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Cas:134-81-6
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inquiryItems Standard Result Assay 99.9%min 99.9% Hangzhou Dingyan Chem is a leading manufacturer and supplier of che
Cas:134-81-6
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inquiryProduct Description Product Name Benzil CAS No. 134-81-6 Appearance Yellowish crystal Assay ≥99% Capacity 200mt/year Min.packing 100gram Applica
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Cas:134-81-6
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inquiryAbout Product Details Benzil Chemical Propert
Cas:134-81-6
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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Cas:134-81-6
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inquiryProduct Name Benzil CAS No. 134-81-6 Molecular Formula C14H10O2
Appearance:Yellow crystal Storage:ln stock Package:25kg/Barrel Application:Organic Synthesis Intermediate Transportation:Express/Sea/Air Port:Any port of china
Cas:134-81-6
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:Yellow powder Storage:Refer to COA / MSDS Packa
Cas:134-81-6
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Cas:134-81-6
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Cas:134-81-6
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inquiryConditions | Yield |
---|---|
With pyridine chromium peroxide In benzene for 0.1h; Product distribution; Heating; effect of various chromium(VI) based oxidants; | 100% |
With pyridine chromium peroxide In benzene for 0.1h; Heating; | 100% |
With 4-dimethylaminopyridine tribromide In dichloromethane for 0.25h; Ambient temperature; | 100% |
Conditions | Yield |
---|---|
With sodium periodate; sulfuric acid; C31H29Br2N3Ru*CH2Cl2 In water; acetonitrile at 25℃; for 0.5h; Inert atmosphere; Schlenk technique; | 100% |
With sodium periodate; sulfuric acid; ruthenium-carbon composite In water; acetonitrile at 25℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Temperature; Time; Solvent; Green chemistry; | 100% |
With SO3-dioxane at 60℃; for 0.25h; | 99% |
1,2-diphenyl-2-thioxoethanone
benzil
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In diethyl ether for 1h; oxidation with nitric acid; | 100% |
1,2-diphenyl-2-(trimethylsilyloxy)ethanone
benzil
Conditions | Yield |
---|---|
With copper nitrate - dinitrogen tetroxide adduct In tetrachloromethane for 0.75h; Oxidation; Heating; | 100% |
With aluminium trichloride; silver bromate In acetonitrile for 0.4h; Heating; | 98% |
With Montmorillonite K10; ferric nitrate Oxidation; deprotection; Irradiation; | 95% |
(2RS)-(+/-)-2-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-1,2-diphenylethanone
benzil
Conditions | Yield |
---|---|
With copper nitrate - dinitrogen tetroxide adduct In tetrachloromethane for 1h; Oxidation; Heating; | 100% |
With N-hydroxyphthalimide; oxygen; cobalt(II) benzoate In acetonitrile at 20℃; for 9h; | 93% |
With manganese(IV) oxide; aluminium trichloride In acetonitrile for 0.333333h; Oxidation; Heating; | 40% |
A
[(6-Ph2TPA)Ni(O2CPh)]ClO4
B
phenacyl benzoate
C
carbon monoxide
D
benzil
E
benzoic acid
Conditions | Yield |
---|---|
With oxygen | A 100% B n/a C n/a D n/a E n/a |
A
phenacyl benzoate
B
carbon monoxide
D
benzil
E
benzoic acid
Conditions | Yield |
---|---|
With oxygen In acetonitrile at 20℃; | A n/a B n/a C 100% D 12% E 11 mg |
1,2-diphenyl-1,2-ethanediol
benzil
Conditions | Yield |
---|---|
With Me2Se*NCS; 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene 1.)1h 0 deg C, 1h room temperature, 2.) 4h room temperature; | 99% |
With octahydro-2,5-epiminopentalen-7-yloxidanyl; acetic acid; sodium nitrite In acetonitrile at 20℃; for 4h; air; | 99% |
With 9-benzyl-9-norazaadamantane N-oxyl; oxygen; acetic acid; sodium nitrite In acetonitrile at 20℃; for 4h; Catalytic behavior; Concentration; Reagent/catalyst; Solvent; Temperature; Time; | 99.3% |
benzil
Conditions | Yield |
---|---|
Stage #1: 2-bromo-2'-hydroxy-diphenyl-2-methylethanone With potassium chloride at 60 - 76℃; for 4.33h; Stage #2: With dimethyltitanocene; isopentyl butanoate for 4.5h; Temperature; | 99.3% |
Conditions | Yield |
---|---|
With hydrogen bromide; dimethyl sulfoxide at 55℃; for 24h; | 99% |
With C14H14N6O2; oxygen; sodium acetate; palladium diacetate at 120℃; under 760.051 Torr; for 48h; | 97% |
With potassium hydrogencarbonate; dimethyl sulfoxide at 80℃; | 96% |
1,2-diphenyl-2-methylthio-1-ethanone
benzil
Conditions | Yield |
---|---|
With CuCl2*2H2O In water; acetone for 1h; Heating; | 99% |
2-hydroxy-2-phenylacetophenone
2-nitro-aniline
A
2,3-diphenylquinoxaline
B
benzil
Conditions | Yield |
---|---|
With sodium hydroxide In toluene at 120℃; for 3h; Inert atmosphere; Sealed tube; | A 99% B 50% |
Conditions | Yield |
---|---|
With antimonypentachloride; dimethyl sulfoxide In nitromethane; benzene for 2h; Heating; | A n/a B 98.7% |
Conditions | Yield |
---|---|
With oxygen; silica gel; 4-aminoperbenzoic acid In dichloromethane at 20℃; for 9h; | 98% |
With graphite oxide In chloroform at 120℃; for 24h; | 17% |
With oxygen; graphite oxide In chloroform at 120℃; for 24h; Sealed tube; | 17% |
With selenium(IV) oxide at 200℃; | |
Multi-step reaction with 2 steps 1: SeO2 / 200 °C / sowie auf 300grad 2: SeO2 / 200 °C View Scheme |
2,2'-Diphenyl-[2,2']bi[[1,3]dithiolanyl]
benzil
Conditions | Yield |
---|---|
With t-butyl bromide; dimethyl sulfoxide at 70 - 75℃; for 4h; | 98% |
With trimethylsilyl iodide; dimethyl sulfoxide In tetrachloromethane at 75 - 80℃; for 6h; | 98% |
With fluorosulfonylchloride In diethyl ether; water Ambient temperature; | 86% |
4-iodoxybiphenyl
diphenyl acetylene
A
4-iodo-biphenyl
B
benzil
Conditions | Yield |
---|---|
In nitrobenzene at 170℃; for 5h; | A 98% B 34.5% |
Conditions | Yield |
---|---|
With (2 equiv); triphenylantimony dibromide; triethylamine In chloroform-d1 for 17h; Product distribution; Mechanism; reactions of α-hydroxyketones and esters in presence of var. bases; | A 98% B n/a |
Conditions | Yield |
---|---|
In acetonitrile; trifluoroacetic acid excess diphenylacetylene was treated with cis-((Cn*)(CF3CO2)Ru(VI)O2)ClO4 in 0.2M CF3COOH/MeCN soln. at room temp.; recrystn. from MeCN/Et2O; elem. anal.; | A 92% B 98% |
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In N,N-dimethyl-formamide at 23 - 25℃; for 4h; | 98% |
Conditions | Yield |
---|---|
With aluminum (III) chloride; Oxone In water at 20℃; for 24h; | 98% |
With iodine; dimethyl sulfoxide; copper(ll) bromide for 8h; Catalytic behavior; Reagent/catalyst; Schlenk technique; Heating; | 95% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; acetic acid; copper(I) bromide at 100℃; for 2h; Mechanism; Reagent/catalyst; Temperature; | 90% |
benzilmonoxime
benzil
Conditions | Yield |
---|---|
With bis(1-CH2Ph-3,5,7-3N-1-N(1+)tricyclo[3.3.1.13,7]decaneS2O8 In acetonitrile for 0.333333h; Oxidation; Heating; | 97% |
With KMnO4/alumina at 50℃; for 0.5h; | 97% |
With Cu(NO3)2-SiO2 for 0.133333h; oxime cleavage; microwave irradiation; | 95% |
Conditions | Yield |
---|---|
With ruthenium(IV) oxide; sodium periodate In dichloromethane; water; acetonitrile for 0.5h; Ambient temperature; | A 97% B n/a |
Conditions | Yield |
---|---|
With Cu(NO3)2-SiO2 for 0.0833333h; Oxidation; oxime cleavage; microwave irradiation; | 97% |
With water; Dess-Martin periodane In dichloromethane at 5 - 20℃; for 0.333333h; | 92% |
With quinolinium monofluorochromate(VI) In dichloromethane for 5h; Product distribution; Oxidation; Heating; | 85% |
With imidazolium fluorochromate In acetonitrile at 20℃; for 0.5h; Oxidation; | 79% |
α-iodo-α-phenylacetophenone
benzil
Conditions | Yield |
---|---|
With dimethyl sulfoxide at 100℃; for 2h; | 97% |
With dimethyl sulfoxide at 100℃; for 2h; | 97% |
With dimethyl sulfoxide at 130℃; for 1h; | 90% |
(R,R)-hydroxybenzoin
benzil
Conditions | Yield |
---|---|
With oxone; C18H17IN2O7PolS(1-)*Na(1+); tetra(n-butyl)ammonium hydrogensulfate In acetonitrile at 70℃; for 18h; Reagent/catalyst; Solvent; Sealed tube; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With water; iodine; oxygen In acetonitrile at 140℃; for 20h; Reagent/catalyst; Solvent; Temperature; Sealed tube; chemoselective reaction; | 96% |
With tert.-butylhydroperoxide; [Ru2Cl(3,6-bis(1-(2-pyridylmethyl)imidazol-2-yliden-3-yl)pyridazine)(CH3CN)4](PF6)3; sodium iodide In water; acetonitrile at 20℃; for 0.166667h; Catalytic behavior; Reagent/catalyst; Solvent; | 92% |
With tert.-butylhydroperoxide; (p-cymene)ruthenium(II) chloride; tetrabutylammonium iodide In water; toluene; acetonitrile at 20℃; for 1h; | 91% |
Conditions | Yield |
---|---|
With 4-methoxypyridine; lithium carbonate In N,N-dimethyl acetamide at 25℃; for 24h; Irradiation; | 96% |
With 4-methoxypyridine; tris(2,2'-bipyridine)ruthenium dichloride; lithium carbonate In N,N-dimethyl acetamide at 25℃; for 24h; Irradiation; | 81% |
With Amberlyst A-26; nitrate form In benzene for 2h; Heating; | 80% |
(benzoylphenylmethylene)triphenylphosphorane
benzil
Conditions | Yield |
---|---|
With potassium permanganate; magnesium sulfate In toluene at 50 - 60℃; for 20h; | 96% |
With N-Sulfonyloxaziridine 3 In dichloromethane at 25℃; for 0.5h; | 76% |
(Z)-1,2,3,4-tetraphenyl-2-butene-1,4-dione
benzil
Conditions | Yield |
---|---|
With formic acid; sulfuric acid for 0.0333333h; microwave irradiation; | 96% |
Conditions | Yield |
---|---|
With N-iodo-succinimide; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((S)-(6-methoxyquinolin-4-yl)((2S,4S,8R)-8-vinylquinuclidin-2-yl)methyl)urea In chloroform at 24℃; Concentration; Reagent/catalyst; Solvent; | 95% |
With 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; toluene-4-sulfonic acid In dichloromethane at 18℃; 1.) 0 deg C, 1 h, 2.) room temp., 72 h; | 88% |
With aluminium(III) phenoxide; p-benzoquinone; benzene |
Conditions | Yield |
---|---|
at 100℃; for 0.25h; | 100% |
With gallium(III) triflate In ethanol at 20℃; for 0.0833333h; | 100% |
With aluminum oxide at 20℃; for 0.166667h; neat (no solvent); | 100% |
Conditions | Yield |
---|---|
With gallium(III) triflate In acetonitrile at 20℃; for 0.0833333h; Reactivity; Solvent; Time; Concentration; | 100% |
With PEG-400 at 110℃; for 0.166667h; Neat (no solvent); | 100% |
With zirconium(IV) chloride In methanol at 20℃; for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
With gallium(III) triflate In ethanol at 20℃; for 0.0833333h; | 100% |
With 1,1,1,3',3',3'-hexafluoro-propanol at 20℃; for 1h; | 92% |
With acetic acid |
Conditions | Yield |
---|---|
at 160℃; for 0.25h; | 100% |
H6P2W18O62 In acetic acid at 20℃; for 0.0833333h; | 98% |
at 120℃; for 0.0583333h; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With titanium(III) chloride In acetone at 0℃; for 1h; | 100% |
Stage #1: benzil With sodium tetrahydroborate at 70℃; for 1.5h; Ball milling; neat (no solvent); Stage #2: With water regiospecific reaction; | 100% |
With hydrogen; palladium In methanol at 20℃; under 3800 Torr; for 46h; | 98% |
Conditions | Yield |
---|---|
With third generation polystyrene supported poly(amidoamine) dendrimer In ethanol at 50℃; for 2h; Knoevenagel condensation; | 100% |
With N,N-dimethyl-aniline In ethanol | |
With potassium carbonate In ethanol for 8h; Reflux; |
benzil
phosphorous acid trimethyl ester
2,2,2-trimethoxy-4,5-diphenyl-2,2-dihydro-1,3,2-dioxaphospholene
Conditions | Yield |
---|---|
100% | |
In benzene |
Conditions | Yield |
---|---|
With titanium(III) chloride In acetone at 0℃; for 1h; Product distribution; Mechanism; various reaction conditions; | 100% |
With titanium(III) chloride In acetone at 0℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With titanium(III) chloride In acetone at 40℃; for 1h; | 100% |
4,5-Diamino-6-(2-hydroxy-ethylamino)-2H-pyridazin-3-one
acetic acid
benzil
Acetic acid 2-(8-oxo-2,3-diphenyl-7,8-dihydro-pyrazino[2,3-d]pyridazin-5-ylamino)-ethyl ester
Conditions | Yield |
---|---|
for 6h; Heating; | 100% |
Conditions | Yield |
---|---|
With titanium(III) chloride In acetone at 0℃; for 1h; | 100% |
4,5-Diamino-6-(2-hydroxy-2-phenyl-ethylamino)-2-methyl-2H-pyridazin-3-one
benzil
8-(2-Hydroxy-2-phenyl-ethylamino)-6-methyl-2,3-diphenyl-6H-pyrazino[2,3-d]pyridazin-5-one
Conditions | Yield |
---|---|
In acetic acid Ambient temperature; | 100% |
benzil
<1,2-2H2>-1,2-diphenyl-1,2-ethanediol
Conditions | Yield |
---|---|
With sodium borodeuteride In methanol for 1h; Ambient temperature; | 100% |
With sodium borodeuteride; water-d2 In tetrahydrofuran at 0℃; for 1h; | 100% |
With lithium aluminium deuteride In diethyl ether at 20℃; for 4h; | 9.7 g |
Conditions | Yield |
---|---|
With bis(acetylacetonate)oxovanadium; oxygen; acetic acid at 80℃; under 760.051 Torr; for 8h; Sealed tube; | 100% |
With dihydrogen peroxide; sodium hydroxide In tetrahydrofuran; water at 0 - 20℃; for 1h; | 99% |
With Oxone In water; acetonitrile for 48h; Reflux; | 97% |
4,5-dimethyl-1,2-phenylenediamine
benzil
6,7-dimethyl-2,3-diphenylquinoxaline
Conditions | Yield |
---|---|
With aluminum oxide at 20℃; for 0.166667h; neat (no solvent); | 100% |
With amberlyst-15 In water at 70℃; for 0.2h; | 99% |
In benzene for 2h; cyclocondensation; Heating; | 97% |
Conditions | Yield |
---|---|
Product distribution; Further Variations:; Temperatures; in melt; solid-state reaction; | 100% |
at 20℃; for 1h; solid-state reaction; |
2-methyl-1H-indole-3-carbaldehyde
benzil
3-(4,5-diphenyl-1H-imidazol-2-yl)-2-methyl-1H-indole
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid Reflux; | 100% |
With ammonium acetate In acetic acid | |
With ammonium acetate In acetic acid for 3 - 5h; Heating / reflux; | |
With ammonium acetate In ethanol for 5h; Reflux; |
oxybis(diphenylborane)
benzamidine monohydrochloride
benzil
1,3,3,5,7-pentaphenyl-2,4-dioxa-8-aza-6-azonia-3-boratabicyclo{3.3.3}oct-6-ene
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol room temp.; crystn. from reaction mixt., washing (ethanol, ether), or evapn., extraction (hot ethanol), crystn. on cooling; elem. anal.; | 100% |
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid Reflux; | 100% |
With ammonium acetate In neat (no solvent) for 0.233333h; Microwave irradiation; Green chemistry; | 92% |
Conditions | Yield |
---|---|
Stage #1: (S)-1-phenylethanol With sec.-butyllithium In diethyl ether; hexane Stage #2: benzil In diethyl ether; hexane at -40 - 20℃; for 24h; Inert atmosphere; | 100% |
3,4,5-trimethoxy-benzaldehyde
benzil
urea
4,5‐diphenyl‐2‐(3,4,5‐trimethoxyphenyl)‐1H‐imidazole
Conditions | Yield |
---|---|
With ammonium acetate; zinc(II) chloride at 70 - 110℃; for 0.5h; Green chemistry; | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; Sealed tube; Schlenk technique; | 100% |
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