DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:6609-54-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
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Min.Order:1 Gram
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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Min.Order:0 Metric Ton
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Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
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Min.Order:1 Gram
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Min.Order:1 Metric Ton
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:Sealed in a cool ,dry and microtherm place , avoid light . Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:It is an impo
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Min.Order:100 Gram
Negotiable
Type:Trading Company
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Min.Order:0
Negotiable
Type:Lab/Research institutions
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Cas:6609-54-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
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Cas:6609-54-7
Min.Order:0
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factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:6609-54-7
Min.Order:0
Negotiable
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Cas:6609-54-7
Min.Order:0
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Type:Lab/Research institutions
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Min.Order:0
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Type:Lab/Research institutions
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Cas:6609-54-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
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factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In water; chlorobenzene at 60 - 65℃; for 17h; Inert atmosphere; | 99% |
With tetrabutylammomium bromide In water; chlorobenzene at 70 - 75℃; for 15h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
In acetonitrile at 60℃; Inert atmosphere; | 99% |
2-cyanothioanisole
Conditions | Yield |
---|---|
With acetic anhydride In pyridine for 24h; Heating; | 83% |
N-cyano-N-phenyl-p-toluenesulfonamide
2-bromo-1-(methylsulfanyl)benzene
2-cyanothioanisole
Conditions | Yield |
---|---|
Stage #1: 2-bromo-1-(methylsulfanyl)benzene With magnesium; lithium chloride In tetrahydrofuran at 20℃; Inert atmosphere; Stage #2: N-cyano-N-phenyl-p-toluenesulfonamide In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With C18H14CuIN4 In acetonitrile at 20℃; for 24h; Inert atmosphere; Sealed tube; UV-irradiation; | 72% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 12h; UV-irradiation; | 72% |
Conditions | Yield |
---|---|
With potassium tert-butylate In acetonitrile at 50℃; for 6h; Sealed tube; | 63% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In water at 189℃; for 24h; | 62% |
Conditions | Yield |
---|---|
bis(tri-t-butylphosphine)palladium(0); zinc In N,N-dimethyl acetamide at 95℃; for 5h; | 56.1% |
methyl magnesium iodide
diethyl ether
o-cyanophenyl thiocyanate
2-cyanothioanisole
Conditions | Yield |
---|---|
With diethyl ether |
o-cyanophenyl thiocyanate
2-cyanothioanisole
Conditions | Yield |
---|---|
With potassium hydroxide; zinc nachfolgend Behandlung mit Dimethylsulfat; |
2-methylsulfanyl-benzamide
2-cyanothioanisole
Conditions | Yield |
---|---|
With diphosphorus pentasulfide; xylene | |
With phosphorus pentaoxide; xylene |
Conditions | Yield |
---|---|
Diazotization.man setzt die Diazoniumsalzloesung bei 60-70grad mit Kaliumkupfercyanuer um; |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: aq. sodium hydroxide (20percent) / 0.5 h 2: concentrated sulfuric acid / neat (no solvent) / 672 h 3: 90 percent / hydroxylamine hydrochloride / ethanol; pyridine / 4 h / Heating 4: 83 percent / acetic anhydride / pyridine / 24 h / Heating View Scheme |
2-cyanothioanisole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: concentrated sulfuric acid / neat (no solvent) / 672 h 2: 90 percent / hydroxylamine hydrochloride / ethanol; pyridine / 4 h / Heating 3: 83 percent / acetic anhydride / pyridine / 24 h / Heating View Scheme |
methyl 2-(2-methylthiophenyl)-2-oxoacetate
2-cyanothioanisole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / hydroxylamine hydrochloride / ethanol; pyridine / 4 h / Heating 2: 83 percent / acetic anhydride / pyridine / 24 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 15 percent / potassium tert-butoxide / liquid ammonia / 90 h / Irradiation View Scheme | |
Multi-step reaction with 2 steps 1: 100 percent Spectr. / potassium tert-butoxide / liquid ammonia / 60 h / Irradiation View Scheme | |
Multi-step reaction with 2 steps 1: 85 percent / potassium tert-butoxide / liquid ammonia / 2 h / Irradiation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: zinc; concentrated hydrochloric acid 2: Diazotization.man setzt die Diazoniumsalzloesung bei 60-70grad mit Kaliumkupfercyanuer um View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether; ammonia 2: phosphorus pentoxide; xylene View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride 2: diethyl ether; ammonia 3: phosphorus pentoxide; xylene View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Diazotization.Eintragen der Diazoloesung in eine Suspension von Kupfer(I)-rhodanid in Kaliumrhodanid-Loesung 2: alcoholic KOH-solution; zinc dust / nachfolgend Behandlung mit Dimethylsulfat View Scheme | |
Multi-step reaction with 2 steps 1: Diazotization.Eintragen der Diazoloesung in eine Suspension von Kupfer(I)-rhodanid in Kaliumrhodanid-Loesung 2: diethyl ether View Scheme |
2-Chlorobenzonitrile
methylthiol
chlorobenzene
2-cyanothioanisole
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide; sodium In water |
2-cyano-benzenediazonium tetrafluoroborate
2-cyanothioanisole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 0 - 20 °C 2: acetonitrile / 12 h / 20 °C / UV-irradiation View Scheme |
methyl-phenyl-thioether
phthalonitrile
A
2-cyanothioanisole
B
benzonitrile
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 1,2-bis-(dicyclohexylphosphino)ethane In o-xylene at 140℃; for 24h; | A n/a B 7 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: 2-cyanothioanisole With chlorine In water; chlorobenzene at 45 - 70℃; for 5h; Stage #2: With water; sodium hydroxide In chlorobenzene at 65 - 70℃; Concentration; Time; | 99% |
Stage #1: 2-cyanothioanisole With hydrogenchloride; water; chlorine In chlorobenzene at 45 - 70℃; for 3h; Stage #2: With water; sodium hydroxide In chlorobenzene at 65 - 70℃; | 98% |
Stage #1: 2-cyanothioanisole With chlorine In chlorobenzene at 40 - 80℃; Stage #2: With sodium hydroxide In water at 60 - 70℃; pH=10 - 12; Stage #3: With hydrogenchloride In water at 20 - 30℃; for 1h; pH=4 - 6; | 90% |
With hydrogenchloride; chlorine In water; chlorobenzene at 25 - 65℃; for 1.5h; | 90.8% |
acetic acid tert-butyl ester
2-cyanothioanisole
N-tert-butyl-o-(methylthio)benzamide
Conditions | Yield |
---|---|
With sulfuric acid at 42℃; for 6h; | 90% |
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; | 86% |
(1S,2R,5S)-(+)-menthol
2-cyanothioanisole
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; | 83% |
2-cyanothioanisole
4-phenylcyclohexan-1-d-1-ol
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; Sealed tube; | 81% |
Conditions | Yield |
---|---|
With (triphenylphosphine)gold(I) chloride In 1,2-dichloro-ethane at 130℃; Schlenk technique; | 80% |
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; | 78% |
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; | 77% |
Conditions | Yield |
---|---|
With bis(trimethylaluminum)–1,4-diazabicyclo[2.2.2]octane adduct In tetrahydrofuran at 130℃; for 0.2h; Microwave irradiation; Inert atmosphere; Sealed tube; | 76% |
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; | 75% |
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; | 71% |
Conditions | Yield |
---|---|
With titanium tetrachloride In toluene for 2h; Reflux; | 70.8% |
(S)-valinol
2-cyanothioanisole
(4S)-4-Isopropyl-2-<2-(methylsulfanyl)phenyl>-4,5-dihydro-1,3-oxazole
Conditions | Yield |
---|---|
zinc(II) chloride In chlorobenzene for 48h; Heating; | 69% |
With zinc(II) chloride In chlorobenzene for 48h; Heating; | 56% |
2-cyanothioanisole
N-Cyanoguanidine
Conditions | Yield |
---|---|
With potassium hydroxide In 2-ethoxy-ethanol at 130 - 135℃; for 10h; | 68% |
Conditions | Yield |
---|---|
With zinc(II) chloride In chlorobenzene for 48h; Heating; | 60% |
zinc(II) chloride In chlorobenzene for 48h; Heating; | 60% |
2-cyanothioanisole
(2S)-2-phenylglycinol
(4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole
Conditions | Yield |
---|---|
With zinc(II) chloride In chlorobenzene for 48h; Heating; | 58% |
zinc(II) chloride In chlorobenzene for 48h; Heating; | 58% |
2-cyanothioanisole
(1S,2S)-2-amino-1-phenyl-1,3-diol
[(4S,5S)-2-(2-Methylsulfanyl-phenyl)-5-phenyl-4,5-dihydro-oxazol-4-yl]-methanol
Conditions | Yield |
---|---|
With potassium carbonate In ethylene glycol; glycerol at 110℃; for 17h; | 55% |
With potassium carbonate In ethylene glycol; glycerol at 115℃; for 18h; | 47% |
2-cyanothioanisole
5-bromo-2-fluorobenzonitrile
Conditions | Yield |
---|---|
With N-Bromosuccinimide; tetrafluoroboric acid dimethyl ether complex In acetonitrile | 55% |
2-cyanothioanisole
(S)-tert-leucinol
Conditions | Yield |
---|---|
With zinc(II) chloride In chlorobenzene for 48h; Heating; | 53% |
zinc(II) chloride In chlorobenzene for 48h; Heating; | 53% |
Conditions | Yield |
---|---|
With potassium tert-butylate In 1,4-dioxane at 80℃; for 16h; Inert atmosphere; Glovebox; | 50% |
Conditions | Yield |
---|---|
With zinc(II) chloride In chlorobenzene for 48h; Heating; | 42% |
zinc(II) chloride In chlorobenzene for 48h; Heating; | 42% |
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