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Cas:3360-41-6
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inquiry4-Phenyl-1-Butanol[CAS:3360-41-6] Name 4-Phenylbutanol Synonyms 4-Phenyl-1-butanol; Benzenebutanol Molecular Formula C10H14O Mol
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inquiryNow we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate ( such as diabtes series, Anti
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiry4-Phenylbutanol CAS:3360-41-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:3360-41-6
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Cas:3360-41-6
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:3360-41-6
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inquiry4-Phenylbutanol BenzenebutanolAppearance:White fine powder Storage:Kept in a cool,dry and ventilated place Package:according to customers' requirements Application:Meets the requirements Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiryProduct name: 4-Phenyl-1-Butanol(Benzenebutanol) CAS No.: 3360-41-6 Molecule Formula:C10H14O Molecule Weight:150.22 Purity: 99.0% Package: 200kg/drum Description:Colorless to light yellow liquid Manufacture Standards:Enterprise Standa
Cas:3360-41-6
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Conditions | Yield |
---|---|
With phosphate buffer; Phenyl acetate In diethyl ether for 2.75h; Ambient temperature; pig liver acetone powder; | A 5% B 100% |
Conditions | Yield |
---|---|
Stage #1: 4-Phenylbutyric acid With sodium tetrahydroborate In tetrahydrofuran at 60℃; for 0.25h; Stage #2: With iodine In tetrahydrofuran for 5h; Reagent/catalyst; | 99% |
Stage #1: 4-Phenylbutyric acid With sodium tetrahydroborate In tetrahydrofuran at 60℃; for 0.25h; Stage #2: With iodine In tetrahydrofuran for 5h; | 98.4% |
With C25H42N6Rh(1+)*CF3O3S(1-); phenylsilane In tetrahydrofuran at 30℃; for 20h; Inert atmosphere; | 96% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate In tetrahydrofuran; methanol at 50℃; Oxidation; | 98% |
With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate In tetrahydrofuran; methanol at 50℃; for 6h; | 96% |
tert-butyldimethylsilyl 4-phenylbutyl ether
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol; dichloromethane at 20 - 25℃; for 0.333333h; Flow reactor; | 98% |
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; | 249 mg |
Conditions | Yield |
---|---|
With ytterbium(III) triflate In isopropyl alcohol for 12h; Deacetylation; Heating; | 95% |
With 2,2-dibutyl-1,3,2-dioxastannane; cesium fluoride In N,N-dimethyl-formamide at 20℃; for 1h; | 95% |
Conditions | Yield |
---|---|
With iron(III) sulfate; water In toluene at 110℃; for 1h; Ionic liquid; | 95% |
4-Phenyl-1-butyne
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With 1-hydroxytetraphenylcyclopentadienyl(tetraphenyl-2,4-cyclopentadien-1-one)-μ-hydrotetracarbonyldiruthenium(II); Ru(Cp)(PPh2PytBu)2(MeCN)PF6; water In isopropyl alcohol at 70℃; for 48h; Inert atmosphere; regioselective reaction; | 95% |
With [2,2]bipyridinyl; formic acid; (η5-cyclopentadienyl) (η6-naphthalene)ruthenium hexafluorophosphate; water In tetrahydrofuran at 55℃; for 48h; | 88% |
With formic acid; F6P(1-)*C16H22N3Ru(1+); water In 1-methyl-pyrrolidin-2-one at 25℃; for 48h; Inert atmosphere; Sealed tube; | 87% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With thiophenol; 1,1'-azobis(1-cyanocyclohexanenitrile) In chlorobenzene at 110℃; for 12h; | 94% |
4-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butane
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
Stage #1: 4-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butane With sodium perborate tetrahydrate; water In tetrahydrofuran at 40℃; for 0.0166667h; Schlenk technique; Flow reactor; Stage #2: With sodium thiosulfate In tetrahydrofuran Schlenk technique; Flow reactor; | 92% |
With sodium hydroxide; dihydrogen peroxide In tetrahydrofuran at 55℃; for 3h; | 80% |
2-(4-phenyl-butoxy)-tetrahydro-pyran
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With indium(III) triflate In methanol; water at 0 - 20℃; for 6h; | 92% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With N1,N1,N12,N12-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere; | 91% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 60℃; for 4h; | 91% |
trimethylstannane
A
3-phenyl-propionaldehyde
C
4-phenyl-butan-1-ol
D
3-benzyl propionaldehyde
Conditions | Yield |
---|---|
In benzene under Ar; 80°C, 5 h; | A <1 B 42% C 7% D 88% |
4-(4-bromophenyl)butanoic acid
A
4-phenyl-butan-1-ol
B
4-(p-bromophenyl)-butan-1-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 25℃; for 2.25h; | A 10% B 88% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With oxalyl dichloride In 1,2-dichloro-ethane at 20℃; for 2.66667h; | 87% |
(4-(benzyloxy)butyl)benzene
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With aluminium trichloride; N,N-dimethyl-aniline In dichloromethane for 0.5h; Ambient temperature; | 86% |
Stage #1: (4-(benzyloxy)butyl)benzene With Bromotrichloromethane; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate In dichloromethane at 20℃; for 12h; Inert atmosphere; Irradiation; Stage #2: With methanol In dichloromethane Inert atmosphere; | 67% |
ethyl 4-phenylbutyrate
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
Stage #1: ethyl 4-phenylbutyrate With polyethylsiloxane; LiTi(OPr-i)4 at 100℃; for 24h; Stage #2: With sodium hydroxide In tetrahydrofuran for 3h; Heating; | 85% |
With lithium aluminium tetrahydride; diethyl ether | |
With ethanol; sodium | |
With sodium hydroxide In tetrahydrofuran; water |
2-benzylsulfanyl-4-phenyl-butyraldehyde
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); n-Bu3SH In benzene for 1.5h; Reduction; Heating; | 85% |
α-(trichloromethyl)benzenepropanol
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With lithium borohydride; sodium hydroxide In isopropyl alcohol Temperature; Jocic Reaction; Heating; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
Stage #1: 4-chlorobutyl benzoate With aluminum (III) chloride In benzene at -5℃; for 2h; Cooling with ice; Large scale; Stage #2: With methanol; water; sodium hydroxide Reflux; Large scale; | 83% |
tetrahydrofuran
phenylmagnesium chloride
A
(3E)-4-phenyl-3-buten-1-ol
B
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
Stage #1: tetrahydrofuran; phenylmagnesium chloride With lithium chloride; manganese(ll) chloride at 0℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: With iodobenzene for 1h; Inert atmosphere; Schlenk technique; Stage #3: With water Inert atmosphere; Schlenk technique; | A 7% B 81% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With potassium (4-methylphenyl)trifluoroborate In dimethyl sulfoxide at 37℃; for 10h; Inert atmosphere; | 80% |
3-phenyl-propionaldehyde
diazomethyl-trimethyl-silane
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
Stage #1: 3-phenyl-propionaldehyde; diazomethyl-trimethyl-silane With triphenylphosphine; isopropyl alcohol; Wilkinson's catalyst In tetrahydrofuran at 20℃; for 2h; Stage #2: pyrocatecholborane In 1,4-dioxane at 20℃; for 2h; Stage #3: With sodium hydroxide; dihydrogen peroxide In 1,4-dioxane at 20℃; for 3h; | 79% |
Conditions | Yield |
---|---|
With bis(cyclopentadienyl)titanium dichloride; manganese; water In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 79% |
With bis(cyclopentadienyl)titanium dichloride; manganese; water In tetrahydrofuran for 6h; | 78% |
(4-(tert-butoxy)butyl)benzene
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With zinc dibromide In dichloromethane for 24h; dealkylation; | 78% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); n-Bu3SH In benzene Reduction; | 77% |
4-phenyl-1-butylamine
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With potassium hydroxide In diethylene glycol at 210℃; for 12h; Product distribution; Further Variations:; Reaction partners; Solvents; | 76% |
With potassium hydroxide In diethylene glycol at 210℃; Substitution; | 59% |
Conditions | Yield |
---|---|
With indium(III) chloride; diphenylsilyl chloride In 1,2-dichloro-ethane at 80℃; for 3h; | 76% |
Conditions | Yield |
---|---|
Stage #1: carbon monoxide; 1-iodo-3-phenylpropan With diethoxymethylane; [CuCl(IPrMe)]; lithium methanolate In tetrahydrofuran at 60℃; under 2280.15 Torr; for 16h; Sealed tube; Stage #2: With tetrabutyl ammonium fluoride In tetrahydrofuran; diethyl ether at 20℃; for 2h; Catalytic behavior; Reagent/catalyst; Pressure; | 75% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; 1,2-dichloro-ethane; triphenylphosphine at 120℃; for 0.5h; Sealed tube; Inert atmosphere; | 100% |
With oxalyl dichloride In dichloromethane at 20℃; Appel Halogenation; Reflux; | 98% |
With thionyl chloride at 20℃; for 1.5h; Cooling with ice; Large scale; | 94% |
4-phenyl-butan-1-ol
3-benzyl propionaldehyde
Conditions | Yield |
---|---|
With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine In dichloromethane at 0℃; for 1h; Inert atmosphere; | 100% |
With pyridinium chlorochromate In dichloromethane at 20℃; for 3h; | 100% |
With oxalyl dichloride; dimethyl sulfoxide In dichloromethane at -55℃; for 0.25h; Oxidation; Swern oxidation; | 99% |
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 25℃; for 16h; Mitsunobu reaction; | 100% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With ammonia; sodium In ethanol at -78 - 20℃; Birch reduction; | 100% |
With lithium In ethanol; ammonia at -78 - 20℃; Birch Reduction; liquid NH3; | 98.3% |
Conditions | Yield |
---|---|
With triphenylphosphine In dichloromethane; hexane-diethyl ether | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-phenyl-butan-1-ol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: With sodium azide at 20℃; Sealed tube; Inert atmosphere; | 100% |
Stage #1: 4-phenyl-butan-1-ol With dmap; triethylamine; p-toluenesulfonyl chloride In dichloromethane at 0 - 20℃; Stage #2: With sodium azide In N,N-dimethyl-formamide at 20℃; | 55% |
With sodium azide; methanesulfonyl chloride | |
Multi-step reaction with 2 steps 1: triphenylphosphine; iodine; 1H-imidazole / 5.25 h / 0 - 20 °C 2: sodium azide / N,N-dimethyl-formamide / 18 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: 4-phenyl-butan-1-ol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: 4-trifluoromethylbenzenethiol at 20℃; Sealed tube; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-phenyl-butan-1-ol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: sodium phenoxide at 20℃; Sealed tube; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-phenyl-butan-1-ol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: sodium 4-methoxyphenolate at 20℃; Sealed tube; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-phenyl-butan-1-ol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere; Stage #2: potassium acetate at 20℃; Sealed tube; Inert atmosphere; | 100% |
4-phenyl-butan-1-ol
4-phenylbutyl benzoate
Conditions | Yield |
---|---|
With potassium hydroxide; benzoic acid | 99.7% |
4-phenyl-butan-1-ol
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With hydrogen bromide for 12h; Reagent/catalyst; Irradiation; Reflux; | 99.6% |
With allyl bromide; 1,1'-carbonyldiimidazole In acetonitrile for 1h; Heating; | 98% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 25℃; | 95% |
4-phenyl-butan-1-ol
methanesulfonyl chloride
4-phenylbutyl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere; | 99% |
With triethylamine In dichloromethane for 16h; Ambient temperature; | 96% |
With triethylamine In dichloromethane at 5 - 10℃; for 1h; | 91% |
Conditions | Yield |
---|---|
With iron(III) chloride at 20℃; for 1h; Esterification; | 99% |
With tetrabutylammomium bromide; oxygen; sodium nitrite at 70℃; for 4h; Green chemistry; | 81% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 1.5h; thioacetylation; | 99% |
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
With hydrogen; water-d2; palladium on activated charcoal at 110℃; under 760.051 Torr; for 24h; | 99% |
4-Cyanochlorobenzene
4-phenyl-butan-1-ol
4-(4-phenylbutoxy)benzonitrile
Conditions | Yield |
---|---|
Stage #1: 4-phenyl-butan-1-ol With sodium methylate In methanol at 130℃; for 2h; Stage #2: 4-Cyanochlorobenzene In methanol at 100℃; for 15h; Reagent/catalyst; Temperature; Solvent; | 98.1% |
phthalimide
4-phenyl-butan-1-ol
2-(4-phenylbutyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With triphenylphosphine; 3,3-dimethyl-1,2,5-thiadiazolidine-1,1-dioxide In dichloromethane for 2.5h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
Stage #1: carbon dioxide; 4-phenyl-butan-1-ol With tetra-(n-butyl)ammonium iodide; caesium carbonate In N,N-dimethyl-formamide at 23℃; for 1h; Stage #2: s-butyl bromide In N,N-dimethyl-formamide at 23℃; for 23h; | 98% |
With tetra-(n-butyl)ammonium iodide; caesium carbonate In N,N-dimethyl-formamide at 23℃; for 4h; | 91% |
Conditions | Yield |
---|---|
With pyridine N-oxide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 20℃; for 2h; Reagent/catalyst; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With cesium hydroxide; 4 A molecular sieve; tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 23℃; for 11h; | 97% |
Conditions | Yield |
---|---|
With cesium hydroxide; 4 A molecular sieve In N,N-dimethyl-formamide at 23℃; for 3h; | 97% |
Stage #1: 4-phenyl-butan-1-ol With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: benzyl bromide In tetrahydrofuran; mineral oil at 20℃; for 12h; Inert atmosphere; |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 95℃; for 36h; | 97% |
methyl 2-fluoro-4-hydroxybenzoate
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
97% |
[(p-cymene)Ru(OTf)2]
4-phenyl-butan-1-ol
Conditions | Yield |
---|---|
In nitromethane (Ar); addn. of ligand to a mixt. of ruthenium complex and CH3NO2, heating to 60°C for 30 min; layering with CH2Cl2 and Et2O, standing overnight at -20°C, sepn., washing with CH2Cl2 and Et2O, drying in vac.; elem. anal.; | 97% |
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