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Specifications of our 2-Chlorobenzonitrile CAS 873-32-5: Items Specifications Results Appearance Powder Conforms
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Items Standard Result Assay 98%min -----------------------------------------------------------------------------------------------
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inquiryCAS 873-32-5 2-chlorobenzonitrile chemical properties melting point 43-46 °c(lit.) boiling point 232 °c(lit.) density 1,18
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inquiryProduct Product name 2-Chlorobenzonitrile Synonyms OCBN CAS No. 873-32-5 EIN
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inquiryAppearance:white to light yellow crystal powder Storage:Room temperature Package:25kg/drum Application:Organic Synthesis Intermediate Transportation:Express/Sea/Air Port:Any port in china
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inquirySynonyms: 2-Chlorbenzoesαurenitril;2-Chlorbenzonitril;2-chloro-benzonitril;2-Chlorophenylcyanide;Benzonitrile, 2-chloro-;Benzonitrile, o-chloro-;Benzonitrile,2-chloro-;Nitril kyseliny o-chlorbenzoove CAS: 873-32-5 MF: C7H4ClN MW: 137.57 E
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:detailed see specifications Storage:Store in dr
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inquiryConditions | Yield |
---|---|
With ammonium hydroxide; sodium persulfate; sodium iodide; iron(II) chloride In 1,2-dichloro-ethane at 20 - 50℃; for 16h; | 99% |
With copper(II) oxide; hydroxylamine hydrochloride In neat (no solvent) for 0.0208333h; Mechanism; Reagent/catalyst; Microwave irradiation; Green chemistry; | 96% |
With ammonium hydroxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In ethanol at 40℃; under 1500.15 - 3000.3 Torr; for 4h; | 96% |
2-Chlorobenzyl alcohol
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
Stage #1: 2-Chlorobenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
With ammonium hydroxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In ethanol at 40℃; under 1500.15 - 3000.3 Torr; for 4h; Reagent/catalyst; | 97.1% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ammonia; oxygen; copper(II) nitrate In water; dimethyl sulfoxide at 80℃; under 760.051 Torr; for 7h; | 95% |
2-chlorothiobenzamide
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With polystyrene-bound diaryl telluroxide In dichloromethane for 1h; Ambient temperature; | 98% |
With polystyrne-bound selenoxide In ethanol for 24h; Heating; | 95% |
Conditions | Yield |
---|---|
With pyridine; Oxone; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; Pyridine hydrobromide In dichloromethane at 20℃; for 12h; Green chemistry; | 98% |
With C68H64Cl2N6P2Ru2(4+)*2F6P(1-)*2Cl(1-); caesium carbonate In N,N-dimethyl-formamide at 100℃; for 24h; Inert atmosphere; Green chemistry; | 91.9% |
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; free radical; trichloroisocyanuric acid In dichloromethane at 10℃; for 2h; | 90% |
Conditions | Yield |
---|---|
Stage #1: 2-(dodecylthio)benzonitrile With sulfuryl dichloride; water In chlorobenzene at 20 - 65℃; for 3h; Stage #2: With sodium hydroxide In water at 60 - 65℃; pH=9 - 10; Stage #3: With hydrogenchloride In water at 20 - 30℃; pH=3 - 4; Reagent/catalyst; | A 106 g B 97.2% C 143 g |
Conditions | Yield |
---|---|
With N-trifluoroacetylimidazole In tetrahydrofuran for 3.5h; Heating; | 97% |
With cerium(IV) oxide In o-xylene at 160℃; for 0.5h; Dean-Stark; Inert atmosphere; | 97% |
With phosphoric acid diethyl ester 2-phenylbenzimidazol-1-yl ester; triethylamine In acetonitrile at 20℃; for 0.416667h; | 96% |
Conditions | Yield |
---|---|
at 350℃; under 48754.9 Torr; for 0.416667h; Supercritical conditions; Flow reactor; | 97% |
With molybdenum hexacarbonyl In tetrachloromethane at 150℃; for 6h; Autoclave; | 28% |
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With iron(III) sulfate; 4-nitro-phenol In cyclohexane at 20℃; for 0.116667h; | 97% |
With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In toluene at 20℃; for 0.116667h; Schlenk technique; | 86% |
Conditions | Yield |
---|---|
With trimethylsilyl methanesulfonate; phosphorus pentoxide at 70 - 75℃; for 3h; further reagents; | 95% |
With triethylamine; trifluoroacetyl chloride In dichloromethane | 93% |
With C8H14N2O4S In dichloromethane for 1h; Reflux; | 93% |
2-Chlorobenzyl alcohol
2-chloro-benzaldehyde
ortho-chlorobenzoic acid
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With ammonium hydroxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In ethanol at 40℃; under 1500.15 - 3000.3 Torr; for 4h; | 95% |
Conditions | Yield |
---|---|
With ammonium hydroxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In ethanol at 40℃; under 1500.15 - 3000.3 Torr; for 4h; | 94.5% |
With hydroxyammonium sulfate; zinc for 0.416667h; Microwave irradiation; | 90% |
2-cyanophenyl octyl sulfide
A
1,2-benzisothiazolin-3-one
B
2-Chlorobenzonitrile
C
1-Chlorooctane
Conditions | Yield |
---|---|
Stage #1: 2-cyanophenyl octyl sulfide With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; Stage #2: With sodium hydroxide In water at 60 - 65℃; pH=9 - 10; Stage #3: With hydrogenchloride In water at 20 - 30℃; pH=3 - 4; | A 103 g B 94.5% C 100 g |
Conditions | Yield |
---|---|
With potassium phenolate; palladium diacetate; potassium carbonate; dimethyl cis-but-2-ene-1,4-dioate; triphenylphosphine In N,N-dimethyl-formamide at 120℃; for 24h; Schlenk technique; Inert atmosphere; | 94% |
A
1,2-benzisothiazolin-3-one
B
2-Chlorobenzonitrile
C
1-chlorooctadecane
Conditions | Yield |
---|---|
Stage #1: 2-(octadecylthio)benzonitrile With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; Stage #2: With sodium hydroxide In water at 60 - 65℃; pH=9 - 10; Stage #3: With hydrogenchloride In water at 20 - 30℃; pH=3 - 4; | A 102 g B 93.5% C 210 g |
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 0.5h; Elimination; Heating; | 93% |
Conditions | Yield |
---|---|
With oxygen; copper(II) trifluoroacetate; urea In dimethyl sulfoxide at 110℃; for 26h; Green chemistry; | 93% |
With iron(III) trifluoromethanesulfonate; sodium nitrite In dimethyl sulfoxide at 50℃; for 10h; Inert atmosphere; Sealed tube; | 46% |
Conditions | Yield |
---|---|
With mesoporous silica SBA-15 supported Cu2O nanoparticles In N,N-dimethyl-formamide at 120℃; for 8h; Green chemistry; | 93% |
With 3% Pd/CeO2; sodium acetate In N,N-dimethyl-formamide; isopropyl alcohol at 55℃; for 12h; Irradiation; | 26% |
o-chlorostyrene oxide
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With ammonia; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In water; acetonitrile at 70℃; | 91% |
With ammonia; iodine In water; acetonitrile at 70℃; | 83% |
Conditions | Yield |
---|---|
With N-chloro-succinimide; palladium diacetate; toluene-4-sulfonic acid In 1,2-dichloro-ethane at 70℃; for 12h; Sealed tube; | 90% |
2-iodochlorobenzene
2-(dimethylamino)malononitrile
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With copper(II) orthophosphate In N,N-dimethyl-formamide at 120℃; for 24h; Inert atmosphere; Sealed tube; | 90% |
2-chloro benzaldehyde oxime
Trichloroacetyl chloride
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 1h; Ambient temperature; | 88% |
Conditions | Yield |
---|---|
With [Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; hydroxylamine hydrochloride; sodium hydrogencarbonate In water at 100℃; for 7h; Inert atmosphere; Sealed tube; Green chemistry; | A n/a B 87% |
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With zirconium(IV) chloride In nitromethane for 0.0333333h; Heating; | 86% |
Conditions | Yield |
---|---|
With C22H48FeOP4 In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; Schlenk technique; | A 86% B n/a |
Conditions | Yield |
---|---|
With aluminum oxide; Oxone for 0.1h; microwave irradiation; | 84% |
Conditions | Yield |
---|---|
With tetraethylammonium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 20℃; for 0.75h; | A 84% B 10% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In water; acetonitrile at 20℃; for 0.75h; | A 8% B 81% |
Conditions | Yield |
---|---|
With sodium hydrogensulfite; sodium nitrite In ethanol; water; acetic acid at 24℃; for 4h; | 82% |
Conditions | Yield |
---|---|
With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; tetrabutylammomium bromide; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 0.166667h; Microwave irradiation; chemoselective reaction; | 82% |
2-iodochlorobenzene
formamide
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; aluminum (III) chloride; nickel(II) acetylacetonate; zinc(II) oxide In 1,2-dimethoxyethane at 145℃; for 12h; | 81% |
2-Chlorobenzonitrile
2-chlorobenzoselenoamide
Conditions | Yield |
---|---|
Stage #1: 2-Chlorobenzonitrile With woollins’ reagent In toluene for 4h; Heating; Stage #2: With water In toluene for 1h; | 100% |
With selenium; sodium tetrahydroborate In ethanol for 8h; Heating; | 58% |
2-Chlorobenzonitrile
4-methylphenylboronic acid
2-Cyano-4'-methylbiphenyl
Conditions | Yield |
---|---|
With potassium carbonate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In n-heptane; water at 60℃; for 1.66667h; Suzuki Coupling; Inert atmosphere; | 100% |
With potassium carbonate In water; isopropyl alcohol at 100℃; for 7h; Catalytic behavior; Suzuki-Miyaura Coupling; Inert atmosphere; | 100% |
With bis({5-chloro-2-[(4-chlorophenyl)(hydroxyimino)methyl]phenyl})cyclodipalladachl-orane-1,3,4-tris(ylium)-2-uide; tetra(n-butyl)ammonium hydroxide; potassium carbonate; tri tert-butylphosphoniumtetrafluoroborate In N,N-dimethyl-formamide at 130℃; for 0.666667h; Suzuki-Miyaura coupling; Microwave irradiation; | 99% |
Conditions | Yield |
---|---|
With potassium phosphate; catacxium A; palladium diacetate In toluene at 100℃; for 20h; Suzuki reaction; | 100% |
With potassium carbonate; 2-(di-tert-butyl-phosphino)-1-phenyl-1H-pyrrole; palladium diacetate In toluene at 60℃; Suzuki coupling; | 99% |
With potassium phosphate; catacxium A; palladium diacetate In toluene at 100℃; for 20h; Suzuki cross-coupling reaction; | 99% |
Conditions | Yield |
---|---|
With tris(2,6-di-tert-butylphenyl) phosphite; tetrabutyl-ammonium chloride; sodium carbonate; Palladacycle In N,N-dimethyl acetamide at 160℃; for 24h; Heck reaction; | 100% |
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); ruphos In tetrahydrofuran at 70℃; Negishi coupling; | 100% |
chloro-trimethyl-silane
2-Chlorobenzonitrile
phenyllithium
2-Chlor-N-trimethylsilyl-benzophenon-imin
Conditions | Yield |
---|---|
Stage #1: 2-Chlorobenzonitrile; phenyllithium In tetrahydrofuran at -78℃; Inert atmosphere; Stage #2: chloro-trimethyl-silane In tetrahydrofuran at 20℃; Inert atmosphere; | 100% |
2-Chlorobenzonitrile
3,3-dimethylbutyl bromide
1-(2-chlorophenyl)-4,4-dimethylpentan-1-one
Conditions | Yield |
---|---|
Stage #1: 3,3-dimethylbutyl bromide With iodine; magnesium In tetrahydrofuran for 1.83333h; Reflux; Stage #2: 2-Chlorobenzonitrile With copper(l) iodide In tetrahydrofuran for 3.5h; Reflux; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 20 - 50℃; for 1h; | 100% |
Stage #1: 3,3-dimethylbutyl bromide With iodine; magnesium In tetrahydrofuran for 1.83333h; Reflux; Stage #2: 2-Chlorobenzonitrile With copper(l) iodide In tetrahydrofuran at 20℃; Reflux; | 100% |
2-Chlorobenzonitrile
1-bromo-2-cyclohexylethane
1-(2-chlorophenyl)-3-cyclohexylpropan-1-one
Conditions | Yield |
---|---|
Stage #1: 1-bromo-2-cyclohexylethane With iodine; magnesium In tetrahydrofuran for 1.83333h; Reflux; Stage #2: 2-Chlorobenzonitrile With copper(l) iodide In tetrahydrofuran for 3.5h; Reflux; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 20 - 50℃; for 1h; | 100% |
Stage #1: 1-bromo-2-cyclohexylethane With iodine; magnesium In tetrahydrofuran for 1.83333h; Reflux; Stage #2: 2-Chlorobenzonitrile With copper(l) iodide In tetrahydrofuran Reflux; | 100% |
2-Chlorobenzonitrile
Conditions | Yield |
---|---|
Stage #1: 1-(2-bromo-ethyl)-adamantane With iodine; magnesium In tetrahydrofuran for 1.83333h; Reflux; Stage #2: 2-Chlorobenzonitrile With copper(l) iodide In tetrahydrofuran for 3.5h; Reflux; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 50℃; for 1h; | 100% |
2-Chlorobenzonitrile
1-(2-bromo-ethyl)-adamantane
1-(2-chlorophenyl)-3-(1-adamantyl)propan-1-one
Conditions | Yield |
---|---|
Stage #1: 1-(2-bromo-ethyl)-adamantane With iodine; magnesium In tetrahydrofuran for 1.83333h; Reflux; Stage #2: 2-Chlorobenzonitrile With copper(l) iodide In tetrahydrofuran at 20℃; Reflux; | 100% |
Conditions | Yield |
---|---|
With manganese(IV) oxide; silica gel for 0.0666667h; microwave irradiation; | 99% |
With dihydrogen peroxide; sodium hydroxide In water at 35℃; for 10h; Large scale; | 98.5% |
With water; potassium carbonate at 150℃; for 0.25h; Microwave irradiation; | 97% |
2-Chlorobenzonitrile
N-(1-methyl-4-piperidinyl)aniline
4-[2-(2-chlorobenzoyl)anilino]-1-methylpiperidine
Conditions | Yield |
---|---|
With hydrogenchloride; boron trichloride In water; toluene | 99% |
With hydrogenchloride; boron trichloride 1) toluene, reflux, 1 h; 2) neat, 150 deg C, 3 h; 3) H2O, 100 deg C, 20 min; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With sodium t-butanolate; palladium diacetate; CyPF-t-Bu In 1,2-dimethoxyethane at 110℃; | 99% |
With potassium carbonate In N,N-dimethyl-formamide for 15h; Heating; | 98% |
With fac-tris[2-phenylpyridinato-C2,N]iridium(III); caesium carbonate In N,N-dimethyl-formamide at 25℃; for 12h; Schlenk technique; Inert atmosphere; Irradiation; | 88% |
With 1,2,3,4-tetrahydroquinolin-8-ol; caesium carbonate; copper(I) bromide In N,N-dimethyl-formamide at 130℃; for 48h; Inert atmosphere; chemoselective reaction; | 72% |
With [2,2]bipyridinyl; (2,2'-bipyridine)nickel(II) dibromide In various solvent(s) Ambient temperature; electrolysis, magnesium anode, stainless steel cathode, 30 mA/cm2; | 50% |
2-Chlorobenzonitrile
Cysteamine
2-(2-chlorophenyl)-4,5-dihydro-1,3-thiazole
Conditions | Yield |
---|---|
With tribromomelamine at 100℃; for 0.0666667h; Neat (no solvent); | 99% |
In ethanol for 5h; Heating; | 40% |
styrene
2-Chlorobenzonitrile
2-((1E)-2-phenylvinyl)benzenecarbonitrile
Conditions | Yield |
---|---|
With sodium acetate; (IMes)Pd(NQ) In Bu4NBr at 140℃; for 24h; Conversion of starting material; Heck Reaction; | 99% |
With tetrabutylammomium bromide; sodium acetate; C84H60N12O8Pd4 at 140℃; for 2h; Heck Reaction; Inert atmosphere; Schlenk technique; | 96% |
With tris(2,6-di-tert-butylphenyl) phosphite; tetrabutyl-ammonium chloride; sodium carbonate; Palladacycle In N,N-dimethyl acetamide at 160℃; for 24h; Heck reaction; | 94% |
Conditions | Yield |
---|---|
With ammonium formate In water at 20℃; for 6h; | 99% |
With Triethoxysilane; C20H24N4Ni; sodium t-butanolate In toluene at 80℃; for 8h; Kumada Cross-Coupling; Inert atmosphere; Schlenk technique; | 83% |
With cyclohexa-1,4-diene; 9-ethyl-N3,N3,N6,N6,-tetramethyl-9H-carbazole-3,6-diamine; N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 23℃; for 0.8h; Inert atmosphere; UV-irradiation; Schlenk technique; | 83% |
2-Chlorobenzonitrile
2-Methylphenylboronic acid
2-(o-Tolyl)benzonitrile
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether; bis-phenanthrylimidazolium chloride; palladium diacetate In tetrahydrofuran at 50℃; for 12h; Suzuki-Miyaura coupling; | 99% |
With potassium phosphate; [2-(dicylohexylphopshino)-2',6'-dimethoxybiphenyl-Pd]2*2BF4 In toluene at 70℃; for 0.5h; Suzuki-Miyaura coupling; | 99% |
With potassium phosphate; C28H31ClN2Ni; triphenylphosphine In tert-Amyl alcohol; toluene at 110℃; for 24h; Suzuki-Miyaura Coupling; Inert atmosphere; Sealed tube; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 150℃; for 3h; Inert atmosphere; Green chemistry; | 97% |
With potassium carbonate; copper(II) oxide In N,N-dimethyl-formamide at 120℃; for 12h; | 91% |
Conditions | Yield |
---|---|
With sodium acetate; (IMes)Pd(NQ) In Bu4NBr at 140℃; for 24h; Conversion of starting material; Heck Reaction; | 99% |
Conditions | Yield |
---|---|
With dichloro[1,1′-bis[bis(1,1-dimethylethyl)phosphino]ferrocene-P,P′]palladium; TPGS-750-M; triethylamine In water at 40℃; Inert atmosphere; | 99% |
With potassium carbonate In ethanol; water at 120℃; for 2.5h; Suzuki-Miyaura reaction; continuous flow reactor; | 54% |
2-Chlorobenzonitrile
2-cyclo-pentylbenzonitrile
Conditions | Yield |
---|---|
With Pd-PEPPSI-IPrAn In tetrahydrofuran; 1,4-dioxane at 0 - 20℃; for 0.5h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In water; chlorobenzene at 60 - 65℃; for 17h; Inert atmosphere; | 99% |
With tetrabutylammomium bromide In water; chlorobenzene at 70 - 75℃; for 15h; Inert atmosphere; | 98% |
2-Chlorobenzonitrile
m-tolylboronic acid
Conditions | Yield |
---|---|
With potassium phosphate tribasic trihydrate; C30H39P; palladium diacetate In tetrahydrofuran at 110℃; for 3h; Suzuki-Miyaura Coupling; Inert atmosphere; | 99% |
2-Chlorobenzonitrile
3-methoxyphenylboronic acid
Conditions | Yield |
---|---|
With C42H32N8O8Pd(2+)*2Cl(1-); tetrabutylammomium bromide; potassium carbonate In water at 100℃; for 1h; Suzuki-Miyaura Coupling; High pressure; | 99% |
2-Chlorobenzonitrile
4-Aminobenzonitrile
2-((4-cyanophenyl)amino)benzonitrile
Conditions | Yield |
---|---|
With sodium phenoxide; C47H70BrO4PPdSi In tetrahydrofuran at 20℃; for 1h; Schlenk technique; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
Stage #1: 2-Chlorobenzonitrile; benzaldehyde With hydrogen In 2-methyltetrahydrofuran at 100℃; under 11251.1 Torr; for 20h; High pressure; Autoclave; Stage #2: With hydrogenchloride In diethyl ether | 99% |
2-Chlorobenzonitrile
5-(2-chlorophenyl)-1H-tetrazole
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 120℃; for 4h; | 98% |
With sodium azide at 120℃; for 2h; | 97% |
With sodium azide at 120℃; for 4.5h; | 97% |
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