CAS No.75-88-7,2-Chloro-1,1,1-trifluoroethane Suppliers

Dayang Chem (Hangzhou) Co.,Ltd.

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2-chloro-1,1,1-trifluoroethane

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Aecochem Corp.

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Hangzhou Yierdechem Co. Ltd

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2-Chloro-1,1,1-trifluoroethane Application:2026602

2-Chloro-1,1,1-trifluoroethane

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Weihai Moochun Bio-Tech Co., Ltd.

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NovaChemistry

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Synthetic route

: 79-01-6
Trichloroethylene

: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
With hydrogen fluoride; antimony pentafluoride at 100℃; for 1h; Temperature; Autoclave;	97%
With hydrogen fluoride; tantalum pentafluoride at 0 - 140℃; under 25858.1 Torr; for 10.5h; Product distribution / selectivity; Neat (no solvent);	90%
With hydrogen fluoride; tantalum pentafluoride at 100 - 140℃; under 25858.1 Torr; for 6h;	80%

: 79-34-5
1,1,2,2-tetrachloroethane

: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
With hydrogen fluoride; antimonypentachloride at 80 - 90℃; Autoclave;	92.3%
With hydrogen fluoride; antimonypentachloride; chlorine at 120℃;

: 1649-08-7
1,2-dichloro-1,1-difluoroethane

: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
With 1,1,2-trichloro-1-fluoroethane; hydrogen fluoride; tantalum pentachloride at 0 - 140℃; for 2h; Product distribution / selectivity; Neat (no solvent);	87.5%
With hydrogen fluoride; tantalum pentachloride at 0 - 140℃; for 2.5h; Product distribution / selectivity; Neat (no solvent);	22%
With antimony dichloride trifluoride; hydrogen fluoride at 144℃; under 33097.9 Torr;

: 75-89-8
2,2,2-trifluoroethanol

: 421-83-0
trifluoromethane sulfonyl chloride

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 333-36-8
1,1,1-trifluoro-2-(2,2,2-trifluoroethoxy)ethane

C: 6226-25-1
2,2,2-trifluoroethyl trifluoromethanesulphonate

Conditions

Conditions	Yield
With potassium carbonate; tetra-n-propylammonium bromide In water at 10.2 - 23.3℃; for 4 - 7h; Product distribution / selectivity;	A 0.2 %Chromat. B 0.13 - 0.28 %Chromat. C 82%

...Expand

: 354-58-5
1,1,1-Trichloro-2,2,2-trifluoroethane

: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
With ammonium persulfate; ammonium formate In N,N-dimethyl-formamide at 30 - 40℃;	77%

: 811-95-0
1,1,2-trichloro-1-fluoroethane

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 1649-08-7
1,2-dichloro-1,1-difluoroethane

Conditions

Conditions	Yield
With hydrogen fluoride; tantalum pentachloride at 110℃; for 1.5h;	A 22% B 74%

: 306-83-2
1,1,1-trifluoro-2,2-dichloroethane

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 359-10-4
1-Chloro-2,2-difluoroethene

Conditions

Conditions	Yield
With water; zinc unter Zusatz eines Netzmittels;

: 359-10-4
1-Chloro-2,2-difluoroethene

: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
With aluminum(III) fluoride; hydrogen fluoride at 300℃;
With hydrogen fluoride; boron trifluoride at 25℃;

: 79-01-6
Trichloroethylene

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 354-15-4
1,2,2-trichloro-1,2-difluoroethane

C: 76-13-1
1,1,2-Trichloro-1,2,2-trifluoroethane

D: 76-12-0
CFC-112a

Conditions

Conditions	Yield
With cobalt (III) fluoride at 120℃; Further byproducts given;

...Expand

: 79-11-8
chloroacetic acid

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 38217-12-8
bis-(2-chloro-1,1-difluoro-ethyl) ether

Conditions

Conditions	Yield
With sulfur tetrafluoride at 65℃; for 3h;

: 593-71-5
Chloroiodomethane

: 2314-97-8
iodotrifluoromethane

: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
Ambient temperature; Irradiation; Hg2I2, Hg;

: 75-38-7
Vinylidene fluoride

: 22082-78-6
trifluoromethyl hypochlorite

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 25957-33-9
Trifluormethyl-1,1-difluor-2-chloraethylaether

Conditions

Conditions	Yield
In trichlorofluoromethane at -111 - 22℃; for 20h; Product distribution; various temperatures, olefins, solvents and times;	A 50 % Spectr. B 50 % Spectr.
In trichlorofluoromethane at -111 - 22℃; for 20h; Yield given. Title compound not separated from byproducts;

...Expand

: 75-38-7
Vinylidene fluoride

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 25957-33-9
Trifluormethyl-1,1-difluor-2-chloraethylaether

Conditions

Conditions	Yield
With trifluoromethyl hypochlorite In trichlorofluoromethane at -111 - 22℃; for 20h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

: 79-01-6
Trichloroethylene

A: 811-97-2
1,1,1,2-tetrafluoroethane

B: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
With hydrogen fluoride; chromium(III) oxide at 250℃; Mechanism; Product distribution; hydrofluorination, chlorine/fluorine exchange mechanism; effect of DF substitution for HF;	A 10 % Chromat. B 90 % Chromat.
With chromium(III) oxide; hydrogen fluoride at 653℃; for 18h; Product distribution; Further Variations:; Temperatures; Fluorination; Addition; Substitution;
With chromium fluoride; magnesium fluoride; hydrogen fluoride at 200℃; under 7600 Torr; Product distribution; Further Variations:; Pressures;

: 151-67-7
1,1,1-trifluoro-2-bromo-2-chloroethane

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 359-10-4
1-Chloro-2,2-difluoroethene

Conditions

Conditions	Yield
With perchloric acid; CoW7-; sodium perchlorate In water; acetonitrile at 20℃; Rate constant; Product distribution; pH 7; reaction with Co(II)sepuchrate2- at 50 deg C; electron transfer reactions of polyhaloalkanes with Co(II)W12O407- and Co(II)sepulchrate2+, order of reactivity toward Co(II)W12O407-, trapping experiments with N-t-butyl-α-phenylnitrone;
With liver microsomes Enzyme kinetics; Enzymatic reaction;

: 28760-99-8
1,1,1-trifluoro-2-chloroethyl radical

: 75-88-7
1,1,1-trifluoro-2-chloroethane

Conditions

Conditions	Yield
With isopropyl alcohol

: 58911-30-1
3-chloro-3-(trifluoromethyl)diazirine

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 79-38-9
Chlorotrifluoroethylene

Conditions

Conditions	Yield
Irradiation;
Irradiation; radiation > 300 nm;

: 354-58-5
1,1,1-Trichloro-2,2,2-trifluoroethane

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 306-83-2
1,1,1-trifluoro-2,2-dichloroethane

Conditions

Conditions	Yield
With hydrogen; RhCl(PPh3)3 In tetrahydrofuran at 100℃; under 6080 Torr; for 5h; Product distribution; further catalysts and times; effect of bases;	A 3.5 % Chromat. B 94.6 % Chromat.
With hydrogen; RhCl(PPh3)3 In tetrahydrofuran at 100℃; under 6080 Torr; for 5h;	A 3.5 % Chromat. B 94.6 % Chromat.

: 306-83-2
1,1,1-trifluoro-2,2-dichloroethane

: 100-52-7
benzaldehyde

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 359-10-4
1-Chloro-2,2-difluoroethene

C: 67230-92-6
2-chloro-3,3-difluoro-1-phenyl-2-propenol

D: 103654-96-2, 121591-61-5, 121591-67-1
1-(α,α-dichloro-β,β,β-trifluoroethyl)benzylalcohol

E: 138950-21-7
2-chloro-1,1,1-trifluoro-3-phenylpropan-3-ol

Conditions

Conditions	Yield
With zinc; copper(l) chloride In N,N-dimethyl-formamide Product distribution; Mechanism; Ambient temperature; various concentrations; without catalyst; further aldehydes;	A 24 % Spectr. B 20 % Spectr. C 37 % Spectr. D 3 % Spectr. E 12 % Spectr.

...Expand

: 306-83-2
1,1,1-trifluoro-2,2-dichloroethane

: 100-52-7
benzaldehyde

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: 67230-92-6
2-chloro-3,3-difluoro-1-phenyl-2-propenol

C: 103654-96-2, 121591-61-5, 121591-67-1
1-(α,α-dichloro-β,β,β-trifluoroethyl)benzylalcohol

D: 138950-21-7
2-chloro-1,1,1-trifluoro-3-phenylpropan-3-ol

Conditions

Conditions	Yield
With zinc; copper(l) chloride 1.) DMF, 24 h; 2.) DMF; Yield given. Multistep reaction. Yields of byproduct given;

...Expand

: 370-69-4
tris(2,2,2-trifluoroethyl)phosphite

: 75-87-6
chloral

A: 75-88-7
1,1,1-trifluoro-2-chloroethane

B: Phosphoric acid 2,2-dichloro-vinyl ester bis-(2,2,2-trifluoro-ethyl) ester

Conditions

Conditions	Yield
Heating;

...Expand

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 75-89-8
2,2,2-trifluoroethanol

: 333-36-8
1,1,1-trifluoro-2-(2,2,2-trifluoroethoxy)ethane

Conditions

Conditions	Yield
With potassium hydroxide In 1,2-dimethoxyethane at 70℃; for 4h; Temperature;	97.4%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 75-89-8
2,2,2-trifluoroethanol

Conditions

Conditions	Yield
With potassium γ-hydroxybutyrate In 4-butanolide at 200℃; under 11251.1 Torr; for 6h;	96%
With 4-butanolide; potassium hydroxide at 200℃; under 11251.1 Torr; for 6h;	68%
With potassium acetate; ethylene glycol; acetic acid

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 753-90-2
trifluoroethylamine

Conditions

Conditions	Yield
With dmap; ammonia at 110℃; Temperature;	94%
With ammonia; water at 190℃;
With ammonia; water at 185℃;

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 68716-49-4
p-bromophenylboronic acid pinacol ester

: 1310949-87-1
4,4,5,5-tetramethyl-2-(4-(2,2,2-trifluoroethyl)phenyl)-1,3,2-dioxaborolane

Conditions

Conditions	Yield
With 4,4'-di-tert-butyl-2,2'-bipyridine; magnesium chloride; nickel dibromide; zinc In N,N-dimethyl acetamide at 80℃; for 12h; Inert atmosphere; Schlenk technique;	94%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 17878-47-6
(3-bromophenyl)trimethylsilane

: trimethyl(3-(2,2,2-trifluoroethyl)phenyl)silane

Conditions

Conditions	Yield
With 4,4'-di-tert-butyl-2,2'-bipyridine; magnesium chloride; nickel dibromide; zinc In N,N-dimethyl acetamide at 80℃; for 12h; Inert atmosphere; Schlenk technique;	93%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: mercury dichloride

: chloro(chlorodifluorovinyl)mercury

Conditions

Conditions	Yield
With BuLi In tetrahydrofuran; diethyl ether (N2); BuLi slowly added to stirred soln. of ligand (1 equiv.) in Et2O at-80°C; react. temp. was maintained between -55°C and -80. degree.C for 2 h; HgCl2 (1 equiv.) in THF added at -110°C; warmedto -35°C for few h; warmed to room temp.; solvent vol. reduced in vac. to half; hexane added; mixt. was allowed to settle; filtered under N2; solvent removed in vac.; washed (hexane); elem. anal.;	87%

Yield

With BuLi In tetrahydrofuran; diethyl ether (N2); BuLi slowly added to stirred soln. of ligand (1 equiv.) in Et2O at-80°C; react. temp. was maintained between -55°C and -80. degree.C for 2 h; HgCl2 (1 equiv.) in THF added at -110°C; warmedto -35°C for few h; warmed to room temp.; solvent vol. reduced in vac. to half; hexane added; mixt. was allowed to settle; filtered under N2; solvent removed in vac.; washed (hexane); elem. anal.;

87%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 32316-92-0
naphthalene-2-boronic acid

: 1204295-99-7
2-(2,2,2-trifluoroethyl)naphthalene

Conditions

Conditions	Yield
With [2,2]bipyridinyl; nickel(II) bromide dimethoxyethane; potassium phosphate In dimethyl sulfoxide at 80℃; for 30h; Inert atmosphere; Sealed tube;	87%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 127-08-2
potassium acetate

: 406-93-9
4,4,4-trifluorobutyric acid

Conditions

Conditions	Yield
Stage #1: 1,1,1-trifluoro-2-chloroethane; potassium acetate In 1-methyl-pyrrolidin-2-one at 180℃; for 23h; Autoclave; Sealed tube; Stage #2: With acetic anhydride In 1-methyl-pyrrolidin-2-one at 35 - 40℃; for 3h; Reagent/catalyst; Solvent;	86.5%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 591-18-4
1-Bromo-3-iodobenzene

: 1-bromo-2-(1-chloro-2,2-difluoro-vinyl)-benzene

Conditions

Conditions	Yield
Stage #1: 1,1,1-trifluoro-2-chloroethane With n-butyllithium; diisopropylamine; zinc(II) chloride In tetrahydrofuran at 15 - 20℃; for 2h; Stage #2: 1-Bromo-3-iodobenzene With tetrakis(triphenylphosphine) palladium(0) at 20℃; for 18h;	85%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 591-18-4
1-Bromo-3-iodobenzene

A: m-bromo-α-chloro-β,β-styrene

B: 1,4-bis-(1-chloro-2,2-difluoro-vinyl)-benzene

Conditions

Conditions	Yield
Stage #1: 1,1,1-trifluoro-2-chloroethane With zinc(II) chloride; lithium diisopropyl amide In tetrahydrofuran at 20℃; for 2h; Stage #2: 1-Bromo-3-iodobenzene; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 18h;	A 85% B 1%

...Expand

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 5720-07-0
4-methoxyphenylboronic acid

: 157928-44-4
1-methoxy-4-(2,2,2-trifluoroethyl)benzene

Conditions

Conditions	Yield
With [2,2]bipyridinyl; nickel(II) bromide dimethoxyethane; potassium phosphate In dimethyl sulfoxide at 80℃; for 30h; Inert atmosphere; Sealed tube;	85%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 49562-28-9
fenofibrate

: isopropyl 2-methyl-2-(4-(4-(2,2,2-trifluoroethyl)benzoyl)phenoxy)propanoate

Conditions

Conditions	Yield
With 4,4'-di-tert-butyl-2,2'-bipyridine; magnesium chloride; nickel dibromide; zinc In N,N-dimethyl acetamide at 80℃; for 12h; Inert atmosphere; Schlenk technique;	85%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 1461-22-9
tributyltin chloride

: 214422-68-1
tributyl(chlorodifluorovinyl)tin

Conditions

Conditions	Yield
With BuLi In diethyl ether BuLi added to soln. of ligand in Et2O at -80°C; after 2 h soln. of Bu3SnCl in Et2O (dissolved at -80°C) added slowly at -110°C; warmed to room temp. overnight; hexane added; filtered; solvent removed on rotary evaporator; distd. in vac. (242°C, 0.2 mmHg); elem. anal.;	84%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 2767-54-6
triethyltin bromide

: 329911-50-4
triethyl(chlorodifluorovinyl)tin

Conditions

Conditions	Yield
With BuLi In diethyl ether (N2); BuLi added to soln. of ligand in Et2O at -80°C; after 2 h soln. of Et3SnBr in Et2O (dissolved at -80°C) added slowly at -110°C; warmed to room temp. overnight; hexane added; filtered; solvent removed on rotary evaporator; distd. in vac. (182°C, 0.2 mmHg); elem. anal.;	84%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 624-31-7
4-tolyl iodide

: 4-methyl-α-chloro-β,β-difluorostyrene

Conditions

Conditions	Yield
Stage #1: 1,1,1-trifluoro-2-chloroethane With n-butyllithium; diisopropylamine; zinc(II) chloride In tetrahydrofuran at 15 - 20℃; for 2h; Stage #2: 4-tolyl iodide With tetrakis(triphenylphosphine) palladium(0) at 20℃; for 12h;	83%
Stage #1: 1,1,1-trifluoro-2-chloroethane With zinc(II) chloride; lithium diisopropyl amide In tetrahydrofuran at 20℃; for 2h; Stage #2: 4-tolyl iodide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 12h;	83%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 86-74-8
9H-carbazole

: 9-(2,2,2-trifluoroethyl)-9H-carbazole

Conditions

Conditions	Yield
With caesium carbonate In N,N-dimethyl-formamide for 16h; Inert atmosphere;	83%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 3972-65-4
1-bromo-4-tert-butylbenzene

: 1099597-89-3
1-(tert-butyl)-4-(2,2,2-trifluoroethyl)benzene

Conditions

Conditions	Yield
With 4,4'-di-tert-butyl-2,2'-bipyridine; magnesium chloride; nickel dibromide; zinc In N,N-dimethyl acetamide at 80℃; for 12h; Inert atmosphere; Schlenk technique;	83%

: 193694-04-1
N-TBS-4-bromoindole

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 1-(tert-butyldimethylsilyl)-4-(2,2,2-trifluoroethyl)-1H-indole

Conditions

Conditions	Yield
With 4,4'-di-tert-butyl-2,2'-bipyridine; magnesium chloride; nickel dibromide; zinc In N,N-dimethyl acetamide at 80℃; for 20h; Inert atmosphere; Schlenk technique;	83%

: 75-88-7
1,1,1-trifluoro-2-chloroethane

: 17282-40-5
N-(ethoxycarbonylmethyl)pyridinium bromide

: 2-fluoro-indolizine-3-carboxylic acid ethyl ester

Conditions

Conditions	Yield
With potassium carbonate; triethylamine In N,N-dimethyl-formamide at 80℃; for 24h;	82%

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