As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:13338-63-1
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inquiryGood supplier high quality 3,4,5-Trimethoxyphenylacetonitrile 13338-63-1 manufacturer Product Details Overview Quick Details Pro Name;3,4,5-Trimethoxyphenylacetonitrile CAS NO:13338-63-1 Purity:99% Application: API Appearance:no
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:13338-63-1
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:13338-63-1
Min.Order:10 Kilogram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:13338-63-1
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inquiry3,4,5-Trimethoxyphenylacetonitrile CAS:13338-63-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qualit
Cas:13338-63-1
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:13338-63-1
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:13338-63-1
Min.Order:10 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryadvantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
Cas:13338-63-1
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:13338-63-1
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:13338-63-1
Min.Order:100 Gram
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:13338-63-1
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:13338-63-1
Min.Order:1 Kilogram
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:13338-63-1
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inquiryProduct Name: 3,4,5-Trimethoxyphenylacetonitrile Synonyms: (3,4,5-trimethoxyphenyl)-acetonitril;3,4,5-trimethoxybenzeneacetonitrile;3,4,5-trimethoxybenzylnitrile;3,4,5-trimethoxyphenylacetylnitryl;LABOTEST-BB LT00847929;3,4,5-TRIMETHOXYPHENYLAC
Cas:13338-63-1
Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:13338-63-1
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:13338-63-1
Min.Order:1 Kilogram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:13338-63-1
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:13338-63-1
Min.Order:1 Metric Ton
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:13338-63-1
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Cas:13338-63-1
Min.Order:1 Kilogram
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Type:Other
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:13338-63-1
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inquiryOxime of 3,4,5-trimethoxyphenylpyruvic acid
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With 1,1'-oxalyldiimidazole In benzene 1.) r.t., 15 min, 2.) 68-70 deg C, 1 h; | 88% |
With acetic anhydride | |
With acetic anhydride for 0.0833333h; Heating; |
3,4,5-trimethoxyphenyl acetic acid
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With sodium azide; TEA; triethylphosphine; (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane; dimethyl sulfoxide at 0℃; for 50h; | 88% |
sodium cyanide
5-(chloromethyl)-1,2,3-trimethoxybenzene
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 20℃; for 36h; | 85% |
In acetonitrile Reflux; | |
In acetonitrile for 4h; Reflux; | |
In dimethyl sulfoxide |
2,3,4-trimethoxybromobenzene
acetonitrile
A
2-(3,4,5-trimethoxyphenyl)acetonitrile
B
Bis-(3,4,5-trimethoxy-phenyl)-acetonitrile
Conditions | Yield |
---|---|
With ethoxyethoxyethanol; sodium amide In 1,2-dimethoxyethane 1.) 45 deg C, 2 h, 2.) -10 deg C, 2 h, 3.) -30 deg C, 4.5 h; | A 83% B 11% |
3,4,5-trimethoxybenzyl bromide
sodium cyanide
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
In dimethyl sulfoxide Ambient temperature; | 75% |
3,4,5-trimethoxybenzoyl cyanide
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With sodium sulfate; ethanethiol; zinc(II) chloride weiteres Reagens: Benzol; Erwaermen des Reaktionsprodukts mit Raney-Nickel in wss. Methanol; |
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With acetic anhydride |
Oxime of 3,4,5-trimethoxyphenylpyruvic acid
acetic anhydride
2-(3,4,5-trimethoxyphenyl)acetonitrile
potassium cyanide
3,4,5-trimethoxy-benzaldehyde
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With water; chloroformic acid ethyl ester; magnesium sulfate Hydrieren des Reaktionsprodukts an Palladium in Benzol; |
2,3,4-trimethoxybromobenzene
acetonitrile
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With sodium amide 1.) liquid ammonia, 5 min, 2.) liquid ammonia, 15 min; Yield given. Multistep reaction; |
potassium cyanide
5-(chloromethyl)-1,2,3-trimethoxybenzene
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
In 1,4-dioxane; water Heating; |
4-hydroxy-3,5-dimethoxyphenylacetonitrile
dimethyl sulfate
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With potassium carbonate In acetone |
sodium cyanide
5-(chloromethyl)-1,2,3-trimethoxybenzene
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With sodium iodide |
potassium cyanide
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With methanol | |
With methanol | |
With ethanol |
tetraethylammoniumcyanide
5-(chloromethyl)-1,2,3-trimethoxybenzene
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
In acetonitrile at 20℃; |
(3,4,5-trimethoxyphenyl)methanol
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2 / dioxane / 20 °C 2: acetonitrile / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 80 percent / PBr3, triethylamine / CCl4 / 1) 1h, 0 degC 2) 3h, roomtemp. 2: 75 percent / dimethylsulfoxide / Ambient temperature View Scheme | |
Multi-step reaction with 5 steps 1: pyridinium chlorochromate / CH2Cl2 / 3 h 2: sodium acetate / acetic anhydride / Heating 3: NaOH / H2O / Heating 4: hydroxylamine hydrochloride / aq. NaOH / 0.5 h / 60 °C 5: acetic anhydride / 0.08 h / Heating View Scheme |
3,4,5-trimethoxy-benzaldehyde
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaBH4 / methanol / 20 °C 2: SOCl2 / dioxane / 20 °C 3: acetonitrile / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: sodium acetate / acetic anhydride / Heating 2: NaOH / H2O / Heating 3: hydroxylamine hydrochloride / aq. NaOH / 0.5 h / 60 °C 4: acetic anhydride / 0.08 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: sodium tetrahydroborate; methanol / tetrahydrofuran / 2 h / 0 °C 2: thionyl chloride / dichloromethane / 1.5 h / 20 °C 3: dimethyl sulfoxide / 36 h / 20 °C View Scheme |
3,4,5-trimethoxybenzoic acid methyl ester
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 70 percent / LAH / tetrahydrofuran 2: 80 percent / PBr3, triethylamine / CCl4 / 1) 1h, 0 degC 2) 3h, roomtemp. 3: 75 percent / dimethylsulfoxide / Ambient temperature View Scheme | |
Multi-step reaction with 6 steps 1: lithium aluminium hydride / diethyl ether / 3 h / Heating 2: pyridinium chlorochromate / CH2Cl2 / 3 h 3: sodium acetate / acetic anhydride / Heating 4: NaOH / H2O / Heating 5: hydroxylamine hydrochloride / aq. NaOH / 0.5 h / 60 °C 6: acetic anhydride / 0.08 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: LiAlH4 / diethyl ether 2: HCl / benzene / 0 °C 3: dioxane; H2O / Heating View Scheme |
3-(3,4,5-trimethoxyphenyl)pyruvic acid
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydroxylamine hydrochloride / aq. NaOH / 0.5 h / 60 °C 2: acetic anhydride / 0.08 h / Heating View Scheme |
2-Phenyl-4-(3',4',5'-trimethoxybenzylidene)oxazolone
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaOH / H2O / Heating 2: hydroxylamine hydrochloride / aq. NaOH / 0.5 h / 60 °C 3: acetic anhydride / 0.08 h / Heating View Scheme |
3,4,5-Trimethoxybenzoyl chloride
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: ethanethiol; ZnCl2; Na2SO4 / weiteres Reagens: Benzol; Erwaermen des Reaktionsprodukts mit Raney-Nickel in wss. Methanol View Scheme |
elemicin
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ozone; ethyl acetate; oxygen / -15 °C / und anschliessende Hydrierung an Palladium/Calciumcarbonat unter Kuehlung; Isolierung als Natriumhydrogensulfit-Addukt 3: acetic acid anhydride View Scheme |
3,4,5-trimethoxyphenylacetaldehyde
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: acetic acid anhydride View Scheme |
1,3-dimethoxy-2-hydroxy-benzene
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: H2O 2: dimethylformamide 3: K2CO3 / acetone View Scheme |
2,6-dimethoxy-4-<(N,N-dimethylamino)methyl>phenol
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylformamide 2: K2CO3 / acetone View Scheme |
5-(chloromethyl)-1,2,3-trimethoxybenzene
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
In water; ethyl acetate; N,N-dimethyl-formamide |
trimethylsilyl cyanide
3,4,5-trimethoxybenzyl bromide
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In acetonitrile Reflux; | |
With tetra-n-butylammoniumfluoride trihydrate In acetonitrile for 6h; Reflux; | |
With tetrabutyl ammonium fluoride In acetonitrile for 6h; Reflux; | |
With tetrabutyl ammonium fluoride In acetonitrile for 6h; Reflux; |
3,4,5-trihydroxybenzoic acid
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium carbonate / acetone / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere; Cooling with ice 3: phosphorus tribromide / dichloromethane / 4 h / Cooling with ice; Inert atmosphere 4: tetra-n-butylammoniumfluoride trihydrate / acetonitrile / 6 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / acetone / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C 3: phosphorus tribromide / dichloromethane / 0 - 20 °C 4: tetrabutyl ammonium fluoride / acetonitrile / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / acetone / 4.5 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere 3: phosphorus tribromide / dichloromethane / 4 h / Inert atmosphere; Cooling with ice 4: tetrabutyl ammonium fluoride / acetonitrile / 6 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / acetone / 4.5 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere; Cooling with ice 3: phosphorus tribromide / dichloromethane / 4 h / Inert atmosphere; Cooling with ice 4: tetrabutyl ammonium fluoride / acetonitrile / 6 h / Reflux View Scheme |
2-(3,4,5-trimethoxyphenyl)acetonitrile
formic acid ethyl ester
Conditions | Yield |
---|---|
With sodium methylate In methanol for 2h; Heating; | 98% |
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 20 - 85℃; for 3h; Inert atmosphere; | 97% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
hexan-1-ol
2-(3,4,5-Trimethoxy-phenyl)-octanenitrile
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere; | 96% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
Diphenylphosphine oxide
(3,4,5-trimethoxybenzyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium tert-butylate; 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine In 1,4-dioxane at 120℃; for 16h; Reagent/catalyst; Inert atmosphere; Glovebox; Schlenk technique; | 96% |
With potassium tert-butylate; nickel dichloride In 1,4-dioxane at 120℃; for 16h; Inert atmosphere; Schlenk technique; | 71% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
O-methoxymethylisovanillin
Conditions | Yield |
---|---|
With sodium hydroxide; Aliquat 336 In dichloromethane for 4h; Ambient temperature; | 95% |
3-iodo-4-methoxybenzaldehyde
2-(3,4,5-trimethoxyphenyl)acetonitrile
C19H18INO4
Conditions | Yield |
---|---|
With sodium methylate In methanol at 45℃; | 93% |
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 10h; Inert atmosphere; Green chemistry; | 93% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
3,4,5-trimethoxyphenyl acetic acid
Conditions | Yield |
---|---|
With potassium hydroxide Heating; | 92% |
With sulfuric acid; acetic acid In water for 22h; Reflux; | 82% |
With hydrogenchloride | |
With potassium hydroxide In ethanol Reflux; | |
With water; potassium hydroxide In ethanol for 15h; Reflux; |
2-Aminonicotinaldehyde
2-(3,4,5-trimethoxyphenyl)acetonitrile
3-(2,3,4-trimethoxyphenyl)-[1,8]naphthyridin-2-ylamine
Conditions | Yield |
---|---|
With aminosulfonic acid for 0.05h; microwave irradiation; | 92% |
ethanol
2-(3,4,5-trimethoxyphenyl)acetonitrile
Ethyl 3,4,5-Trimethoxyphenylacetimidate Hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Ambient temperature; | 91% |
With hydrogenchloride In benzene | 82% |
With hydrogenchloride In chloroform for 2h; Ambient temperature; | |
With hydrogenchloride In diethyl ether at 0℃; | |
With hydrogenchloride In diethyl ether |
2-(3,4,5-trimethoxyphenyl)acetonitrile
cyclohexanone
Conditions | Yield |
---|---|
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate at 0 - 15℃; for 1h; | 90% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
3,4-dimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere; | 90% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
ethyl 3,4,5,-trimethoxy-α-cyanobenzeneacetate
Conditions | Yield |
---|---|
89% | |
89% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
dimethyl sulfate
2-methyl-2-(3,4,5-trimethoxyphenyl)propanenitrile
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran at -30 - 20℃; | 88% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
(4-ethoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium fluoride; palladium diacetate; trifluoroacetic acid In tetrahydrofuran; water at 80℃; for 2h; Inert atmosphere; Schlenk technique; | 87% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
3-fluoro-4-methoxy-phenylboronic acid
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium fluoride; palladium diacetate; trifluoroacetic acid In tetrahydrofuran; water at 80℃; for 2h; Inert atmosphere; Schlenk technique; | 85% |
1-ethynyl-2-methylbenzene
2-(3,4,5-trimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With potassium tert-butylate; tert-butyl alcohol In dimethyl sulfoxide at 80℃; for 12h; Inert atmosphere; stereoselective reaction; | 84% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
4-methylphenylboronic acid
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium fluoride; palladium diacetate; trifluoroacetic acid In tetrahydrofuran; water at 80℃; for 2h; Inert atmosphere; Schlenk technique; | 84% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
naphthalene-2-boronic acid
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium fluoride; palladium diacetate; trifluoroacetic acid In tetrahydrofuran; water at 80℃; for 2h; Inert atmosphere; Schlenk technique; | 84% |
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 10h; Inert atmosphere; Green chemistry; | 83% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
4-Methoxybenzyl alcohol
(E)-3,4,4',5-tetramethoxystilbene
Conditions | Yield |
---|---|
With C15H25Cl2N3NiO3; potassium tert-butylate In octane at 120℃; for 24h; Schlenk technique; Inert atmosphere; | 83% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
4-methoxy-benzaldehyde
Conditions | Yield |
---|---|
With sodium methylate In methanol at 20℃; Reflux; | 82% |
With sodium hydroxide; Aliquat 336 In dichloromethane for 4h; Ambient temperature; | 75% |
Stage #1: 2-(3,4,5-trimethoxyphenyl)acetonitrile; 4-methoxy-benzaldehyde In methanol at 60℃; for 0.5h; Stage #2: With sodium methylate In methanol at 60℃; |
methanol
2-(3,4,5-trimethoxyphenyl)acetonitrile
α-methyl-3,4,5-trimethoxybenzeneacetonitrile
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere; | 82% |
2-(3,4,5-trimethoxyphenyl)acetonitrile
4-methoxyphenylboronic acid
1-(4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)ethane-1-one
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium fluoride; palladium diacetate; trifluoroacetic acid In tetrahydrofuran; water at 80℃; for 2h; Inert atmosphere; Schlenk technique; | 82% |
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