Product Name tert-Butyl acetate Synonyms ACETIC ACID TERT-BUTYL ESTER;Acetic acid 1,1-dimethylethyl ester;1,1-dimethylacetate;1,1-Dimethylethylacetate;2-methyl-2-propylacetate;acetatedebutyletertiare;Aceti
Cas:540-88-5
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name tert-Butyl acetate CAS number 540-88-5 Assay ≥99% Appearance Colorless transparent liquid Capacity 5000mt/year Application Organic intermedi
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inquiryOur advantage: 1: High quality and Competitive price 2: Quality control, GC&HPLC&NMR or as your requested 3: Packing as your requested, and double check before shipment 4: Prompt shipment with professional documents 5: Excellent after-
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inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:Clear colorless Liquid Storage:Sealed, dry, mi
Specifications: Tert-Butyl acetate CAS No.:540-88-5 Clear, colorless liquid good pharmaceutical intermediates Appearance:Colorless transparent liquid Package:175~200kg/drum,as customer request Application:intermediates Transportation:by
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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Cas:540-88-5
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
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inquiryCAS:540-88-5 EINECS:208-760-7 MW:116.16 MF:C6H12O2 Melting point:-62°C Boiling point:98 °C Appearance:colorless liquid Package:200kg/Steel drum Transportation:by sea Port:Shanghai
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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Superior quality, moderate price & quick delivery. Appearance:white powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used for active pharmaceutical ingr
ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
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1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
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inquiryConditions | Yield |
---|---|
at 200℃; under 22502.3 Torr; for 0.166667h; Product distribution / selectivity; | 100% |
With Cp2Ti(OSO2C8F17)2 at 100℃; for 0.0833333h; Neat (no solvent); | 99% |
With bismuth(lll) trifluoromethanesulfonate In acetonitrile at 20℃; for 0.166667h; | 98% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; benzaldehyde In 1,2-dichloro-ethane at 40℃; for 18h; Baeyer-Villiger Ketone Oxidation; | 99.3% |
With Oxone at 40℃; for 8h; Baeyer-Villiger oxidation; Ionic liquid; | 88% |
With oxygen; benzaldehyde; nickel(II) iodide; Dowex 50W; iron(II) In 1,2-dichloro-ethane at 20℃; for 15h; Baeyer-Villiger oxidation; | 52% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 24h; | 98% |
zirconium(IV) oxychloride at 20℃; for 0.0666667h; | 96% |
bismuth(III) oxychloride at 20℃; for 0.0666667h; | 96% |
Conditions | Yield |
---|---|
With calcined zinc oxide; acetic anhydride at 15℃; for 0.5h; | 96% |
tert-butyl peroxyacetate
triphenylantimony
A
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
With water; acetic anhydride In tetrahydrofuran; toluene byproducts: tert-butanol, phenol; toluene soln. of peracetate, acetic anhydride, and Sb-compd. heating in evacuated tube (70°C, 35 h), liquid fraction condensing in cold trap, THF+H2O addn., liquid fraction condensing; solid residue extracting by hexane (removing SbPh3) and CHCl3 (product);elem. anal.; | A n/a B 94% |
tert-butoxytrimethylsilane
acetic anhydride
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
at 20℃; for 0.666667h; | 93% |
Conditions | Yield |
---|---|
With manganese (VII)-oxide In tetrachloromethane; acetone at -45℃; | 92% |
With sodium hypochlorite; cis-{RuCl2(Me2SO)4} In dichloromethane at 20℃; for 5h; pH=9.5; | |
With sodium hypochlorite; cis-Ru(dmso)2Cl2 In dichloromethane at 20℃; for 5h; pH=9.5; Product distribution; Further Variations:; Catalysts; Solvents; | 73 % Chromat. |
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate for 1.41667h; Heating; | 84% |
With sulfuric acid; silica gel In hexane for 0.833333h; Heating; | 82% |
With silica gel In dichloromethane for 4h; Ambient temperature; | 80% |
acetyl chloride
tert-butyl alcohol
A
acetic acid tert-butyl ester
B
tertiary butyl chloride
Conditions | Yield |
---|---|
In dichloromethane 1.) 0 deg C, 2.) room temperature, 1 h; Yield given; | A n/a B 81% |
In dichloromethane for 1h; Rate constant; Mechanism; Ambient temperature; further solvents and times; further alcohols; |
tert-butyl alcohol
A
acetic acid tert-butyl ester
B
tertiary butyl chloride
Conditions | Yield |
---|---|
With acetyl chloride In dichloromethane for 1h; 0 deg C -> room temperature; Yields of byproduct given; | A n/a B 81% |
Acetic acid 3-tert-butylperoxy-2,3-dimethyl-4-oxo-3,4-dihydro-naphthalen-1-yl ester
A
1a,7a-dimethylnaphtho[2,3-b]oxirene-2,7(1aH,7aH)-dione
B
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
zinc trifluoromethanesulfonate In chloroform for 48h; Ambient temperature; | A 80% B 46% |
Conditions | Yield |
---|---|
With iodine at 85 - 90℃; for 0.0833333h; | 75% |
meta-fluoroaniline
bromoacetic acid tert-butyl ester
7-fluoro-4-[2-[4-(thieno[3,2-c]pyridin-4-yl)piperazin-1-yl]ethyl]quinolin-2(1H)-one
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In tetrahydrofuran; dichloromethane | 75% |
acetic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester
tert-butyl alcohol
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: tert-butyl alcohol With n-butyllithium In tetrahydrofuran; hexane at 20℃; for 0.25h; Metallation; Stage #2: acetic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester In tetrahydrofuran; hexane for 1h; Acetylation; Heating; | 74% |
tert-butyl peroxyacetate
triphenylbismuthane
B
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
With water; acetic anhydride In tetrahydrofuran; toluene byproducts: tert-butanol, phenol, phenylacetate; toluene soln. of peracetate, acetic anhydride, and Bi-compd. heating (evacuated tube, 70°C, 35 h), liquid fraction condensing in cold trap (liquid N2), THF+H2O addn., liquid fraction condensing; solid residue extracting by hexane (removing BiPh3) and CHCl3 (product);elem. anal.; | A 59% B 72% |
With water In tetrahydrofuran; toluene byproducts: tert-butanol, tert-butoxyphenol, phenol; toluene soln. of peracetate and Bi-compd. (evacuated tube), liquid fraction condensing in cold trap, THF+H2O addn., liquid fraction condensing; solid residue extracting by hexane (removing BiPh3) and CHCl3 (product); | A 32% B 24% |
acetic acid methyl ester
potassium tert-butylate
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
In diethyl ether at 20℃; | 69% |
Conditions | Yield |
---|---|
phosphotungstic acid at 65 - 70℃; for 1h; | 62% |
K2CO3 + 5percent Carbowax 6000 at 170℃; Product distribution; |
Conditions | Yield |
---|---|
With potassium carbonate; tetraoctyl ammonium bromide In chloroform for 0.25h; sonicated; | 60% |
With pyridine In benzene at 80℃; for 18h; | 33% |
Conditions | Yield |
---|---|
With pyridine In benzene at 80℃; for 2h; | 50% |
Conditions | Yield |
---|---|
With polyethylene glycol 400 at 65 - 70℃; for 7h; | 41% |
tert-Butyl 2,4-dinitro-3-(n-propylamino)-6-(trifluoromethyl)phenyl trithiocarbonate
A
acetic acid tert-butyl ester
B
4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione
Conditions | Yield |
---|---|
With acetic acid at 110 - 115℃; for 1.33333h; | A 40% B 38% |
carbon disulfide
vinyl acetate
potassium tert-butylate
methyl iodide
A
acetic acid tert-butyl ester
B
3,3-bis(methylthio)acrylaldehyde
Conditions | Yield |
---|---|
Stage #1: vinyl acetate; potassium tert-butylate In tetrahydrofuran at -78℃; Metallation; Substitution; Stage #2: carbon disulfide In tetrahydrofuran at 0℃; for 0.75h; Addition; Stage #3: methyl iodide In tetrahydrofuran at 0℃; for 12h; Methylation; | A n/a B 40% |
Conditions | Yield |
---|---|
With cobalt acetate; iodine; oxygen; N–hydroxysaccharin; sodium nitrite at 60℃; under 8250.83 Torr; for 6h; Temperature; Pressure; Reagent/catalyst; Concentration; | 35.9% |
ortho-methylphenyl iodide
tert-Butyl acrylate
N-(2-bromophenyl)-2,2,2-trifluoroacetamide
A
7-methylphenanthridine
B
acetic acid tert-butyl ester
C
5,6-dihydro-6-t-butoxycarbonylmethyl-7-methylphenanthridine
Conditions | Yield |
---|---|
With norborn-2-ene; palladium diacetate; potassium carbonate; triphenylphosphine In N,N-dimethyl-formamide at 105℃; for 24h; Inert atmosphere; chemoselective reaction; | A 35% B 32 %Chromat. C 10% |
methyl (E)-4-bromo-2-pentenoate
(2-tert-butoxy-2-oxoethyl)zinc(II) bromide
A
acetic acid tert-butyl ester
B
di-tert-Butyl succinate
C
(E)-4-Methyl-hex-2-enedioic acid 6-tert-butyl ester 1-methyl ester
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide at 25℃; | A n/a B n/a C 20% |
tert-butyl tetrahydropyranyl ether
acetyl chloride
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
With montmorillonite K-10 In chloroform at 20℃; for 0.3h; | 10% |
(4RS,5SR)-2,4-dimethyl-5-trimethylstannyl-2-hexanol
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
With borontrifluoride acetic acid In chloroform-d1 at -23℃; for 0.75h; | 9% |
pyridine
tetrachloromethane
acetyl chloride
tert-butyl alcohol
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
at 65℃; |
tetrachloromethane
N-isobutyl-N-nitroso-acetamide
A
acetic acid tert-butyl ester
B
sec-Butyl acetate
C
2-methylpropyl acetate
Conditions | Yield |
---|---|
at 77℃; |
Conditions | Yield |
---|---|
With acetic acid; silver(l) oxide |
acetic acid tert-butyl ester
1,2-bis(4-methoxyphenyl)butanone
t-butyl 3-hydroxy-3,4-bis-(p-methoxyphenyl)-hexanoate
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at 0℃; for 2h; | 100% |
acetic acid tert-butyl ester
(S)-methyl 4-(tert-butyldiphenylsilyloxy)-3-hydroxybutanoate
(5S)-6-(tert-butyl-diphenylsilanyloxy)-5-hydroxy-3-oxohexanoic acid tert-butyl ester
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -70 - -15℃; for 1.75h; | 100% |
Stage #1: acetic acid tert-butyl ester With n-butyllithium; diisopropylamine In tetrahydrofuran; hexanes at -40℃; for 0.5h; Claisen condensation; Inert atmosphere; Stage #2: (S)-methyl 4-(tert-butyldiphenylsilyloxy)-3-hydroxybutanoate In tetrahydrofuran; hexanes at -40 - 0℃; Inert atmosphere; | 85% |
acetic acid tert-butyl ester
3-(Tetrahydro-pyran-2-yloxy)-8-{2-[2-(tetrahydro-pyran-2-yloxy)-heptyl]-[1,3]dithiolan-2-yl}-octanal
t-butyl 3-hydroxy-5,13-di(tetrahydropyranyl)oxy-11-oxooctadecanoate-11-ethylenedithioketal
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 3h; | 100% |
acetic acid tert-butyl ester
(R,S)-4,5-diaminopentanoic acid dihydrochloride
Conditions | Yield |
---|---|
With perchloric acid for 22h; Ambient temperature; | 100% |
acetic acid tert-butyl ester
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 2h; | 100% |
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