 solns. 20°C; |
Conditions | Yield |
---|---|
In water reaction of an excess of InCl with aq. LiNO3 solns. 20°C; |
Conditions | Yield |
---|---|
In water reaction of an excess of InCl with aq. LiNO3 solns. 20°C; |
Conditions | Yield |
---|---|
In water reaction of an excess of InCl with aq. LiNO3 solns. 20°C; |
Conditions | Yield |
---|---|
In water reaction of an excess of InCl with aq. LiNO3 solns. 20°C; |
indium(III) chloride
Conditions | Yield |
---|---|
With hydrogenchloride byproducts: NH4Cl; |
Conditions | Yield |
---|---|
In neat (no solvent) mixt. of the starting materials heated in evacuated sealed quartz tubes to 500-900°C; decompn. of educts ocurrs, InCl3 sublimates off; | A 0% B n/a |
Conditions | Yield |
---|---|
With water | |
In water Kinetics; stirring of monohalide in H2O, disproportionation within several minutes at 20°C; products not isolated, detn. of In(III) in soln. after sepn. of solid phase (In); | |
With water | |
In dichloromethane disproportionation at temp. above -80°C; |
indium(III) chloride
Conditions | Yield |
---|---|
by strong heating; | |
by strong heating; |
Conditions | Yield |
---|---|
With water In hydrogenchloride formation of InCl3 and In from InCl and InCl2 in aq. HCl by addn. of H2O;; | |
With H2O In hydrogenchloride formation of InCl3 and In from InCl and InCl2 in aq. HCl by addn. of H2O;; |
Conditions | Yield |
---|---|
In diethyl ether; hexane under N2, stirring, 20 h, 25 °C; filtn.; | 100% |
In diethyl ether; hexane under N2, stirring, 20 h, 25 °C; evapn. (vac.); redissolving (hexane); extn. (refluxing, 2 h); evapn.; | 80% |
indium(III) chloride
diethylammonium N,N-diethyldiselenocarbamate
tris(diethyldiselenocarbamato)indium(III)
Conditions | Yield |
---|---|
In methanol; ethanol to a soln. of (Et2NH2)(Et2dsc) in methanol a soln. of InCl3 in ethanol is added (Ar); ppt. is sucked off, washed with water and ethanol and dried, dissolved in small amount chloroform, filtration of soln. in vac., crystn.; | 100% |
methyl methylphenylphosphinate
indium(III) chloride
Conditions | Yield |
---|---|
In further solvent(s) byproducts: MeCl; slow heating in neat Ph(Me)P(O)OMe until complete pptn.; particle size and polymerization degree depending on heating rate; | 100% |
nitrido(tetra-tert-butylphthalocyaninato)rhenium(V)
indium(III) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane; dichloromethane Re compd. dissolved in CH2Cl2/THF/hexane and cooled to -5°C, electrophile added dropwise to this soln., stirred for 6 h at -5°C; solvent removed at -5°C, elem. anal.; | 100% |
indium(III) chloride
Conditions | Yield |
---|---|
at 80℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With diethylamine In benzene N2; refluxed for 3h; molar ratio InCl3/ligand/base: 1/3.1/3.1;; recrystn. from dichloromethane-ethanol (1:1); elem. anal.;; | 99% |
With ethanol; sodium isocyanate In tetrahydrofuran N2; refluxed for 3h; molar ratio InCl3/ligand/base=3.1/3.1;; recrystn. from dichloromethane-ethanol (1:1); elem. anal.;; | 91% |
With sodium isocyanate In ethanol N2; refluxed for 3h; molar ratio InCl3/ligand/base: 1/3.1/3.1;; recrystn. from dichloromethane-ethanol (1:1); elem. anal.;; | 89% |
With NaOAc In ethanol; water addn. of ethanolic dibenzoylmethane with stirring to aq. InCl3 buffered with NaOAc; recrystn. (acetone); elem. anal.; |
potassium hydridotris(3,5-dimethylpyrazolyl)borate
indium(III) chloride
(tris(3,5-dimethyl-1-pyrazolyl)hydridoborate)InCl2
Conditions | Yield |
---|---|
In tetrahydrofuran stirring (18 h, room temp.), solvent removal (vacuum); extraction (CH2Cl2), recrystn. (MeCN); | 99% |
Conditions | Yield |
---|---|
With sodium isocyanate In ethanol byproducts: alkyl carbamate; refluxing for 3h; molar ratio of (acetylacetone)/InCl3=3.1-3.3 and (NaOCN)/(InCl3)=6.6-6.7;; | 99% |
With sodium isocyanate In methanol byproducts: alkyl carbamate; addn. of NaOCN (120mmol) and acetylacetone (120mmol) to a soln. of InCl3 (18.1mmol) in methanol (80ml) at room temp.; refluxing at 68°C for 3h; cooling; filtration;; washing solids with benzene; distn. (solvents, acetylacetone) under reduced pressure; addn. of benzene; filtration; concg. soln. under reduced pressure; heating solid at 60-70°C in vac. for 1-2h; recrystn. from ethanol;; | 98.6% |
With sodium isocyanate In tetrahydrofuran refluxing for 3h; molar ratio of (acetylacetone)/InCl3=3.1-3.3 and (NaOCN)/(InCl3)=6.6-6.7;; | 91% |
Conditions | Yield |
---|---|
In benzene molar ratio In/Si: 1:3, N2 atmosphere, refluxed, 6 h, pptn.; ppt. extd. with ether, washed with pentane, dried in vacuum, elem. anal.; | 99% |
Conditions | Yield |
---|---|
In benzene byproducts: (CH3)3SiCl; molar ratio In/Si: 1:2, N2 atmosphere, refluxed, 6 h, pptn.; ppt. extd. with ether, washed with pentane, dried in vacuum, elem. anal.; | 99% |
In benzene byproducts: (CH3)3SiCl; molar ratio In/Si: 1:1, N2 atmosphere, refluxed, 6 h, pptn.; ppt. extd. with ether, washed with pentane, dried in vacuum, elem. anal.; | 46% |
indium(III) chloride
Conditions | Yield |
---|---|
In methanol; dichloromethane; acetone | 99% |
Conditions | Yield |
---|---|
In diethyl ether; hexane byproducts: Me3SiCl; N2-atmosphere; dropwise addn. of stoic. mixt. of metal salts (in ether) to Me3SiCN (in hexane), stirring for 12 h; collection (filtration), heating in hexane (several h), washing (hexane); | 99% |
(2S)-methylbuthyl-1-magnesium bromide
indium(III) chloride
Conditions | Yield |
---|---|
In diethyl ether inert atmosphere; slow addn. of 2 equiv. of Mg-compd. to InCl3 suspn. at0°C, stirring overnight; solvent removal (vac.), extn. into pentane, filtration, solvent removal (vac.); | 99% |
indium(III) chloride
indium(III) N-methylpiperazine dithiocarbamate
Conditions | Yield |
---|---|
In methanol to a soln. of metal salt added slowly a soln. of S compd., stirred for 3h; solvent removed (vac.), extrd. (CH2Cl2), filtered (G-3), evapd. (vac.); elem. anal., IR; | 99% |
methanol
indium(III) chloride
Conditions | Yield |
---|---|
In methanol addn. of Zn compd. in MeOH to InCl3, heating under reflux for 2 h or stirring overnight; | 99% |
In methanol addn. of Zn compd. in MeOH to InCl3, heating under reflux for 6 h; cooling to room temp., filtration, washing with Et2O, drying under vacuum, elem. anal.; | 27% |
indium(III) chloride
Conditions | Yield |
---|---|
In methanol addn. of Zn compd. in MeOH to InCl3, heating under reflux for 2 h or stirring overnight; | 99% |
In methanol addn. of Zn compd. in MeOH to InCl3, heating under reflux for 6 h; cooling to room temp., filtration, washing with Et2O, drying under vacuum, elem. anal.; | 62% |
indium(III) chloride
acetonitrile
Conditions | Yield |
---|---|
In acetonitrile byproducts: KCl; CH3CN added to metal complex, sealed in a glass ampule, kept at 100°C for 3-4 d, filtered (Ar), treated with excess of InCl3, sealed, heated at 100°C for 12 h; evapd. slowly; | 99% |
2,2':6,2''-terpyridine
indium(III) chloride
(2,2',2''-terpyridine)In(N3)3
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene byproducts: NaCl; Ar-atmosphere; stoich. amts.; treatment of InCl3 (in PhMe) with terpy and then with NaN3 (in THF), refluxing for 5 h; filtration off of NaCl, cooling to -30°C (pptn.); | 98.4% |
Conditions | Yield |
---|---|
In toluene a soln. of tribenzylindane and InCl3 (ratio 1:2) in toluene is heated under reflux for 8 h, cooling to room temp. (under Ar); filtn. of residue, drying in vac., elem. anal.; | 98% |
In benzene N2 atmosphere, dry and degassed solvent, addn. of In-compd. in benzene to SnCl3, refluxing (5 h), pptn. on cooling; filtration, drying in vac.; | 90% |
Conditions | Yield |
---|---|
In toluene addn. of InCl3 to soln. of iPr3In, stirring, 6h, 80°C, filtration, washed with toluene (8x), evapn. in vac., under Ar; elem. anal.; | 97% |
sodium N-morpholinocarbamodithioate
indium(III) chloride
(O(C2H4)S)2indium(III) morpholine dithiocarbamate
Conditions | Yield |
---|---|
In benzene anhydrous condns.; a soln. of metal salt and thiolate stirred for 3 h inbenzole, a metal compd. treated with carbamate, stirred for 3 h at room temp.; filtered, solvent removed (vac.); elem. anal., IR; | 97% |
Conditions | Yield |
---|---|
In neat (no solvent) (Ar); Schlenk techniques; InCl3 dissolved in Me2Se at 0°C; stirred for 1 h at room temp.; crystd. by slow diffusion of pentane; elem. anal.; | 97% |
Conditions | Yield |
---|---|
In benzene byproducts: (CH3)3SiCl; molar ratio In/Si: 1:2, N2 atmosphere, refluxed, 6 h, pptn.; ppt. extd. with ether, washed with pentane, dried in vacuum, elem. anal.; | 96% |
In benzene byproducts: (CH3)3SiCl; molar ratio In/Si: 1:1, N2 atmosphere, refluxed, 6 h, pptn.; ppt. extd. with ether, washed with pentane, dried in vacuum, elem. anal.; | 25% |
sodium acetate
indium(III) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: KCl, NaCl; N2 atmosphere; stirring (room temp., 5 h); evapn. of solvent (vac.), extn. (benzene), filtration, removal of solvent (vac); elem. anal.; | 96% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In hydrogenchloride In-compd. addn. to soln. of complex, Ar atmosphere, borohydride addn. inportions, dilution by aq. HCl, sepn. on cation-exchange column (Dowex); | 96% |
sodium N,N'-diisopropyldithiocarbamate
indium(III) chloride
chlorobis(diisopropyldithiocarbamato)indium(III)
Conditions | Yield |
---|---|
In methanol byproducts: NaCl; (N2); stirring (ca. 30°C, 3-4 h); evapn., extn. (CHCl3), filtration, removal of solvent (reduced pressure), crystn. (CH2Cl2/hexane); elem. anal.; | 96% |
potassium 1,2-cyclobutane-3,4-dithiolate
indium(III) chloride
benzyltrimethylammonium chloride
Conditions | Yield |
---|---|
In water 3-3 equiv. of K-salt and N-compd. were dissolved in H2O, 1 equiv. of InCl3 was slowly added in H2O; ppt. was filtered off, dried in an exsiccator, elem. anal.; | 96% |
indium(III) chloride
Conditions | Yield |
---|---|
In diethyl ether byproducts: LiCl, Me2Si(NHMe)2; addn. of the Li compd. in Et2O to a slurry of InCl3 in Et2O at room temp., stirring (24 h); removal of ether (vac. distn.), drying (24 h), extraction (hexane), filtration (Celite), removal of hexane (vac.); crystals may be obtained by dissoln. of the solid in hexane/Et2O (1:9) and cooling 24 h at -35°C; elem. anal.; | 96% |
3-diethylamino-propan-1-ol
indium(III) chloride
Conditions | Yield |
---|---|
In dichloromethane (N2); ligand added to a suspn. of InCl3, stirred for 12 h; added to stirring pentane, filtered, dried (vac.); | 96% |
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