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inquirybest price high quality 1,1,2-Trichlorotrifluoroethane Basic information Product Name: 1,1,2-Trichlorotrifluoroethane Synonyms: 1,1,2-Trichlor-1,2,2-trifluorethan;1,1,2-trichloro-1,2,2
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryTop purity 1,1,2-Trichlorotrifluoroethane GR for analysis with high quality cas:76-13-1 Application:Top purity 1,1,2-Trichlorotrifluoroethane GR for analysis with high quality cas:76-13-1
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inquiryTop purity 1,1,2-Trichlorotrifluoroethane GR for analysis with high quality cas:76-13-1Appearance:Colorless transparent liquid Storage:Rom tep. Package:25kg net/paper drum Application:used Transportation:By express (Door to door) such as FEDEX, DHL,
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inquiryOur Services 1.Certificate Of Analysis (COA) 2.Material Safety Data Sheet (MSDS) 3.Route of synthesis (ROS) 4.Method of Aanlysis (MOA) 5.Nuclear Magnetic Resonance (NMR) 6.Packing pictures and loading video before loading 7.Free Sampl
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inquirysub/micron to mesh powders (near/spheres, whiskers, flake, fiber, porous) and grain/ball, thin/ thick metal / alloys pieces / parts, thin and thick (particle) film materials /target, and custom-made crystals, substrates/parts. In the industries and a
ProName: 1,1,2-Trichlorotrifluoroethane high qu...CasNo: 76-13-1 Molecular Formula: C2Cl3F3 Appearance: colourless liquid Application: ORGANIC chemicals DeliveryTime: Within 15 workdays after payment PackAge: according to the clients
Best quality & Attractive price & Professional service; Trial & Pilot & CommercialHenan Fine Chemicals Co., LTD. is a diversified technology - oriented integrated company, which mainly concentrates on fine chemicals. Our company is committed to becom
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inquiryplease contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant informationAppearance:Colorless liquid Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated pl
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inquiryThe system can just identify the products information in first sheet, it is not be permitted to add or edit new sheet by userself.Our products are required in MG to Gram only. · Pharmaceutical Reference Standards· Traceable workin
Shanghai AngewChemCo., Ltd. is an innovative enterprise on fine chemicals and pharmaceuticals. Based on Shanghai R&D center and Hunan chemical manufacturing plant, we offer chemical research, process development, and large-scale production. Complete
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inquiry1,1,2-Trichlorotrifluoroethane Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
Top purity 1,1,2-Trichlorotrifluoroethane GR for analysis with high quality cas:76-13-1 Application:used
Conditions | Yield |
---|---|
With aluminum(III) fluoride; hydrogen fluoride at 120℃; under 11251.1 Torr; for 10h; Reagent/catalyst; Temperature; Autoclave; | 97.06% |
With CFC-112a; antimonypentachloride; fluorine at 32℃; unter vermindertem Druck; | |
With antimonypentachloride; antimony(III) fluoride at 48℃; |
1,2,2-trifluorodichloroethanesulfonyl chloride
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
sulfur dioxide
Conditions | Yield |
---|---|
200°C, 7 days; | A 97% B 97% |
100°C, 7 days; | A 19% B 18% |
Conditions | Yield |
---|---|
With benzophenone; chlorine at -80℃; | 92% |
Conditions | Yield |
---|---|
With bromine trifluoride; antimonypentachloride In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20 - 25℃; | 90% |
With chromium(III) oxyfluoride; hydrogen fluoride at 500℃; |
Chlorotrifluoroethylene
chloro(trifluoromethyl)disulfane
A
2,2-dichlorotrifluoroethyl(trifluoromethyl)disulfane
B
1,1,2-Trichloro-1,2,2-trifluoroethane
C
bis(trifluoromethyl)tetrasulfide
D
1,2-dichlorotrifluoroethyl(trifluoromethyl)disulfane
Conditions | Yield |
---|---|
Irradiation (UV/VIS); | A n/a B n/a C n/a D 80% |
Irradiation (UV/VIS); | A n/a B n/a C n/a D 80% |
Conditions | Yield |
---|---|
With iodine at 140 - 165℃; for 4h; | A n/a B 63% |
Trichloroethylene
A
1,2,2-trichloro-1,2-difluoroethane
B
1,1,2-Trichloro-1,2,2-trifluoroethane
Conditions | Yield |
---|---|
With hydrogen fluoride; fluorine In trichlorofluoromethane at -70℃; for 4h; Product distribution / selectivity; Inert atmosphere; | A 50% B 18% |
Chlorotrifluoroethylene
sulfur bis(trifluoromethyl)amide chloride
A
2,4-dichlorohexafluorothiolane
B
1,1,2-Trichloro-1,2,2-trifluoroethane
C
N,N-bistrifluoromethyl-2,2-dichlorotrifluoroethanesulfenamide
Conditions | Yield |
---|---|
for 528h; Irradiation; Further byproducts given; | A 11% B 16% C 31% D 31% |
Chlorotrifluoroethylene
sulfur bis(trifluoromethyl)amide chloride
A
1,1,3,4-Tetrachlorohexafluorobutane
B
1,1,2-Trichloro-1,2,2-trifluoroethane
C
N,N-bistrifluoromethyl-2,2-dichlorotrifluoroethanesulfenamide
Conditions | Yield |
---|---|
for 528h; Irradiation; Further byproducts given; | A 6.5% B 16% C 31% D 31% |
Chlorotrifluoroethylene
sulfur bis(trifluoromethyl)amide chloride
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
sulfur bis{bis(trifluoromethyl)amide}
C
N,N-bistrifluoromethyl-2,2-dichlorotrifluoroethanesulfenamide
Conditions | Yield |
---|---|
for 528h; Irradiation; Further byproducts given; | A 16% B 15% C 31% D 31% |
Chlorotrifluoroethylene
sulfur bis(trifluoromethyl)amide chloride
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
N,N-bistrifluoromethyl-2,2-dichlorotrifluoroethanesulfenamide
Conditions | Yield |
---|---|
for 528h; Irradiation; Further byproducts given; | A 16% B 31% C 31% D 4% |
Chlorotrifluoroethylene
sulfur bis(trifluoromethyl)amide chloride
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
disulfur bis{bis(trifluoromethyl)amide}
C
N,N-bistrifluoromethyl-2,2-dichlorotrifluoroethanesulfenamide
Conditions | Yield |
---|---|
for 528h; Irradiation; Further byproducts given; | A 11% B 12% C 26% D 26% |
Chlorotrifluoroethylene
α-chlorocarbonylhexafluoroisopropylsulfenyl chloride
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
bis-(α-chlorocarbonylhexafluoroisopropyl) disulfide
Conditions | Yield |
---|---|
at 150 - 160℃; for 10h; | A n/a B n/a C 21% |
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride at 75 - 100℃; | |
With antimony (III)-antimony (V)-fluoro chloride ene; hydrogen fluoride; chlorine at 160 - 165℃; unter Druck; | |
With zirconium(IV) fluoride; hydrogen fluoride at 350 - 360℃; |
1,1-difluorotetrachloroethane
A
1,1,1-Trichloro-2,2,2-trifluoroethane
B
1,1,2-Trichloro-1,2,2-trifluoroethane
Conditions | Yield |
---|---|
With hydrogen fluoride; pyrographite; lithium fluoride at 375 - 550℃; |
1,1,1,2-tetrachoroethane
A
1,2-dichloro-1,1,2,2-tetrafluoroethane
B
1,1,2-Trichloro-1,2,2-trifluoroethane
Conditions | Yield |
---|---|
With antimony (III)-antimony (V)-fluoro chloride; hydrogen fluoride; chlorine at 160 - 165℃; unter Druck; | |
With antimony (III)-antimony (V)-fluoro chloride; hydrogen fluoride; chlorine at 160 - 165℃; unter Druck; | |
With antimony (III)-antimony (V)-fluoro chloride; hydrogen fluoride; chlorine at 160 - 165℃; unter Druck; |
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride at 125℃; |
Conditions | Yield |
---|---|
With nitrogen; copper; fluorine at 70℃; |
Conditions | Yield |
---|---|
With hydrogen fluoride; antimonypentachloride at 125℃; |
hexachloroethane
A
1,2-dichloro-1,1,2,2-tetrafluoroethane
B
1,1,2-Trichloro-1,2,2-trifluoroethane
Conditions | Yield |
---|---|
With antimony (III)-antimony (V)-fluoro chloride; hydrogen fluoride; chlorine at 160 - 165℃; unter Druck; | |
With antimony (III)-antimony (V)-fluoro chloride; hydrogen fluoride; chlorine at 160 - 165℃; unter Druck; | |
With antimony (III)-antimony (V)-fluoro chloride; hydrogen fluoride; chlorine at 160 - 165℃; unter Druck; |
Conditions | Yield |
---|---|
With fluorine at 0℃; | |
With sulfur tetrafluoride; hydrogen fluoride; chlorine at 20℃; for 10h; Yield given; |
Trichloroethylene
A
1,2-dichloro-1,2,2-trifluoroethane
B
1,1-dichloro-1,2,2-trifluoroethane
C
1,2,2-trichloro-1,2-difluoroethane
D
1,1,2-Trichloro-1,2,2-trifluoroethane
Conditions | Yield |
---|---|
With manganese(III) fluoride at 120℃; | |
With manganese(III) fluoride at 220℃; |
Trichloroethylene
A
1,2-dichloro-1,2,2-trifluoroethane
B
1,2,2-trichloro-1,2-difluoroethane
C
1,1,2-Trichloro-1,2,2-trifluoroethane
D
CFC-112a
Conditions | Yield |
---|---|
With cobalt (III) fluoride at 120℃; Further byproducts given; |
Trichloroethylene
A
1,1,1-trifluoro-2-chloroethane
B
1,2,2-trichloro-1,2-difluoroethane
C
1,1,2-Trichloro-1,2,2-trifluoroethane
D
CFC-112a
Conditions | Yield |
---|---|
With cobalt (III) fluoride at 120℃; Further byproducts given; |
Trichloroethylene
A
1,1-dichloro-1,2,2-trifluoroethane
B
1,2,2-trichloro-1,2-difluoroethane
C
1,1,2-Trichloro-1,2,2-trifluoroethane
D
CFC-112a
Conditions | Yield |
---|---|
With cobalt (III) fluoride at 120℃; Further byproducts given; |
Chlorotrifluoroethylene
A
1,2-Dinitro-1-chlortrifluoraethan
B
1,1,2-Trichloro-1,2,2-trifluoroethane
C
chlorodifluoroacetyl fluoride
D
1,2-dichloro-1,2,2-trifluoronitrosoethane
Conditions | Yield |
---|---|
With nitrogen(II) oxide; iron(III) chloride Further byproducts given; |
Chlorotrifluoroethylene
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
1,2-dichloro-1,2,2-trifluoro-1-iodoethane
C
1,1-Dichloro-2-iodotrifluoroethane
Conditions | Yield |
---|---|
With Iodine monochloride |
Chlorotrifluoroethylene
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
chlorodifluoroacetyl fluoride
C
1,2-dichloro-1,2,2-trifluoronitrosoethane
Conditions | Yield |
---|---|
With nitrogen(II) oxide; iron(III) chloride |
Chlorotrifluoroethylene
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
chlorodifluoroacetyl fluoride
C
1,2-dichloro-1,2,2-trifluoronitrosoethane
D
2-nitro-1,1-dichlorotrifluoroethane
Conditions | Yield |
---|---|
With nitrogen(II) oxide; iron(III) chloride Further byproducts given; |
Chlorotrifluoroethylene
A
1,1,2-Trichloro-1,2,2-trifluoroethane
B
chlorodifluoroacetyl fluoride
C
1,2-dichloro-1,2,2-trifluoronitrosoethane
D
1-chloro-1,2,2-trifluoro-2-nitro-1-nitroso-ethane
Conditions | Yield |
---|---|
With nitrogen(II) oxide; iron(III) chloride Further byproducts given; |
Conditions | Yield |
---|---|
With potassium zinc trihydride at 250 - 320℃; under 7500.75 Torr; for 5h; Temperature; Pressure; Inert atmosphere; Large scale; | 99.22% |
With ammonium chloride; zinc(II) chloride In methanol; water electrochemical process; | 90% |
With zinc(II) chloride; zinc In ethanol at 50℃; for 3h; Dehalogenation; | 75% |
1,1,2-Trichloro-1,2,2-trifluoroethane
1,3,3,3-tetrafluoro-1-methoxy-2-trifluoromethyl-propene
Conditions | Yield |
---|---|
at 120℃; for 2.5h; | 98% |
1,1,2-Trichloro-1,2,2-trifluoroethane
malononitrile
dimethyl 1,3-propanediimidate dihydrochloride
Conditions | Yield |
---|---|
In hydrogenchloride; methanol | 96% |
1,1,2-Trichloro-1,2,2-trifluoroethane
A
1,2-dichloro-1,2,2-trifluoroethane
B
Chlorotrifluoroethylene
C
1,1,2-trifluoroethylene
Conditions | Yield |
---|---|
With hydrogen; silica gel; nickel at 450℃; under 760 Torr; Title compound not separated from byproducts; | A n/a B 95.8% C n/a |
bismuth(III) chloride; silica gel; palladium at 250℃; Yield given. Yields of byproduct given; | |
With hydrogen; silica gel; nickel at 450℃; under 760 Torr; Product distribution; other supported Ni catalysts and metal oxides; | |
bismuth(III) chloride; silica gel; palladium at 250℃; under 760 Torr; Product distribution; other catalysts and modifier; variation of condition: selectivity; |
1-Heptene
1,1,2-Trichloro-1,2,2-trifluoroethane
1,1-Dichloro-1,2,2-trifluoro-nonane
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; sodium formate In N,N-dimethyl-formamide at 40℃; for 4h; | 88.5% |
1-hexene
1,1,2-Trichloro-1,2,2-trifluoroethane
1,1-Dichloro-1,2,2-trifluoro-octane
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; sodium formate In N,N-dimethyl-formamide at 40℃; for 3h; other alkenes and alkynes; | 86.5% |
With ammonium peroxydisulfate; sodium formate In N,N-dimethyl-formamide at 40℃; for 3h; | 86.5% |
1,1,2-Trichloro-1,2,2-trifluoroethane
sodium thiophenolate
A
2-chloro-1,1,2-trifluoro-1-(phenyl thio) ethane
B
<(2,2-dichloro-1,1,2-trifluoroethyl)thio>benzene
C
diphenyldisulfane
Conditions | Yield |
---|---|
In dimethyl sulfoxide for 0.5h; Product distribution; Mechanism; Ambient temperature; various per(chloro,fluoro)ethanes and conditions; | A 0.9 % Chromat. B 86% C 3 % Chromat. |
In dimethyl sulfoxide for 0.5h; Ambient temperature; | A 0.9 % Chromat. B 86% C 3 % Chromat. |
In water; dimethyl sulfoxide for 48h; Ambient temperature; | A 18 % Chromat. B 16 % Chromat. C 38 % Chromat. |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 30 - 35℃; for 0.833333h; | 84% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 40 - 45℃; for 0.5h; | 81% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 45 - 50℃; for 0.5h; | 81% |
Conditions | Yield |
---|---|
With ammonium persulfate; ammonium formate In N,N-dimethyl-formamide at 30 - 40℃; | 80% |
With ammonium persulfate; ammonium formate In N,N-dimethyl-formamide at 30 - 40℃; Product distribution; Mechanism; also with further polyhalofluoroalkanes; | 80% |
Irradiation; | |
With water; sodium formate; titanium(IV) oxide Mechanism; Ambient temperature; Irradiation; |
1,1,2-Trichloro-1,2,2-trifluoroethane
cyclohexene
(2,2-Dichloro-1,1,2-trifluoro-ethyl)-cyclohexane
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; sodium formate In N,N-dimethyl-formamide at 50℃; for 8h; | 79.5% |
1,1,2-Trichloro-1,2,2-trifluoroethane
potassium phenolate
A
1-hydro-1-chloro-2-phenoxyperfluoroethane
B
<(2,2-dichloro-1,1,2-trifluoroethyl)oxy>benzene
Conditions | Yield |
---|---|
In dimethyl sulfoxide for 1h; Ambient temperature; Yields of byproduct given; | A n/a B 79% |
In dimethyl sulfoxide for 4h; | A 9% B 37% |
1,1,2-Trichloro-1,2,2-trifluoroethane
Allyl acetate
Acetic acid 5,5-dichloro-4,4,5-trifluoro-pentyl ester
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; sodium formate In N,N-dimethyl-formamide at 40℃; for 2h; | 78.4% |
1,1,2-Trichloro-1,2,2-trifluoroethane
A
Hexafluoroethane
B
Chloropentafluoroethane
C
1,2-dichloro-1,1,2,2-tetrafluoroethane
Conditions | Yield |
---|---|
With chromium fluoride; magnesium fluoride; hydrogen fluoride at 250 - 500℃; Product distribution; | A 3% B 78% C 19% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 40 - 45℃; for 0.666667h; | 78% |
2,4-Bis(methylthio)pyrimidine
1,1,2-Trichloro-1,2,2-trifluoroethane
4-chloro-2,6-bis(methylthio)pyrimidine
Conditions | Yield |
---|---|
Stage #1: 2,4-Bis(methylthio)pyrimidine With bis(2,2,6,6-tetramethylpiperidin-1-yl)magnesium-bis(lithium chloride) complex In tetrahydrofuran at -20℃; for 1h; Inert atmosphere; Stage #2: 1,1,2-Trichloro-1,2,2-trifluoroethane In tetrahydrofuran at -35 - -20℃; for 3h; Inert atmosphere; regioselective reaction; | 78% |
Conditions | Yield |
---|---|
With bis(fluorosulfuryl) peroxide; antimony pentafluoride; fluorosulphonic acid at 20 - 30℃; for 0.5h; | A 75.4% B n/a |
1,1,2-Trichloro-1,2,2-trifluoroethane
potassium 2-methylbutan-2-olate
B
2-(2,2-Dichloro-1,1,2-trifluoro-ethoxy)-2-methyl-butane
Conditions | Yield |
---|---|
In various solvent(s) for 1h; Ambient temperature; Yields of byproduct given; | A n/a B 75% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 50 - 55℃; for 0.5h; | 75% |
Conditions | Yield |
---|---|
With sodium dithionite; sodium hydrogencarbonate In dimethyl sulfoxide at 60℃; for 6h; | 74% |
With sodium dithionite; water; sodium hydrogencarbonate In acetonitrile at 40 - 45℃; for 20h; | 56% |
With sodium dithionite; sodium hydrogencarbonate In acetonitrile at 40 - 45℃; for 20h; | 56% |
1,1,2-Trichloro-1,2,2-trifluoroethane
1-benzyl-3-hydroxy-1H-indazole
1-benzyl-3-(2,2-dichloro-1,1,2-trifluoroethoxy)-1H-indazole
Conditions | Yield |
---|---|
Stage #1: 1-benzyl-3-hydroxy-1H-indazole With potassium tert-butylate In tert-butyl alcohol at 20℃; for 2h; Stage #2: 1,1,2-Trichloro-1,2,2-trifluoroethane In N,N-dimethyl-formamide at 100℃; for 48h; | 74% |
1,1,2-Trichloro-1,2,2-trifluoroethane
1,7-Octadiene
10,10-Dichloro-9,9,10-trifluoro-dec-1-ene
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; sodium formate In N,N-dimethyl-formamide at 45℃; for 4h; | 72.5% |
NH-pyrazole
1,1,2-Trichloro-1,2,2-trifluoroethane
1-(2,2-dichlorotrifluoroethyl)pyrazole
Conditions | Yield |
---|---|
With sodium hydride; tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 50 - 55℃; for 2h; | 72% |
tetramethylorthosilicate
1,1,2-Trichloro-1,2,2-trifluoroethane
p-trifluoromethylphenyl bromide
trimethoxy(4-(trifluoromethyl)phenyl)silane
Conditions | Yield |
---|---|
With n-butyllithium In diethyl ether; hexane | 72% |
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