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Product Description Product name 1,2-Benzisothiazolin-3-one (BIT 85%) CAS number 2634-33-5 Appearance Yellowish to white powder Assay ≥85% Capactiy 500mt/year Packing 25kg fi
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inquiryItem Specifications Results Appearance White to light yellow powder White to light yellow powder Assay HPLC
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inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
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inquiryProduct Name: 1,2-Benzisothiazolin-3-one Synonyms: 1,2-benzisothiazoline-3-one;proxelpl;Proxan;proxel;Proxel XL;proxil;Benzisothiazolin-3-one;BIT CAS: 2634-33-5 MF: C7H5NOS MW: 151.19 EINECS: 220-120-9 398
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inquiryChemical Name:1,2-Benzisothiazolin-3-one (BIT) CAS NO.:2634-33-5 Formula :C7H5NOS Molecular Weight :151.1826 Appearance: White or Light yellow powder Assay: 99.0%min Melting point: 155-158°C Color of Alkali solution: 4max
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inquiryConditions | Yield |
---|---|
Stage #1: 2-cyanothioanisole With chlorine In water; chlorobenzene at 45 - 70℃; for 5h; Stage #2: With water; sodium hydroxide In chlorobenzene at 65 - 70℃; Concentration; Time; | 99% |
Stage #1: 2-cyanothioanisole With hydrogenchloride; water; chlorine In chlorobenzene at 45 - 70℃; for 3h; Stage #2: With water; sodium hydroxide In chlorobenzene at 65 - 70℃; | 98% |
Stage #1: 2-cyanothioanisole With chlorine In chlorobenzene at 40 - 80℃; Stage #2: With sodium hydroxide In water at 60 - 70℃; pH=10 - 12; Stage #3: With hydrogenchloride In water at 20 - 30℃; for 1h; pH=4 - 6; | 90% |
Conditions | Yield |
---|---|
With sulfuryl dichloride; water In chlorobenzene at 20 - 65℃; for 3h; Reagent/catalyst; | A 97.2% B 143 g |
With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; Reagent/catalyst; |
Conditions | Yield |
---|---|
Stage #1: 2-(dodecylthio)benzonitrile With sulfuryl dichloride; water In chlorobenzene at 20 - 65℃; for 3h; Stage #2: With sodium hydroxide In water at 60 - 65℃; pH=9 - 10; Stage #3: With hydrogenchloride In water at 20 - 30℃; pH=3 - 4; Reagent/catalyst; | A 106 g B 97.2% C 143 g |
Conditions | Yield |
---|---|
Stage #1: 2-Chlorobenzonitrile With tetrabutylammomium bromide; sodium thioethylate In water; chlorobenzene for 2h; Inert atmosphere; Reflux; Stage #2: With sulfuryl dichloride; water In chlorobenzene at 5 - 80℃; for 1h; | 97% |
Stage #1: 2-Chlorobenzonitrile With potassium carbonate; ethane-1,2-dithiol In 1,2-dichloro-ethane at 80℃; for 5h; Stage #2: With chlorine at 40 - 80℃; for 3h; | 93.08% |
With tetrabutylammomium bromide; sodium thiomethoxide at 70 - 80℃; for 0.666667h; Temperature; Reagent/catalyst; | 92% |
2,2 dithiobis(benzonitrile)
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
With oxygen; (tetracarboxyphalocyaninato)copper(II) In water at 40℃; under 4500.45 Torr; for 8h; Reagent/catalyst; Temperature; Pressure; | 96% |
2-cyanophenyl octyl sulfide
A
1,2-benzisothiazolin-3-one
B
1-Chlorooctane
Conditions | Yield |
---|---|
With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; | A 94.5% B 100 g |
With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; |
2-cyanophenyl octyl sulfide
A
1,2-benzisothiazolin-3-one
B
2-Chlorobenzonitrile
C
1-Chlorooctane
Conditions | Yield |
---|---|
Stage #1: 2-cyanophenyl octyl sulfide With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; Stage #2: With sodium hydroxide In water at 60 - 65℃; pH=9 - 10; Stage #3: With hydrogenchloride In water at 20 - 30℃; pH=3 - 4; | A 103 g B 94.5% C 100 g |
Conditions | Yield |
---|---|
With oxygen; sodium thiosulfate; alpha cyclodextrin; iron(II) chloride In water at 40℃; Reagent/catalyst; Temperature; | 94.5% |
Conditions | Yield |
---|---|
With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; | A 93.5% B 210 g |
With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; |
A
1,2-benzisothiazolin-3-one
B
2-Chlorobenzonitrile
C
1-chlorooctadecane
Conditions | Yield |
---|---|
Stage #1: 2-(octadecylthio)benzonitrile With water; chlorine In chlorobenzene at 20 - 65℃; for 3h; Stage #2: With sodium hydroxide In water at 60 - 65℃; pH=9 - 10; Stage #3: With hydrogenchloride In water at 20 - 30℃; pH=3 - 4; | A 102 g B 93.5% C 210 g |
Conditions | Yield |
---|---|
With chlorine; potassium iodide In 1,2-dichloro-ethane at 25 - 40℃; for 0.416667h; | 93% |
With bromine In dichloromethane at 0 - 20℃; | 53% |
With sodium hydroxide |
Conditions | Yield |
---|---|
Stage #1: bis[2-(methoxycarbonyl)phenyl]disulfide With acetamide; sodium methylate In toluene at 80℃; for 2h; Stage #2: With dihydrogen peroxide at 50 - 55℃; Stage #3: With hydrogenchloride at 25℃; | 90% |
2-methoxycarbonylbenzenesulfenamide
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 20℃; for 0.5h; Cyclization; | 87% |
Conditions | Yield |
---|---|
With ammonia In dichloromethane at -15 - 20℃; for 2h; | 85% |
With ammonia In 1,2-dichloro-ethane at 60℃; for 3h; | 84% |
With ammonium hydroxide | |
With ammonia In tetrachloromethane for 3h; Ambient temperature; Yield given; | |
With ammonium hydroxide In dichloromethane for 1h; Yield given; |
2-methylsulfanyl-benzamide
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
With N-bromophthalimide In 1,1,2,2-tetrachloroethane at 50 - 60℃; | 85% |
With Selectfluor In acetonitrile at 80℃; for 12h; Schlenk technique; Sealed tube; | 80% |
With sulfuryl dichloride In toluene |
Conditions | Yield |
---|---|
With pyridine; diphenyl phosphoryl azide; triethylamine at 20℃; for 6h; Cyclization; | 81% |
Multi-step reaction with 2 steps 2: alcohol; ammonia gas View Scheme | |
Multi-step reaction with 2 steps 2: alcohol; ammonia gas View Scheme |
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
In toluene at 100℃; for 4h; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In 1-methyl-pyrrolidin-2-one; water at 20℃; for 0.5h; | 80.8% |
With potassium hydroxide; hydroxylamine-O-sulfonic acid In methanol; water at 0℃; for 3h; | 52% |
Multi-step reaction with 2 steps 1: air 2: durch Bromieren in Tetrachlorkohlenstoff und Kochen des Reaktionsprodukts mit Eisessig View Scheme |
Conditions | Yield |
---|---|
Stage #1: 2-chlorobenzamide With sodium sulfide In 1-methyl-pyrrolidin-2-one; water at 130 - 190℃; for 4h; Inert atmosphere; Stage #2: With dihydrogen peroxide In 1-methyl-pyrrolidin-2-one; water Temperature; Solvent; | 80.8% |
With carbon disulfide; L-proline; copper(I) bromide In dimethyl sulfoxide at 80℃; for 6h; | 35% |
Multi-step reaction with 2 steps 1: sodium sulfide hydrate / 1-methyl-pyrrolidin-2-one / 4 h / 160 °C 2: dihydrogen peroxide / 1-methyl-pyrrolidin-2-one; water / 0.5 h / 20 °C View Scheme |
phenyl isocyanate
A
2-(phenylamino)-4H-benzo[e][1,3]thiazin-4-one
B
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
In toluene at 100℃; for 4h; Inert atmosphere; | A 79% B 5% |
Conditions | Yield |
---|---|
With carbon disulfide; L-proline; copper(I) bromide In dimethyl sulfoxide at 80℃; for 6h; Reagent/catalyst; Solvent; Temperature; | 77% |
methanol
N-[(2-methoxycarbonylbenzene)sulfenyl]-1,2-benzisothiazolin-3-one
A
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
With sodium methylate In dichloromethane at 20℃; for 2.5h; Cyclization; alkoxylation; | A 34% B 71% |
ethyl 2-sulfenamoylbenzoate
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 20℃; for 0.5h; Cyclization; | 69% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; 1,10-Phenanthroline; tetra-(n-butyl)ammonium iodide In water at 20 - 140℃; for 48.5h; Inert atmosphere; | 60% |
2-methoxycarbonylbenzenesulfenamide
A
1,2-benzisothiazolin-3-one
B
bis[2-(methoxycarbonyl)phenyl]disulfide
C
N-2-methoxycarbonylphenylthio-2-methoxycarbonylbenzenesulfenamide
D
N-[(2-methoxycarbonylbenzene)sulfenyl]-1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
In toluene at 100℃; for 5h; Cyclization; | A 23% B 13% C 5% D 58% |
1-oxo-1H-1λ4-benzo[1,2]dithiol-3-one
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
With ammonia In dichloromethane for 1h; Ambient temperature; | 55% |
aniline
2-methoxycarbonylbenzenesulfenamide
A
1,2-benzisothiazolin-3-one
B
methyl 2-(N-phenylsulfenamoyl)benzoate
Conditions | Yield |
---|---|
In toluene at 100℃; for 8h; | A 49% B 48% |
Conditions | Yield |
---|---|
With carbon disulfide; L-proline; copper(I) bromide In dimethyl sulfoxide at 80℃; for 6h; | 48% |
Stage #1: 2-Bromobenzamide With sulfur; [2,2]bipyridinyl; copper(l) iodide; potassium carbonate In 1-methyl-pyrrolidin-2-one at 110℃; for 24h; Inert atmosphere; Stage #2: With pyridine; N-methoxylamine hydrochloride In 1-methyl-pyrrolidin-2-one at 110℃; for 3h; Inert atmosphere; | 15% |
Conditions | Yield |
---|---|
With sodium azide; sulfuric acid In dichloromethane for 72h; Ambient temperature; | 45% |
1,2-benzisothiazolin-3-one
tetramethyl ammoniumhydroxide
tetramethylammonium 1,2-benzisothiazol-3-one
Conditions | Yield |
---|---|
In water pH=9.58; | 100% |
In water pH=9.0; |
1,2-benzisothiazolin-3-one
4-Methoxyphenyl isocyanate
N-(4-methoxyphenyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 99% |
1,2-benzisothiazolin-3-one
1-phenylethylisocyanate
N-(α-methylbenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 99% |
1,2-benzisothiazolin-3-one
3-fluorobenzylisocyanate
N-(3-fluorobenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 99% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.5h; | 98% |
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 98% |
In tetrahydrofuran at 45℃; for 1h; | 88% |
1,2-benzisothiazolin-3-one
1-Isocyanato-2-methoxy-benzene
N-(2-methoxyphenyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 98% |
1,2-benzisothiazolin-3-one
1-Fluoro-2-isocyanato-benzene
N-(2-fluorophenyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 98% |
1,2-benzisothiazolin-3-one
4-methoxybenzyl isocyanate
N-(4-methoxybenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 98% |
1,2-benzisothiazolin-3-one
sale sodico del 1,2-benzisotiazolin-3-one
Conditions | Yield |
---|---|
With sodium hydroxide In methanol at 50℃; for 1h; | 98% |
With sodium hydroxide In ethanol at 20℃; for 0.5h; | 95% |
With sodium hydroxide at 50℃; | 92% |
With sodium hydride In methanol for 2h; Reflux; |
1,2-benzisothiazolin-3-one
n-butyl methanesulfonate
2-butyl-1,2-benzothiazolin-3-one
Conditions | Yield |
---|---|
Stage #1: 1,2-benzisothiazolin-3-one With sodium methylate In methanol at 0℃; for 1h; Stage #2: n-butyl methanesulfonate In methanol for 6h; Temperature; | 98% |
Conditions | Yield |
---|---|
In water; cyclohexanone at 95 - 156℃; Temperature; Solvent; Large scale; | 97.6% |
1,2-benzisothiazolin-3-one
methylene chloride
2-methyl-1,2-benzisothiazole-3(2H)-one
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; potassium iodide; sodium hydroxide In water at 30 - 100℃; Reagent/catalyst; | 97.6% |
Stage #1: 1,2-benzisothiazolin-3-one; methylene chloride In water at 20 - 30℃; for 1h; Stage #2: With sodium hydroxide In water at 60 - 70℃; pH=10 - 12; | 124.4 g |
Conditions | Yield |
---|---|
In cyclohexanone at 95 - 156℃; Temperature; Solvent; Large scale; | 97.5% |
1,2-benzisothiazolin-3-one
Conditions | Yield |
---|---|
With lithium hydroxide In ethanol at 80℃; for 2h; | 97.4% |
With lithium hydroxide monohydrate at 80℃; for 1.5h; | 71.2% |
With lithium hydroxide In methanol; water for 1h; Heating / reflux; |
1,2-benzisothiazolin-3-one
1,2-benzisothiazolin-3-one potassium salt
Conditions | Yield |
---|---|
With potassium hydroxide In acetic acid at 50℃; for 1h; | 97.2% |
With potassium hydroxide In water |
1,2-benzisothiazolin-3-one
3-methoxyphenyl isocyanate
N-(3-methoxyphenyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 97% |
In dichloromethane for 0.5h; Reflux; | 88% |
1,2-benzisothiazolin-3-one
para-fluorophenyl isocyanate
N-(4-fluorophenyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 97% |
1,2-benzisothiazolin-3-one
4-chloro-3-(trifluoromethyl)phenyl isocyanate
N-[4-chloro-3-(trifluoromethyl)phenyl]benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 97% |
1,2-benzisothiazolin-3-one
4-fluorobenzylisocyanate
N-(4-fluorobenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 97% |
1,2-benzisothiazolin-3-one
1-(isocyanatomethyl)-2-methoxybenzene
N-(2-methoxybenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 96% |
1,2-benzisothiazolin-3-one
N-(2-fluorobenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 96% |
1,2-benzisothiazolin-3-one
phenyl isocyanate
3-oxo-N-phenylbenzo[d]isothiazole-2(3H)-carboxamide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 95% |
1,2-benzisothiazolin-3-one
1-fluoro-3-isocyanatobenzene
N-(3-fluorophenyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 95% |
1,2-benzisothiazolin-3-one
1-(isocyanatomethyl)-3-methoxybenzene
N-(3-methoxybenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 95% |
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