Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:13633-25-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:13633-25-5
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryHebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
Cas:13633-25-5
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
Type:Manufacturers
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:13633-25-5
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:13633-25-5
Min.Order:1 Kilogram
FOB Price: $3.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:13633-25-5
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryName: 1-Bromo-4-phenylbutane Synonyms: 4-Phenyl-1-Butyl Bromide CAS:13633-25-5 MF: C10H13Br Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Syntheses Material Intermediates
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:13633-25-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: 1-Bromo-4-phenylbutane CAS: 13633-25-5 MF: C10H13Br MW: 213.11 EINECS: Mol File: 13633-25-5.mol 1-Bromo-4-phenylbutane Structure 1-Bromo-4-phenylbutane Chemical Properties Melting point 52 °C Boiling point
Cas:13633-25-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:13633-25-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:13633-25-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have stoc
Cas:13633-25-5
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:13633-25-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:13633-25-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:13633-25-5
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:13633-25-5
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:13633-25-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:13633-25-5
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
Product name: 1-Bromo-4-Phenylbutane CAS No.:13633-25-5 Molecule Formula:C10H13Br Molecule Weight:213.11 Purity: 90.0% Package: 200kg/drum Description:Light yellow liquid Manufacture Standards:Enterprise Standard T
Cas:13633-25-5
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:13633-25-5
Min.Order:1 Kilogram
FOB Price: $1000.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:13633-25-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:13633-25-5
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:13633-25-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:13633-25-5
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Conditions | Yield |
---|---|
With triphenylphosphine In dichloromethane; hexane-diethyl ether | 100% |
4-phenyl-butan-1-ol
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With hydrogen bromide for 12h; Reagent/catalyst; Irradiation; Reflux; | 99.6% |
With allyl bromide; 1,1'-carbonyldiimidazole In acetonitrile for 1h; Heating; | 98% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 25℃; | 95% |
N-methyl-N-[4-(diphenylphosphino)benzyl]pyrrolidinium bromide
4-phenyl-butan-1-ol
A
Br(1-)*C24H27NOP(1+)
B
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With carbon tetrabromide In 1,2-dichloro-ethane at 40℃; for 2h; | A n/a B 97% |
4-Phenylbutyric acid
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With trimethylsilyl bromide; 1,1,3,3-Tetramethyldisiloxane; indium tribromide In chloroform at 60℃; for 4h; Sealed tube; Inert atmosphere; | 97% |
With indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane; trimethylsilyl cyanide In chloroform at 60℃; Inert atmosphere; | |
Multi-step reaction with 2 steps 1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere 2: triphenylphosphine; carbon tetrabromide / acetonitrile / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 20 °C 2: triphenylphosphine; carbon tetrabromide / acetonitrile / 3 h / 20 °C View Scheme |
(4-bromo-1-buten-1-yl)benzene
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethanol; water under 225.023 Torr; for 5h; | 93% |
4-(diphenylphosphino)-benzyltrimethylammonium bromide
4-phenyl-butan-1-ol
A
Br(1-)*C22H25NOP(1+)
B
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With carbon tetrabromide In 1,2-dichloro-ethane at 60℃; for 2h; | A n/a B 91% |
Conditions | Yield |
---|---|
at 5℃; for 2h; Temperature; | 85.8% |
Conditions | Yield |
---|---|
With copper(I) bromide; lithium bromide In tetrahydrofuran at 50 - 55℃; for 1h; | 85% |
benzenediazonium tetrafluoroborate
4-bromo-1-butylboronic acid catechol ester
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; palladium diacetate In tetrahydrofuran at 20℃; for 4.5h; Sizuki-Miyaura cross coupling; | 61% |
4-phenyl-butan-1-ol
triphenylphosphine
A
1-Bromo-4-phenylbutane
B
Triphenylphosphine oxide
Conditions | Yield |
---|---|
With carbon tetrabromide In 1,2-dichloro-ethane | A 53% B n/a |
5-Phenylpentanoic acid
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate; Diethyl 2-bromomalonate In chlorobenzene at 20℃; for 4h; Inert atmosphere; Irradiation; | 45% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 95℃; for 23h; | A 11% B 21% C 44% D 3% |
With rubidium carbonate In N,N-dimethyl-formamide at 95℃; for 23h; Product distribution; other reag; | A 12% B 34% C 20% D 18% |
Conditions | Yield |
---|---|
With n-butyllithium In diethyl ether; hexane for 2h; Heating; | 42% |
2-phenylbut-2-ene
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With hydrogen bromide; dihydrogen peroxide |
Conditions | Yield |
---|---|
Multistep reaction; |
4-phenylbutyl acetate
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With hydrogen bromide Heating; Yield given; |
Conditions | Yield |
---|---|
Anlagerung von HBr; |
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With hydrogen bromide at 130 - 140℃; im Rohr; |
benzylmagnesium chloride
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With diethyl ether |
4-phenyl-but-3-yn-1-ol
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H2 / Pd-CaCO3 2: PBr3 View Scheme |
phenylacetylene
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) EtMgBr, (ii) /BRN= 102378/ 2: H2 / Pd-CaCO3 3: PBr3 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 79 percent / LiAlH4 2: 61 percent / PBr3 View Scheme |
methyl 3-(benzyl)propanoate
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LAH 2: PBr3 View Scheme | |
Multi-step reaction with 2 steps 1: LiAlH4 / diethyl ether 2: (i) TsCl, Py, Et2O, (ii) LiBr, acetone View Scheme |
ethyl 4-phenylbutyrate
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium; alcohol 2: fuming hydrobromic acid / 100 °C View Scheme |
3-phenylpropylmagnesium bromide
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: fuming hydrobromic acid / 100 °C View Scheme | |
Multi-step reaction with 2 steps 2: phosphorus pentabromide View Scheme |
1-phenyl-2-bromoethane
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) Mg, Et2O, (ii) /BRN= 102378/ 2: HBr / benzene View Scheme | |
Multi-step reaction with 2 steps 2: aq. HBr, aq. H2SO4 View Scheme | |
Multi-step reaction with 2 steps 1: Mg / diethyl ether 2: PBr3 View Scheme |
4-phenyl-butan-1-ol
A
1-Bromo-4-phenylbutane
B
4-(Bromobutyl)benzene
Conditions | Yield |
---|---|
With phosphorus tribromide; sodium hydrogencarbonate In 1,4-dioxane; n-heptane; water; ethyl acetate |
p-imidazo-1-ylphenol
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With NaH In N,N-dimethyl-formamide |
1-Bromo-4-phenylbutane
1-(4-azidobutyl)benzene
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 80℃; | 100% |
With sodium azide In N,N-dimethyl-formamide at 70℃; for 9h; Inert atmosphere; | 99% |
With sodium azide In dimethyl sulfoxide at 20℃; for 36h; | 85% |
1-Bromo-4-phenylbutane
trimethyl(difluoromethyl)silane
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; cesium fluoride; bis(dibenzylideneacetone)-palladium(0) In N,N-dimethyl-formamide at 50℃; for 6h; Inert atmosphere; Glovebox; Schlenk technique; | 100% |
1-Bromo-4-phenylbutane
triphenylphosphine
(4-phenylbut-1-yl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In toluene Reflux; | 99% |
In toluene at 110℃; for 20h; Inert atmosphere; | 63% |
In toluene Heating; |
1-Bromo-4-phenylbutane
4'-hydroxy-3-biphenylcarbonitrile
4'-(4-phenylbutoxy)-[1,1'-biphenyl]-3-carbonitrile
Conditions | Yield |
---|---|
With potassium carbonate at 20 - 40℃; Inert atmosphere; | 99% |
1-Bromo-4-phenylbutane
methyl 3-hydroxybenzoate
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide for 12h; Williamson Ether Synthesis; Inert atmosphere; Reflux; | 99% |
1-Bromo-4-phenylbutane
isopropylamine
N-isopropyl-4-phenylbutan-1-amine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; | 99% |
1-Bromo-4-phenylbutane
A
polymer, CH2Cl2-insoluble; monomer(s): 1-bromo-4-phenylbutane; 5-(4-(4-ethenylphenyl)butoxy)methyl-1,3-dithiane, 1 molar part; styrene, 19 molar partspolymer, CH2Cl2-insoluble; monomer(s): 1-bromo-4-phenylbutane; 5-(4-(4-ethenylphenyl)butoxy)methyl-1,3-dithiane, 1 molar part; styrene, 19 molar parts
Conditions | Yield |
---|---|
Stage #1: polymer; monomer(s): 5-(4-(4-ethenylphenyl)butoxy)methyl-1,3-dithiane, 5 mol percent; styrene, 95 mol percent With n-butyllithium In tetrahydrofuran; hexane at -40 - -30℃; Stage #2: 1-Bromo-4-phenylbutane In tetrahydrofuran; hexane at -30 - -10℃; | A 0.7% B 98.9% |
1-Bromo-4-phenylbutane
methyl 4-hydroxylbenzoate
4-(4-phenyl-1-butoxy)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-4-phenylbutane; methyl 4-hydroxylbenzoate With potassium carbonate In N,N-dimethyl-formamide at 115℃; for 11h; Stage #2: With water; sodium hydroxide In ethanol for 3h; Reflux; Stage #3: With hydrogenchloride In ethanol; water pH=2; Reagent/catalyst; Concentration; | 98.7% |
1-Bromo-4-phenylbutane
sodium 4-phenylbutane-1-sulfonate
Conditions | Yield |
---|---|
With sodium sulfite In water for 24h; Heating; | 96% |
With sodium sulfite In tetrahydrofuran; ethanol; water at 160℃; for 0.25h; Microwave irradiation; |
1-Bromo-4-phenylbutane
N-benzylidene-4-fluoroaniline
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-4-phenylbutane With lithium In diethyl ether at -40 - 0℃; for 2h; Inert atmosphere; Stage #2: N-benzylidene-4-fluoroaniline In diethyl ether at -78 - 20℃; for 3h; Inert atmosphere; | 96% |
1-Bromo-4-phenylbutane
4-methoxy-N-[(3-methoxyphenyl)methylene]benzenamine
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-4-phenylbutane With lithium In diethyl ether at -40 - 0℃; for 2h; Inert atmosphere; Stage #2: 4-methoxy-N-[(3-methoxyphenyl)methylene]benzenamine In diethyl ether at -78 - 20℃; for 3h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetonitrile for 18h; Reflux; | 93% |
Conditions | Yield |
---|---|
With 6,6'-dimethyl-2,2'-bipyridine; nickel(II) bromide trihydrate; di-tert-butyl dicarbonate; sodium iodide; magnesium chloride; zinc In N,N-dimethyl acetamide at 30℃; for 24h; regioselective reaction; | 93% |
1-Bromo-4-phenylbutane
3,4-dihydroxybenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 2h; | 93% |
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-4-phenylbutane With lithium In diethyl ether at -40 - 0℃; for 2h; Inert atmosphere; Stage #2: N-(3-methylbenzylidene)-4-methoxybenzenamine In diethyl ether at -78 - 20℃; for 3h; Inert atmosphere; | 93% |
1-Bromo-4-phenylbutane
(3S)-1-(pent-4-enyl)-[(1R)-hydroxyethyl]azetidin-2-one
(3S)-1-(pent-4-enyl)-[(1R)-(4-phenylbutoxy)ethyl]azetidin-2-one
Conditions | Yield |
---|---|
Stage #1: (3S)-1-(pent-4-enyl)-[(1R)-hydroxyethyl]azetidin-2-one With sodium hydride In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #2: 1-Bromo-4-phenylbutane With potassium iodide In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 92% |
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
Stage #1: tert-butyl (R)-3-(3-(4-(1-(hydroxyimino)ethyl)phenyl)-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Stage #2: 1-Bromo-4-phenylbutane In tetrahydrofuran for 16h; Reflux; | 92% |
1-Bromo-4-phenylbutane
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 80℃; for 20h; | 91.4% |
1-Bromo-4-phenylbutane
(3S)-1-(4-methoxybenzyl)-[(1R)-hydroxyethyl]azetidin-2-one
(3S)-1-(4-methoxybenzyl)-[(1R)-(4-phenylbutoxy)ethyl]azetidin-2-one
Conditions | Yield |
---|---|
Stage #1: (3S)-1-(4-methoxybenzyl)-[(1R)-hydroxyethyl]azetidin-2-one With sodium hydride In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #2: 1-Bromo-4-phenylbutane With potassium iodide In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 91% |
1-Bromo-4-phenylbutane
mercaptoacetic acid
((4-phenylbutyl)sulfanyl)acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol at 20℃; | 91% |
2-pyrrolidinon
1-Bromo-4-phenylbutane
1-[4-phenylbutyl]pyrrolidin-2-one
Conditions | Yield |
---|---|
Stage #1: 2-pyrrolidinon With sodium hydride In toluene; paraffin oil for 10h; Inert atmosphere; Reflux; Stage #2: 1-Bromo-4-phenylbutane In 5,5-dimethyl-1,3-cyclohexadiene; toluene; paraffin oil for 4h; Inert atmosphere; Reflux; | 91% |
Conditions | Yield |
---|---|
With 6,6'-dimethyl-2,2'-bipyridine; nickel(II) bromide trihydrate; di-tert-butyl dicarbonate; sodium iodide; magnesium chloride; zinc In N,N-dimethyl acetamide at 30℃; for 24h; regioselective reaction; | 91% |
1-Bromo-4-phenylbutane
Methyl thioglycolate
methyl 2-[(4-phenylbutyl)thio]acetate
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide; acetone at 25℃; for 30h; | 90% |
With potassium carbonate In dimethyl sulfoxide; acetone at 25℃; for 30h; | 90% |
Stage #1: Methyl thioglycolate With potassium carbonate In acetone for 0.25h; Stage #2: 1-Bromo-4-phenylbutane In acetone for 21h; Reflux; |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View