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inquiryItems Standard Result Appearance Flaky crystal Complies Assay(by GC) 99%min
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inquiry3,4,5-Trimethoxybenzaldehyde CAS NO : 86-81-7 Product Product name 3,4,5-Trimethoxybenzaldehyde CAS No. 86-81-7
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryCHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
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inquiryName:3,4,5-Trimethoxybenzaldehyde CAS NO:86-81-7 Grade:Medical scientific research and export Molecular formula:C10H12O4 Molecular weight: 196.1999 Product Quality 12 years of chemical raw materials Mature operation of the industry System
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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inquiryName 3 4 5-trimethoxybenzaldehyde CAS No 86-81-7 MF C10H12O4 Purity 99% Appearance white powder Appearance: white powder Storage:
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inquiryAppearance:White or pale yellow crystalline flakes or solid Storage:R.T Package:25kg/drum Application:Intermediate Transportation:Express/Sea/Air Port:Any port in China
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inquiry3,4,5-Trimethoxybenzaldehyde CAS: 86-81-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Appearance:Off-white to white solid powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:It is used to synthesize antibacterial synergistic drug trimethoprim. It is
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiryProduct Name: 3,4,5-Trimethoxybenzaldehyde Synonyms: Trimetazidine Impurity 9;AKOS 214-88;AKOS BBS-00003169;3,4,5-TRIMETHOXY PHENYL ALDEHYDE;3,4,5-TRIMETHOXYBENZALDEHYDE;LABOTEST-BB LT00931453;OTAVA-BB BB7018801952;TMBA CAS: 86-81-7 MF: C10H
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inquiryacetoxy(benzo[1,3]dioxol-5-yl)(dimethylphenylsilyloxy)methane
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With silica gel Hydrolysis; | 100% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; V/SiO2 In decane; tert-butyl alcohol at 25℃; for 5h; | 99.6% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In aq. phosphate buffer; acetonitrile at 20℃; for 24h; pH=6; Enzymatic reaction; | 99% |
With Iron(III) nitrate nonahydrate; oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone In 1,2-dichloro-ethane at 60℃; for 3h; Schlenk technique; Green chemistry; | 99% |
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 2,6-dibromo-3,4,5-trimethoxybenzyl alcohol With potassium pyrosulfate In hexane at 36℃; for 120h; Stage #2: With sodium nitrate; hydrogen hexachloroiridate In hexane at 45℃; for 3h; Temperature; | 99.1% |
(dimethylphenylsilyl)(3,4,5-trimethoxyphenyl)methanol
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: (dimethylphenylsilyl)(3,4,5-trimethoxyphenyl)methanol With tert.-butylnitrite In benzene Nitrosation; Stage #2: In benzene at 0℃; Elimination; Photolysis; Further stages.; | 98% |
Conditions | Yield |
---|---|
With 1-dodecyl-3-methylimidazolium iron chloride; periodic acid at 30℃; for 1.5h; | 98% |
Multi-step reaction with 2 steps 1: 90 °C 2: acetic acid; water / 80 °C View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide; adogen 464 In dichloromethane; water for 16h; Ambient temperature; | 96% |
With potassium hydroxide; sodium carbonate In water; acetone for 18h; Heating; | 91.5% |
With potassium carbonate In acetone for 2h; Heating; | 9 g |
With potassium carbonate In acetone Williamson Ether Synthesis; |
2-(3,4,5-trimethoxyphenyl)-1,3-dithiane
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-(3,4,5-trimethoxyphenyl)-1,3-dithiane With acetyl chloride; sodium nitrite In dichloromethane at 0 - 5℃; for 0.25h; Stage #2: With water In dichloromethane at 0 - 20℃; for 1.25h; | 96% |
With tetra-N-butylammonium tribromide In dichloromethane at 0 - 5℃; for 0.5h; | 86% |
With tert.-butylhydroperoxide In methanol; water Heating; | 76% |
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With tetra-N-butylammonium tribromide In dichloromethane at 0 - 5℃; for 0.0833333h; | 96% |
Stage #1: 5-(bis-ethylsulfanyl-methyl)-1,2,3-trimethoxy-benzene With acetyl chloride; sodium nitrite In dichloromethane at 0 - 5℃; for 0.25h; Stage #2: With water In dichloromethane at 0 - 20℃; for 0.5h; | 96% |
With dihydrogen peroxide; vanadia; ammonium bromide In dichloromethane; water at 0 - 5℃; for 1.5h; | 94% |
With ammonium heptamolybdate; dihydrogen peroxide; ammonium bromide; perchloric acid In dichloromethane; water at 0 - 5℃; for 0.5h; | 80% |
tetramethlyammonium chloride
syringic aldehyde
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With caesium carbonate In 1,2-dimethoxyethane at 145℃; for 0.416667h; Microwave irradiation; Inert atmosphere; Sealed vessel; | 96% |
1,2-dihydro-1-(3,4,5-trimethoxybenzoyl)-2-quinolinecarbonitrile
A
quinoline-2-carboxylic acid
B
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With sulfuric acid at 107℃; for 1h; | A n/a B 95% |
2-(3,4,5-trimethoxyphenyl)-1,3-dithiane
A
1,2-dithiolane
B
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With tetrafluoroboric acid; tris(2,2'-bipyridine)iron(III) perchlorate In water; acetonitrile for 0.0833333h; Ambient temperature; | A n/a B 95% |
(3,4,5-trimethoxyphenyl)methanol
Dess-Martin periodane
A
1-acetoxy-1,2-benziodoxol-3-one
B
3,4,5-trimethoxy-benzaldehyde
C
acetic acid
Conditions | Yield |
---|---|
In dichloromethane at 25℃; for 0.333333h; Product distribution; reaction with other alcohols; | A n/a B 94% C n/a |
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With potassium peroxomonosulphate In water; acetic acid at 40 - 45℃; for 0.5h; Oxidation; | 94% |
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-(3,4,5-trimethoxyphenyl)-1,3-oxathiolane In ethanol at 20℃; Stage #2: With water In ethanol at 20℃; | 94% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; β‐cyclodextrin In water; acetone at 20℃; for 0.416667h; | 87% |
With ammonium bromide; dihydrogen peroxide; vanadia In dichloromethane at 0 - 5℃; for 1.25h; | 82% |
With perchloric acid; dihydrogen peroxide; ammonium bromide; molybdic acid In dichloromethane at 0 - 5℃; for 3h; | 75% |
3,4,5-trimethoxybenzaldehyde oxime
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With N-Bromosuccinimide; water at 20℃; for 0.0833333h; Hydrolysis; | 93% |
With iron(III) chloride In benzene Heating; | 92% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; water at 20℃; for 2.5h; Oxidation; oxidative cleavage; | 89% |
5-iodo-1,2,3-trimethoxybenzene
9-methyl-9H-fluorene-9-carbonyl chloride
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With dichloro(1,5-cyclooctadiene)palladium(II); N-Methyldicyclohexylamine; potassium formate; tetra-(n-butyl)ammonium iodide; tricyclohexylphosphine tetrafluoroborate; bis(dibenzylideneacetone)-palladium(0); tri tert-butylphosphoniumtetrafluoroborate In acetonitrile at 80℃; for 18h; Sealed tube; Glovebox; Inert atmosphere; | 93% |
2-bromo-3,4,5-tri-methoxybenzaldehyde
A
(+/-)-4,4',5,5',6,6'-hexamethoxy-1,1'-biphenyl-2,2'-dicarbaldehyde
B
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With copper at 250℃; for 0.25h; | A 92% B 3.5% |
at 190℃; for 1h; Product distribution; other temperatures and other reaction times; | A 73.5% B 23.5% |
at 320℃; for 0.0833333h; | A 25% B 50% |
With zinc; bis(triphenylphosphine)nickel(II) chloride In N,N-dimethyl-formamide at 60℃; for 9h; Ullmann-pinacol coupling; | A 50% B 30% |
(E)-3,4,5-trimethoxybenzaldehyde oxime
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With antimonypentachloride In dichloromethane at 20℃; for 2h; | 92% |
With lanthanum(III) chloride; sodium dihydrogenphosphate In water; acetonitrile at 20℃; for 18h; | 90% |
With triethylammonium chlorochromate(VI) In 1,2-dichloro-ethane for 2h; | 76% |
4-methyl-N′-(3,4,5-trimethoxybenzylidene)-benzenesulfonohydrazide
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In tetrahydrofuran; dimethyl sulfoxide for 0.416667h; Ambient temperature; | 92% |
With silica gel; iron(III) chloride for 0.03h; microwave irradiation; | 92% |
3,4,5-Trimethoxybenzaldehyde N,N-dimethylhydrazone
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With triethylene diamine nickel thiosulfate; water In chloroform at 20℃; for 0.0833333h; Hydrolysis; | 92% |
With chloro-trimethyl-silane; sodium iodide In water; acetonitrile for 0.0833333h; deprotection; | 87% |
3,4,5-trimethoxybenzaldehyde dimethyl acetal
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 25℃; for 16h; | 92% |
With β‐cyclodextrin In methanol; water at 50℃; for 10h; | 78% |
(3,4,5-Trimethoxyphenyl)methylene diacetate
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With water; titanium(IV) fluoride at 60℃; for 24h; screw-capped vial; | 92% |
With ammonium acetate for 0.00416667h; microwave irradiation; | 85% |
N-(2,4-dinitrophenyl)-N'-(3',4',5'-trimethoxybenzylidene)hydrazone
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
aluminum oxide; potassium permanganate at 20℃; for 0.0166667h; | 92% |
Conditions | Yield |
---|---|
With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.5h; | 92% |
3,4,5-trimethoxytoluene
A
3,4,5-trimethoxybenzyl acetate
B
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With oxygen; cobalt(II) acetate; manganese(II) acetate In acetic acid at 110℃; under 2280 Torr; for 2h; | A 4.2% B 91.2% |
1,2-bis(3,4,5-trimethoxyphenyl)ethane-1,2-diol
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With silica gel; periodic acid at 20℃; for 0.25h; Neat (no solvent); | 91% |
With aluminum oxide; potassium metaperiodate for 0.166667h; Microwave irradiation; | 40% |
5-[(3,4,5-trimethoxyphenyl)methylene]-2,2-dimethyl-1,3-dioxane-4,6-dione
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With oxone In water; acetonitrile at 45℃; for 1h; Reagent/catalyst; Solvent; Temperature; | 91% |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 20℃; | 90% |
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 20℃; for 6h; | 90% |
With potassium carbonate In N,N-dimethyl-formamide Heating; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With ammonium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In chloroform at 20℃; for 0.5h; | 89.2% |
With ammonium hydroxide; potassium hexacyanoferrate(III) In dichloromethane; water at 20℃; for 4h; | 85% |
Stage #1: 3,4,5-trimethoxybenzohydrazide With potassium hexacyanoferrate(III) Stage #2: With ammonium hydroxide In toluene Stage #3: In water at 20℃; | 81% |
With ammonium hydroxide; potassium hexacyanoferrate(III) | |
Multi-step reaction with 2 steps 1: pyridine 2: Na2CO3; ethylene glycol / 150 - 160 °C View Scheme |
3,4,5-trimethoxy-benzaldehyde
aniline
N-(3,4,5-trimethoxybenzylidene)aniline
Conditions | Yield |
---|---|
In chloroform Ambient temperature; | 100% |
sodium hydrogen sulfate; silica gel at 60 - 62℃; for 0.025h; microwave irradiation; | 94% |
In ethanol at 20℃; | 87% |
Conditions | Yield |
---|---|
Stage #1: 3,4,5-trimethoxy-benzaldehyde With hydrazine hydrate; potassium hydroxide In ethylene glycol at 70℃; for 2h; Wolff-Kishner Reduction; Stage #2: In ethylene glycol at 150℃; for 2h; | 100% |
With hydrogenchloride; hydrogen; palladium on activated charcoal In methanol at 20℃; under 760.051 Torr; for 1.5h; | 98% |
With hydrogen; palladium on activated charcoal In acetic acid under 30002.4 Torr; for 72h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 0 - 20℃; for 4h; | 100% |
With sodium tetrahydroborate In methanol at 0 - 20℃; for 1h; Inert atmosphere; | 100% |
With sodium tetrahydroborate In methanol at 20℃; for 1h; | 99% |
diethoxyphosphoryl-acetic acid ethyl ester
3,4,5-trimethoxy-benzaldehyde
ethyl (E)-3-(3,4,5-trimethoxyphenyl)acrylate
Conditions | Yield |
---|---|
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With lithium chloride In tetrahydrofuran at 20℃; for 0.25h; Horner-Wadsworth-Emmons Olefination; Inert atmosphere; Stage #2: 3,4,5-trimethoxy-benzaldehyde With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran Horner-Wadsworth-Emmons Olefination; Inert atmosphere; | 100% |
With potassium carbonate In water at 70℃; for 4h; | 90% |
With potassium carbonate In water at 70℃; for 4h; Wittig Olefination; stereoselective reaction; | 90% |
Conditions | Yield |
---|---|
With potassium hydroxide In methanol at 0℃; | 100% |
3,4,5-trimethoxy-benzaldehyde
Trimethylenediamine
N,N'-bis-(3,4,5-trimethoxybenzylidene)-1,3-diaminopropane
Conditions | Yield |
---|---|
In methanol for 1h; Ambient temperature; | 100% |
In ethanol for 1h; Heating; | 59% |
In methanol at 20℃; |
3,4,5-trimethoxy-benzaldehyde
Dimethyl phosphite
dimethyl α-hydroxy-α-(3,4,5-trimethoxyphenyl)methanephosphonate
Conditions | Yield |
---|---|
With dibutylamine In diethyl ether at 20℃; for 3h; | 100% |
With sodium methylate In methanol at 50℃; | 96.5% |
With methanol; sodium for 0.5h; Heating; | 90% |
3,4,5-trimethoxy-benzaldehyde
ethyl 2-cyanoacetate
2-cyano-3-(3,4,5-trimethoxyphenyl)acrylic acid ethyl ester
Conditions | Yield |
---|---|
With ytterbium(III) triflate at 80 - 85℃; Knoevenagel condensation; neat (no solvent); | 100% |
With recovered palladium catalyst In ethanol at 20℃; for 18h; Knoevenagel Condensation; Green chemistry; | 97% |
With montmorillonitesilylpropylidenediamine In toluene Ambient temperature; | 96% |
With piperidine In ethanol at 20℃; | |
In ethanol at 20℃; Knoevenagel Condensation; Sonication; |
3,4,5-trimethoxy-benzaldehyde
acetone
4-(3,4,5-trimethoxyphenyl)-3-buten-2-one
Conditions | Yield |
---|---|
With sodium hydroxide for 72h; Ambient temperature; | 100% |
With sodium hydroxide In ethanol; water for 0.75h; Ambient temperature; | 79% |
With sodium hydroxide In water at 20℃; for 20h; | 57% |
3,4,5-trimethoxy-benzaldehyde
(R)-Thiazolidine-4-carboxylic acid hydrazide
Conditions | Yield |
---|---|
In ethanol at 20℃; for 1h; | 100% |
3,4,5-trimethoxy-benzaldehyde
2,2-dimethoxyethylamine
2,2-dimethoxy-N-<(3',4',5'-trimethoxyphenyl)methylene>ethylamine
Conditions | Yield |
---|---|
In benzene for 5.25h; Heating; | 100% |
With magnesium sulfate In chloroform at 20℃; for 24h; | 100% |
With magnesium sulfate In chloroform at 20℃; for 24h; | 100% |
3,4,5-trimethoxy-benzaldehyde
trimethyl orthoformate
3,4,5-trimethoxybenzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With montmorillonite K10 In methanol at 40℃; for 18h; Inert atmosphere; | 100% |
With camphorsulfonic acid In methanol at 20℃; for 60h; Inert atmosphere; | 99% |
Stage #1: 3,4,5-trimethoxy-benzaldehyde; trimethyl orthoformate With ammonium chloride In methanol for 3h; Inert atmosphere; Reflux; Stage #2: With triethylamine In methanol at 20℃; for 0.0833333h; | 99% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride In 1-methyl-pyrrolidin-2-one at 100℃; for 0.5h; | 100% |
With oxygen; copper; ammonium chloride In pyridine at 60℃; for 24h; | 98% |
With trifluorormethanesulfonic acid; trimethylsilylazide In acetonitrile at 25℃; for 0.00277778h; Schmidt Reaction; Flow reactor; | 98% |
4-(1,3-benzodioxol-5-ylmethyl)-4,5-dihydrofuran-2(3H)-one
3,4,5-trimethoxy-benzaldehyde
4-Benzo[1,3]dioxol-5-ylmethyl-3-[hydroxy-(3,4,5-trimethoxy-phenyl)-methyl]-dihydro-furan-2-one
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -10 - 10℃; | 100% |
With lithium diisopropyl amide 1.) THF, -70 deg C, 10 min, 2.) THF, -70 deg C, 30 min; Multistep reaction; | |
Stage #1: 4-(1,3-benzodioxol-5-ylmethyl)-4,5-dihydrofuran-2(3H)-one With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.75h; Stage #2: 3,4,5-trimethoxy-benzaldehyde In tetrahydrofuran at -78℃; for 0.166667h; |
carbon tetrabromide
3,4,5-trimethoxy-benzaldehyde
1,1-Dibromo-2-(3',4',5'-trimethoxyphenyl)ethene
Conditions | Yield |
---|---|
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0℃; for 0.25h; Corey-Fuchs homologation; Stage #2: 3,4,5-trimethoxy-benzaldehyde In dichloromethane at 0℃; for 0.0833333h; Corey-Fuchs homologation; | 100% |
With triphenylphosphine In dichloromethane at 25℃; for 16h; | 99% |
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: 3,4,5-trimethoxy-benzaldehyde In dichloromethane Inert atmosphere; Schlenk technique; | 94% |
3,4,5-trimethoxy-benzaldehyde
propan-1-ol-3-amine
2-(3,4,5-trimethoxy)phenyltetrahydro-(2H)-1,3-oxazine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene Heating; | 100% |
3,4,5-trimethoxy-benzaldehyde
1-(trimethylsilyl)-1H-benzotriazole
Conditions | Yield |
---|---|
With potassium trimethylsilonate at 20℃; for 0.5h; | 100% |
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With potassium tert-butylate at 100℃; for 4.5h; | 100% |
vinyl magnesium bromide
3,4,5-trimethoxy-benzaldehyde
1-(3,4,5-trimethoxyphenyl)prop-2-en-1-ol
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 100% |
In tetrahydrofuran at 0 - 20℃; | 95% |
In tetrahydrofuran | 88% |
Conditions | Yield |
---|---|
Stage #1: 3-bromopropylamine hydrochloride With triethylamine In chloroform at 20℃; for 0.0833333h; Stage #2: 3,4,5-trimethoxy-benzaldehyde With magnesium sulfate In chloroform at 20℃; for 16h; | 100% |
3,4,5-trimethoxy-benzaldehyde
N-(3,4,5-trimethoxybenzyl)hydroxylamine
Conditions | Yield |
---|---|
Stage #1: 3,4,5-trimethoxy-benzaldehyde With hydroxylamine hydrochloride; sodium acetate; sodium cyanoborohydride In methanol; water for 6h; Stage #2: With hydrogenchloride; water In methanol for 16h; pH=1; | 100% |
3,4,5-trimethoxy-benzaldehyde
aniline
(E)-N-phenyl-1-(3,4,5-trimethoxyphenyl)methanimine
Conditions | Yield |
---|---|
at 80℃; under 15.0015 Torr; for 3h; | 100% |
In ethanol at 20℃; for 120h; | 90% |
With 4 A molecular sieve | |
at 80℃; under 15.0015 - 15.7516 Torr; |
3,4,5-trimethoxy-benzaldehyde
N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 0 - 25℃; | 100% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; | 100% |
3,4,5-trimethoxy-benzaldehyde
4-[(tert-butyldimethylsilyl)oxy]aniline
Conditions | Yield |
---|---|
In ethanol for 3h; Reflux; | 100% |
Conditions | Yield |
---|---|
With pyrrolidine In neat (no solvent) at 20℃; for 0.166667h; Aldol Condensation; | 100% |
With piperidine In ethanol at 65℃; Knoevenagel Condensation; |
3,4,5-trimethoxy-benzaldehyde
benzil
urea
4,5‐diphenyl‐2‐(3,4,5‐trimethoxyphenyl)‐1H‐imidazole
Conditions | Yield |
---|---|
With ammonium acetate; zinc(II) chloride at 70 - 110℃; for 0.5h; Green chemistry; | 100% |
(S)-1-Aminoindane
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) Milling; | 100% |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) Milling; | 100% |
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