Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:66943-05-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:66943-05-3
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:66943-05-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAza-15-crown-5 CAS:66943-05-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
Cas:66943-05-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:66943-05-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:66943-05-3
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Manufacturers
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Trading Company
inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white crystals powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as
Aza-15-crown-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:66943-05-3
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryPrice, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
Qingdao Sigma Chemical Ltd is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additives, herbal extracts, agrochemicals and fine chemicals etc. Our Labo
Cas:66943-05-3
Min.Order:1 Gram
FOB Price: $1.0
Type:Trading Company
inquiryThe Aza-15-crown-5, with CAS registry number 66943-05-3, belongs to the following product categories: (1)Azacrown Ethers; (2)Crown Ethers; (3)Macrocycles for Host-Guest Chemistry; (4)Functional Materials. It has the systematic name of 1,4,7,10-tetr
Cas:66943-05-3
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryWuhan Sun-shine Bio-technology Corporation Limited is specializing in the anticancer, antitumor,heart head blood-vessel,pharmaceutical intermediates,fine Chemicals production and customization..Company has strong ability of research and development,
At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryJoyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryMolecular Formula C10H21NO4 Molecular Weight 219.28 CAS Registry Number 66943-05-3 EINECS 266-523-3 Aza-15-crown-5Synonyms…
Cas:66943-05-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry1-benzyl-1-aza-15-crown-5
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal | 98% |
With hydrogen; palladium on activated charcoal In ethanol at 25℃; under 3102.9 Torr; for 24h; | 98% |
With hydrogen; palladium on activated charcoal In ethanol under 5171.5 Torr; for 6h; | 89% |
13-(p-Tolylsulfonyl)-1,4,7,10-tetraoxa-13-azacyclopentadecan
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | 83% |
With lithium aluminium tetrahydride In tetrahydrofuran Heating; |
2,2'-iminobis[ethanol]
triethylene glycol di-(p-toluenesulfonate)
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With sodium t-butanolate In 1,4-dioxane; tert-butyl alcohol at 40℃; for 2h; | 59% |
With sodium t-butanolate In 1,4-dioxane at 40℃; for 1h; | 45% |
With sodium In tert-butyl alcohol at 40℃; | 35% |
With sodium t-butanolate In 1,4-dioxane; tert-butyl alcohol at 20 - 40℃; for 3h; | 25% |
With sodium t-butanolate In 1,4-dioxane; tert-butyl alcohol at 40℃; for 4h; | 3.19 g |
2,2'-iminobis[ethanol]
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With sodium; tert-butyl alcohol at 40℃; for 19h; Inert atmosphere; Glovebox; | 28% |
1,2-bis(2-chloroethoxy)ethane
2,2'-iminobis[ethanol]
B
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With sodium t-butanolate In tert-butyl alcohol at 60℃; for 38h; | A n/a B 12% |
1,4,7,10-Tetraoxa-13-aza-cyclopentadecane-13-carboximidic acid methyl ester
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With acetic acid for 24h; Heating; Yield given; |
3,6,12-trioxa-9-azatetradecane-1,14-diol
A
2-[2-(2-morpholin-4-yl-ethoxy)-ethoxy]-ethanol
B
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With sodium hydroxide; p-toluenesulfonyl chloride In 1,4-dioxane at 60℃; for 5h; Yields of byproduct given; | A n/a B 50 % Spectr. |
With sodium hydroxide; p-toluenesulfonyl chloride In 1,4-dioxane at 20℃; for 5h; Product distribution; variation of arenesulphonyl chloride, base and temperature; | A 10 % Spectr. B 48 % Spectr. |
1,2-bis(2-chloroethoxy)ethane
2,2'-iminobis[ethanol]
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With sodium t-butanolate In tert-butyl alcohol at 60℃; Yield given; |
3,6,9-trioxa-12-azatetradecane-1,14-diol
A
2-{2-[2-(2-Aziridin-1-yl-ethoxy)-ethoxy]-ethoxy}-ethanol
B
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With sodium hydroxide; p-toluenesulfonyl chloride In 1,4-dioxane at 60℃; for 5h; Yields of byproduct given; | A n/a B 59 % Spectr. |
13-(4-nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With hydrogen sulfite In ethanol at 60 - 70℃; for 0.333333h; Yield given; |
A
3,5-di-tert-butyl-2-hydroxybenzaldehyde
C
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; |
A
3,5-di-tert-butyl-2-hydroxybenzaldehyde
C
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; |
A
3,5-di-tert-butyl-2-hydroxybenzaldehyde
C
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; |
A
3,5-di-tert-butyl-2-hydroxybenzaldehyde
C
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; |
A
3,5-di-tert-butyl-2-hydroxybenzaldehyde
C
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; |
2,2'-[1,2-ethanediylbis(oxy)]bisethanol
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 93 percent / aq. KOH / tetrahydrofuran / 10 h / 0 - 20 °C 2: 25 percent / sodium tert-butoxide / 2-methyl-propan-2-ol; dioxane / 3 h / 20 - 40 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 6.5 h 2.1: sodium hydroxide; tetrabutylammomium bromide / water; benzene / 10 h / 70 °C 3.1: hydrogen; palladium 10% on activated carbon; acetic acid / methanol / 4 - 5 h 3.2: pH 9 - 10 View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide / tetrahydrofuran; water / 18 h / 0 - 20 °C / Inert atmosphere; Glovebox 2: tert-butyl alcohol; sodium / 19 h / 40 °C / Inert atmosphere; Glovebox View Scheme | |
Multi-step reaction with 3 steps 1.1: dmap / dichloromethane / Inert atmosphere 1.2: 12 h / 0 - 20 °C / Inert atmosphere 2.1: sodium hydroxide; tetrabutylammomium bromide / water; toluene / 10 h / 70 °C / Inert atmosphere 3.1: acetic acid; palladium on activated charcoal; hydrogen / methanol / 12 h / 20 °C / 7500.75 Torr / Autoclave; Inert atmosphere View Scheme |
penta(ethylene glycol) bis(p-toluenesulfonate)
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 86 percent / Na2CO3 / toluene / 3 h / Heating 2: 89 percent / H2 / Pd/C / ethanol / 6 h / 5171.5 Torr View Scheme | |
Multi-step reaction with 3 steps 1: 12 percent / NaH, NaBr / dimethylsulfoxide / 2 h / 40 °C 2: 95 percent / KCN / 20 h / Heating 3: aqueous AcOH / 24 h / Heating View Scheme |
triethylene glycol di-(p-toluenesulfonate)
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 46 percent / NaH / tetrahydrofuran 2: 98 percent / H2, trace HCl / Pd-C View Scheme | |
Multi-step reaction with 2 steps 1: 52 percent / 80 percent NaH / tetrahydrofuran / Heating 2: 83 percent / LiAlH4 View Scheme | |
Multi-step reaction with 2 steps 1: (i) NaH, THF, (ii) /BRN= 632509/ 2: LiAlH4 / tetrahydrofuran / Heating View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydroxide; tetrabutylammomium bromide / water; benzene / 10 h / 70 °C 2.1: hydrogen; palladium 10% on activated carbon; acetic acid / methanol / 4 - 5 h 2.2: pH 9 - 10 View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydroxide; tetrabutylammomium bromide / water; toluene / 10 h / 70 °C / Inert atmosphere 2: acetic acid; palladium on activated charcoal; hydrogen / methanol / 12 h / 20 °C / 7500.75 Torr / Autoclave; Inert atmosphere View Scheme |
1,14-diiodo-3,6,9,12-tetraoxatetradecane
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Na2CO3 / acetonitrile / Heating 2: 88 percent / H2 / Pd/C / ethanol View Scheme |
2-(2-(2-(2-chloroethoxy)ethoxy)ethoxy)ethanol
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 64 percent / Na2CO3 / 24 h / 120 °C 2: 59 percent Spectr. / p-toluenesulphonyl chloride, NaOH / dioxane / 5 h / 60 °C View Scheme |
1,14-dichloro-3,6,9,12-tetraoxatetradecane
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 34 percent / NaH, NaBr / dimethylsulfoxide / 2 h / 40 °C 2: 95 percent / KCN / 20 h / Heating 3: aqueous AcOH / 24 h / Heating View Scheme |
N-cyano monoaza 15-crown-5
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / KCN / 20 h / Heating 2: aqueous AcOH / 24 h / Heating View Scheme |
carbon disulfide
1,4,7,10-tetraoxa-15-azacyclopentadecane
sodium (aza-15-crown-5) dithiocarbamate
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 0 - 5℃; for 2 - 3h; | 100% |
With sodium hydroxide In water at 0℃; for 6h; | 68% |
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 100℃; under 6000480 Torr; for 96h; | 100% |
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide at 120℃; for 18h; Inert atmosphere; | 100% |
2,7-bis(bromomethyl)naphthalene
1,4,7,10-tetraoxa-15-azacyclopentadecane
C32H50N2O8
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 18h; Heating; | 99% |
2-chlorothiazole
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 100℃; under 6000480 Torr; for 120h; | 99% |
2-chloro-1,3-benzoxazole
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 100℃; under 6000480 Torr; for 96h; | 99% |
2-chlorobenzo[d][1,3]thiazole
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 100℃; under 6000480 Torr; for 96h; | 99% |
1,4,7,10-tetraoxa-15-azacyclopentadecane
(C10O4NH21)2Ag(1+)*SbF6(1-)=(C10O4NH21)2AgSbF6
Conditions | Yield |
---|---|
In not given | 99% |
hydrogen fluoride
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
In water Ta2O5 reacted with 40% aq. HF; treated with aza-15-crown-5; crystals obtained; elem. anal.; | 99% |
1,4,7,10-tetraoxa-15-azacyclopentadecane
1-dicyanomethylene-2-chloro-3-(4,7,10,13-tetraoxa-1-azacyclopentadec-1-yl)indene
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 99% |
7-isothiocyanato-4-methyl-2H-chromen-2-one
1,4,7,10-tetraoxa-15-azacyclopentadecane
C21H28N2O6S
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; Inert atmosphere; | 99% |
meta-hydroxybenzaldehyde
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
Stage #1: meta-hydroxybenzaldehyde; 1,4,7,10-tetraoxa-15-azacyclopentadecane In tetrahydrofuran for 1h; Schlenk technique; Stage #2: With sodium tris(acetoxy)borohydride In tetrahydrofuran Schlenk technique; | 98.8% |
methanol
formaldehyd
1,4,7,10-tetraoxa-15-azacyclopentadecane
N-Methoxymethylmonoaza-15-crown-5 ether
Conditions | Yield |
---|---|
at 20℃; for 12h; | 98% |
for 0.5h; |
1-isothiocyanato-2-[2-(isothiocyanato)ethoxy]ethane
1,4,7,10-tetraoxa-15-azacyclopentadecane
C26H50N4O9S2
Conditions | Yield |
---|---|
In methanol at 40 - 45℃; for 0.25h; | 98% |
1,15-dithioxo-5,8,11-trioxa-2,14-diazapentadecane
1,4,7,10-tetraoxa-15-azacyclopentadecane
C30H58N4O11S2
Conditions | Yield |
---|---|
In methanol at 40 - 45℃; for 0.25h; | 98% |
1,18-dithioxo-5,8,11,14-tetraoxa-2,17-diazaoctadecane
1,4,7,10-tetraoxa-15-azacyclopentadecane
C32H62N4O12S2
Conditions | Yield |
---|---|
In methanol at 40 - 45℃; for 0.25h; | 98% |
ferrocenoyl chloride
1,4,7,10-tetraoxa-15-azacyclopentadecane
1,4,7,10-tetraoxa-13-azacyclopentadec-13-ylcarbonylferrocene
Conditions | Yield |
---|---|
With triethylamine In benzene soln. of chlorocarbonylferrocene added slowly to a soln. of aza-15-crown-5 and NEt3; stirring (1 h); filtration, evapn. (reduced pressure), column chromy. (neutral Al2O3; CH2Cl2, then CH2Cl2/MeOH); | 98% |
1,3-bis(bromomethyl)-2-nitrobenzene
1,4,7,10-tetraoxa-15-azacyclopentadecane
C28H47N3O10
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 18h; Heating; | 97% |
25,27-bis(methoxycarboxylic, acid)-26,28-dihydroxy-4-tert-butylcalix-[4]arene
1,4,7,10-tetraoxa-15-azacyclopentadecane
2,2'-[5,11,17,23-tetra-tert-butyl-26,28-dihydroxycalix[4]arene-25,27-diylbis(oxy)]bis[1-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)ethanone]
Conditions | Yield |
---|---|
Stage #1: 25,27-bis(methoxycarboxylic, acid)-26,28-dihydroxy-4-tert-butylcalix-[4]arene With benzotriazol-1-ol; dicyclohexyl-carbodiimide In chloroform at 0 - 20℃; Stage #2: 1,4,7,10-tetraoxa-15-azacyclopentadecane In chloroform for 12h; | 97% |
Stage #1: 25,27-bis(methoxycarboxylic, acid)-26,28-dihydroxy-4-tert-butylcalix-[4]arene With benzotriazol-1-ol; dicyclohexyl-carbodiimide In tetrahydrofuran; dichloromethane at 0℃; for 1h; Stage #2: 1,4,7,10-tetraoxa-15-azacyclopentadecane In tetrahydrofuran; dichloromethane at 0℃; | 96.7% |
4-(oxiran-2-ylmethyl)morpholine
1,4,7,10-tetraoxa-15-azacyclopentadecane
13-/2-hydroxy-3-(morpholino)propyl/-1,4,7,10-tetraoxa-13-azacyclopentadecane
Conditions | Yield |
---|---|
at 80℃; for 9h; | 96% |
2-nitrobenzyl chloride
1,4,7,10-tetraoxa-15-azacyclopentadecane
N-(2-nitrobenzyl)monoaza-15-crown-5
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile Heating; | 96% |
With sodium carbonate In acetonitrile for 24h; Heating; | 96% |
With sodium carbonate In acetonitrile for 24h; Heating; | 35% |
3,6-dichlorpyridazine
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 100℃; under 6000480 Torr; for 96h; | 96% |
ruthenocenecarbonyl chloride
1,4,7,10-tetraoxa-15-azacyclopentadecane
1,4,7,10-tetraoxa-13-azacyclopentadec-13-ylcarbonylruthenocene
Conditions | Yield |
---|---|
With triethylamine In benzene soln. of Ru-complex added dropwise to soln. of aza-15-crown-5 and NEt3; stirring (1 h); filtration, evapn. (reduced pressure), column chromy. (neutral Al2O3; CH2Cl2, then CH2Cl2/MeOH); | 96% |
1-fluoro-2-methoxy-4-nitrobenzene
1,4,7,10-tetraoxa-15-azacyclopentadecane
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide for 10h; Reflux; | 96% |
N-(Hydroxymethyl)-aziridine
1,4,7,10-tetraoxa-15-azacyclopentadecane
N-(Aziridinomethyl)-aza-15-crown-5
Conditions | Yield |
---|---|
In benzene at 20℃; for 3h; | 95% |
1-chloro-2,4-dinitro-benzene
1,4,7,10-tetraoxa-15-azacyclopentadecane
1-(2,4-dinitrophenyl)-1-aza-4,7,10,13-tetraoxapentadecane
Conditions | Yield |
---|---|
With tetrabutylammonium acetate In diethyl ether for 24h; Substitution; Heating; | 95% |
3,5-dibromobenzyl bromide
1,4,7,10-tetraoxa-15-azacyclopentadecane
13-(3,5-dibromobenzyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 24h; Reflux; | 95% |
1,3,5-Tris(bromomethyl)benzene
1,4,7,10-tetraoxa-15-azacyclopentadecane
1,3,5-tris[(1'-aza-4',7',10',13'-tetraoxapentadec-1'-yl)methyl]benzene
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile at 20℃; for 24h; Inert atmosphere; Reflux; | 95% |
1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene
1,4,7,10-tetraoxa-15-azacyclopentadecane
1,3,5-tris[(1'-aza-4',7',10',13'-tetraoxapentadec-1'-yl)methyl]-2,4,6-trimethylbenzene
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile at 20℃; for 35h; Inert atmosphere; Reflux; | 95% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View