Products

Refine

Country

Business Type

Certificate

Display

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

(S)-(+)-2-Phenylglycinol Manufacturer/High quality/Best price/In stock

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality L-2-Phenylglycinol supplier in China

Cas:20989-17-7

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Wuhan Fortuna Chemical Co.,Ltd

Unique advantages of (S)-(+)-2-Phenylglycinol Cas 20989-17-7 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White to pale yellow crystalline powder Storage:cool dry place Package:1

Manufacturer high quality (S)-(+)-2-Phenylglycinol Cas 20989-17-7 with good price

Cas:20989-17-7

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply L-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality Oled CAS 20989-17-7 (S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap

(S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

(S)-(+)-α-Phenylglycinol

Cas:20989-17-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Density: 1.0630 (rough estimate) Melting point: 76-79 ° C Boiling point: 252.03 ° C (rough estimate) Specific rotation: -25.5 º (c=6, MeOH) Flash point: 125.3 ° C Solubility in chloroform, dimethyl sulfoxide and methanol Limited solu

(S)-(+)-2-Phenylglycinol 20989-17-7

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

20989-17-7 (S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top Purity CAS 20989-17-7 with fast shipping

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

(S)-(+)-2-Phenylglycinol/ LIDE PHARMA- Factory supply / Best price

Cas:20989-17-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

(S)-(+)-2-Amino-2-phenylethanolCAS:20989-17-7

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $20.0 / 30.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

(S)-(+)-2-Phenylglycinol 20989-17-7

Cas:20989-17-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

HANWAYS CHEMPHARM CO.,LIMITED

Hanways Chempharm Co., Limited, the former is Hubei Hanways Pharchem CO.,Limited, set up in 2009 in Wuhan, China. We specialize in sourcing and supplying APIs, pharmaceutical intermediates, and fine chemicals for worldwide markets. The founder has d

For Eliglustat (S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Trading Company

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

(S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $75.0 / 90.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

(S)-(+)-2-Phenylglycinol CAS:20989-17-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic

(S)-(+)-2-Phenylglycinol CAS:20989-17-7

Cas:20989-17-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

(S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:20989-17-7

Cas:20989-17-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Product Parameters Product Name (S)-(+)-2-Phenylglycinol CAS No. 20989-17-7 Appearance White or off-white crystalline powder Assay ≥99% Capacity 200mt/year MOQ 100G

Lonwin Chemical Group Limited

(S)-(+)-2-Phenylglycinol CAS: 20989-17-7 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The IR s

Factory supply (S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Leader Biochemical Group

PRODUCT DETAILS

China Largest Manufacturer factory sales (S)-(+)-2-Phenylglycinol CAS 20989-17-7

Cas:20989-17-7

Min.Order:500 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

L-2-Phenylglycinol

Cas:20989-17-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

(S)-(+)-2-PHENYLGLYCINOL

Cas:20989-17-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

L-2-Phenylglycinol

Cas:20989-17-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemsigma International Co.,Ltd.

superiority 1,high quality with competitive price in china market 2,fast and safe delivery,goods can be sent out immediately after payment. tracking number is available. 3,our products are with mature technical support. 4.packing as your re

(S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Metric Ton

FOB Price: $2.0 / 3.0

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

(S)-(+)-2-Phenylglycinol/Manufacturer/High quality/Best price

Cas:20989-17-7

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality L-2-Phenylglycinol

Cas:20989-17-7

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

(S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

(S)-(+)-2-Phenylglycinol Basic information Product Name: (S)-(+)-2-Phenylglycinol Synonyms: L-(+)-ALPHA-PHENYLGLYCINOL;L-(+)-A-PHENYLGLYCINOL;L-2-PHENYLGLYCINOL;L-beta-Aminophenethyl alcohol;H-PHG-OL;H-PHENYLGLYCINOL;H-L-PHG-OL;D-2-PHENYLGLYCIN

(S)-(+)-2-Phenylglycinol

Cas:20989-17-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

USP standard (S)-(+)-2-Phenylglycinol Manufacturer/High quality/Best price/In stock CAS NO.20989-17-7

Cas:20989-17-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Synthetic route

N-<(2R,4E)-2-Methyl-4-hexenoyl>-S-phenylglycinol
118958-06-8

N-<(2R,4E)-2-Methyl-4-hexenoyl>-S-phenylglycinol

A

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

B

(2R,4E)-2-Methyl-4-hexenoic acid
93553-73-2

(2R,4E)-2-Methyl-4-hexenoic acid

Conditions
ConditionsYield
With sulfuric acid In 1,4-dioxane at 70 - 80℃; for 3h;A 92%
B 99%
(S)-2-phenylglycine
2935-35-5

(S)-2-phenylglycine

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran Heating;97%
With lithium aluminium tetrahydride In tetrahydrofuran Heating;97%
With lithium aluminium tetrahydride In tetrahydrofuran Heating;95%
tert-butyl N-[(1S)-2-hydroxy-1-phenylethyl]carbamate
117049-14-6

tert-butyl N-[(1S)-2-hydroxy-1-phenylethyl]carbamate

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
In acetonitrile at 300℃; under 75007.5 Torr;93%
(S)-Phenylglycine methyl ester
6591-61-3, 24461-61-8, 26682-99-5, 37760-98-8

(S)-Phenylglycine methyl ester

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 1.5h; Reflux;88%
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 1.5h; Reflux;88%
Stage #1: (S)-Phenylglycine methyl ester With sodium tetrahydroborate In tetrahydrofuran at 65℃; for 0.25h;
Stage #2: With methanol In tetrahydrofuran at 65℃; stereospecific reaction;
73%
With sodium tetrahydroborate In methanol at 20℃; for 1h;
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 1h; Cooling with ice; Inert atmosphere;
(S)-4-phenyl-2-oxazolidinone
99395-88-7

(S)-4-phenyl-2-oxazolidinone

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With 3-azapentane-1,5-diamine at 140℃; for 18h;85%
L-2-phenylglycine methyl ester hydrochloride
15028-39-4

L-2-phenylglycine methyl ester hydrochloride

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol 1) RT, 9h, b) 5.5h, reflux, c) RT, 8h;83%
With sodium tetrahydroborate In ethanol; water for 5.5h; Heating;
Stage #1: L-2-phenylglycine methyl ester hydrochloride With triethylamine In methanol; diethyl ether at -10℃; for 1h;
Stage #2: With sodium tetrahydroborate In methanol at 0 - 20℃;
4.4 g
N-(2-methoxymethoxy-1-phenyl-ethyl)-acetamide
217650-36-7

N-(2-methoxymethoxy-1-phenyl-ethyl)-acetamide

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
In methanol Hydrolysis; Acid hydrolysis;81%
benzyl (S)-(2-hydroxy-1-phenylethyl)carbamate
130406-31-4

benzyl (S)-(2-hydroxy-1-phenylethyl)carbamate

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With hydrogen; palladium dihydroxide In methanol for 0.25h;80%

A

(R)-Phenylglycinol
56613-80-0

(R)-Phenylglycinol

B

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With hydrogenchloride; (S)-(+)-3,3′-bis(3,5-bis(trifluoromethyl)phenyl)-1,1′-binaphthyl-2,2′-diyl hydrogenphosphate In dichloromethane; water at 21.84℃; pH=2.32; Centrifugal contactor separators; Resolution of racemate; optical yield given as %ee;A n/a
B 36%
With chiral stationary phase including isopropyl-functionalized CF6 In methanol; acetic acid; triethylamine; acetonitrile at 20℃; Purification / work up;
With 3,3'-bis[3,5-bis(trifluoromethyl)phenyl]-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In tetrachloromethane at 6℃; pH=3; aq. buffer; enantioselective reaction;
(S)-2-phenylglycine
2935-35-5

(S)-2-phenylglycine

A

(2S)-(-)-2-amino-2-phenylethanol N-borane

(2S)-(-)-2-amino-2-phenylethanol N-borane

B

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Stage #1: (S)-2-phenylglycine With sodium tetrahydroborate; sulfuric acid In tetrahydrofuran; diethyl ether at 0 - 20℃; for 20h; Inert atmosphere;
Stage #2: With hydrogenchloride In water at 20℃; for 2h;
A 27%
B 33%
(S)-phenylglycine ethyl ester
15962-49-9

(S)-phenylglycine ethyl ester

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With lithium aluminium tetrahydride
(S)-2-azido-2-phenylethanol
126923-25-9

(S)-2-azido-2-phenylethanol

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran Heating; Yield given;
(1S,2S,5S)-3-[(E)-(S)-2-Hydroxy-1-phenyl-ethylimino]-2,6,6-trimethyl-bicyclo[3.1.1]heptan-2-ol
127718-96-1

(1S,2S,5S)-3-[(E)-(S)-2-Hydroxy-1-phenyl-ethylimino]-2,6,6-trimethyl-bicyclo[3.1.1]heptan-2-ol

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With hydroxylamine acetate In ethanol for 20h; Ambient temperature; Yield given;
tert-butyl 2-hydroxy-1-phenylethylcarbamate
102089-74-7, 117049-14-6, 138457-46-2, 67341-01-9

tert-butyl 2-hydroxy-1-phenylethylcarbamate

A

(R)-Phenylglycinol
56613-80-0

(R)-Phenylglycinol

B

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane for 1h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
(1S,1'S)-N-2'-hydroxy-1'-phenylethyl-1-phenylethylamine
126927-38-6

(1S,1'S)-N-2'-hydroxy-1'-phenylethyl-1-phenylethylamine

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With hydrogen S, Ram, L. D. Spicer Synth. Commun. 1987, 17, 415.;
(R)-Styrene oxide
20780-53-4

(R)-Styrene oxide

A

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

B

(R)-2-Amino-1-phenylethanol
2549-14-6

(R)-2-Amino-1-phenylethanol

Conditions
ConditionsYield
With ammonium hydroxide In water at 130℃; under 9000.72 Torr; microwave irradiation;A 20 % Chromat.
B 80 % Chromat.
(S)-2-Hydrazino-2-phenyl-ethanol

(S)-2-Hydrazino-2-phenyl-ethanol

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
With hydrogen; nickel In methanol at 25℃; under 25857.4 Torr; for 28h;0.136 g
C18H26N2O5
1026035-75-5

C18H26N2O5

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NaBH4 / methanol
2: TFA / CH2Cl2 / 3 h / 20 °C
3: 0.136 g / H2 / Raney-Ni / methanol / 28 h / 25 °C / 25857.4 Torr
View Scheme
C18H28N2O5
1027539-12-3

C18H28N2O5

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: TFA / CH2Cl2 / 3 h / 20 °C
2: 0.136 g / H2 / Raney-Ni / methanol / 28 h / 25 °C / 25857.4 Torr
View Scheme
phenylacetaldehyde
122-78-1

phenylacetaldehyde

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: D-proline / CH2Cl2 / 3 h / 20 °C
2: NaBH4 / methanol
3: TFA / CH2Cl2 / 3 h / 20 °C
4: 0.136 g / H2 / Raney-Ni / methanol / 28 h / 25 °C / 25857.4 Torr
View Scheme
ethyl 2-(hydroxyimino)-2-phenylacetate
131934-09-3, 135765-81-0, 712-41-4

ethyl 2-(hydroxyimino)-2-phenylacetate

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 85 percent / NaBH4; I2 / tetrahydrofuran / 4 h / Heating
2.1: dibenzoyl-L-tartaric acid / acetone / 6 h / 25 °C
2.2: aq. KOH / CH2Cl2
View Scheme
(4-Methoxy-phenyl)-[(S)-1-phenyl-2-((R)-toluene-4-sulfinyl)-ethyl]-amine
121411-08-3

(4-Methoxy-phenyl)-[(S)-1-phenyl-2-((R)-toluene-4-sulfinyl)-ethyl]-amine

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 80 percent / CAN / H2O; acetonitrile / 0.5 h / 0 °C
2: 80 percent / K2CO3 / dioxane; H2O / 0.17 h / Ambient temperature
3: 1.) (CF3CO)2O, sym-collidine, 2.) K2CO3, NaBH4 / 1.) MeCN, 0 deg C, 5 min, 2.) H2O, 0 deg C to room temperature, 15 min
4: 80 percent / H2 / Pd(OH)2/C / methanol / 0.25 h
View Scheme
benzaldehyde
100-52-7

benzaldehyde

HI, I2

HI, I2

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 70 percent / DOWEX 50W X8-400 / benzene / Heating
2: LDA / tetrahydrofuran; hexane / -70 °C / 1.) 15 min, 2.) 30 min
3: 80 percent / CAN / H2O; acetonitrile / 0.5 h / 0 °C
4: 80 percent / K2CO3 / dioxane; H2O / 0.17 h / Ambient temperature
5: 1.) (CF3CO)2O, sym-collidine, 2.) K2CO3, NaBH4 / 1.) MeCN, 0 deg C, 5 min, 2.) H2O, 0 deg C to room temperature, 15 min
6: 80 percent / H2 / Pd(OH)2/C / methanol / 0.25 h
View Scheme
Multi-step reaction with 3 steps
1: 4 Angstroem mol. sieves / CH2Cl2
2: TiCl4 / 15 °C / Irradiation
3: H2 / S, Ram, L. D. Spicer Synth. Commun. 1987, 17, 415.
View Scheme
4-methoxy-N-[(E)-phenylmethylidene]aniline
1613-90-7

4-methoxy-N-[(E)-phenylmethylidene]aniline

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: LDA / tetrahydrofuran; hexane / -70 °C / 1.) 15 min, 2.) 30 min
2: 80 percent / CAN / H2O; acetonitrile / 0.5 h / 0 °C
3: 80 percent / K2CO3 / dioxane; H2O / 0.17 h / Ambient temperature
4: 1.) (CF3CO)2O, sym-collidine, 2.) K2CO3, NaBH4 / 1.) MeCN, 0 deg C, 5 min, 2.) H2O, 0 deg C to room temperature, 15 min
5: 80 percent / H2 / Pd(OH)2/C / methanol / 0.25 h
View Scheme
(S)-1-Phenyl-2-((R)-toluene-4-sulfinyl)-ethylamine
224433-92-5

(S)-1-Phenyl-2-((R)-toluene-4-sulfinyl)-ethylamine

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 80 percent / K2CO3 / dioxane; H2O / 0.17 h / Ambient temperature
2: 1.) (CF3CO)2O, sym-collidine, 2.) K2CO3, NaBH4 / 1.) MeCN, 0 deg C, 5 min, 2.) H2O, 0 deg C to room temperature, 15 min
3: 80 percent / H2 / Pd(OH)2/C / methanol / 0.25 h
View Scheme
[(S)-1-Phenyl-2-((R)-toluene-4-sulfinyl)-ethyl]-carbamic acid benzyl ester
224433-96-9

[(S)-1-Phenyl-2-((R)-toluene-4-sulfinyl)-ethyl]-carbamic acid benzyl ester

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) (CF3CO)2O, sym-collidine, 2.) K2CO3, NaBH4 / 1.) MeCN, 0 deg C, 5 min, 2.) H2O, 0 deg C to room temperature, 15 min
2: 80 percent / H2 / Pd(OH)2/C / methanol / 0.25 h
View Scheme
N-benzylidene-(S)-α-methylbenzylamine
69350-13-6

N-benzylidene-(S)-α-methylbenzylamine

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: TiCl4 / 15 °C / Irradiation
2: H2 / S, Ram, L. D. Spicer Synth. Commun. 1987, 17, 415.
View Scheme
1-phenyl-2-hydroxyethanone
582-24-1

1-phenyl-2-hydroxyethanone

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: LiH / dimethylformamide
2: H2NOH*HCl; NaOAc / ethanol; H2O
3: Fe / dimethylformamide
4: 100 percent / H2 / {1,2-bis[(R,R)-2,5-dimethylphospholane]benzene}rhodium(I) / toluene / 20 °C / 7600 Torr
5: 81 percent / methanol / Acid hydrolysis
View Scheme
With ω-transaminase from Arthrobacter; isopropylamine In tert-butyl methyl ether at 25℃; for 24h; Enzymatic reaction; enantioselective reaction;n/a
With (R)-1-phenyl-ethyl-amine; (R)-ω-transaminase from Mycobacterium vanbaalenii; NAD Enzymatic reaction; enantioselective reaction;
2-methoxymethoxy-1-phenyl-ethanone
103548-06-7

2-methoxymethoxy-1-phenyl-ethanone

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: H2NOH*HCl; NaOAc / ethanol; H2O
2: Fe / dimethylformamide
3: 100 percent / H2 / {1,2-bis[(R,R)-2,5-dimethylphospholane]benzene}rhodium(I) / toluene / 20 °C / 7600 Torr
4: 81 percent / methanol / Acid hydrolysis
View Scheme
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

(S)-2-(tert-butyldimethylsilyloxy)-1-phenylethylamine
120417-13-2

(S)-2-(tert-butyldimethylsilyloxy)-1-phenylethylamine

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃; for 41h; Substitution;100%
With dmap; triethylamine In dichloromethane at 20℃; for 12h;85%
With dmap; triethylamine In dichloromethane at 20℃;85%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

acetoacetic acid methyl ester
105-45-3

acetoacetic acid methyl ester

(Z)-3-((S)-2-Hydroxy-1-phenyl-ethylamino)-but-2-enoic acid methyl ester
476187-10-7

(Z)-3-((S)-2-Hydroxy-1-phenyl-ethylamino)-but-2-enoic acid methyl ester

Conditions
ConditionsYield
In methanol for 24h; Heating;100%
formaldehyd
50-00-0

formaldehyd

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(S)-2-(N,N-dimethylamino)-2-phenylethanol
95977-53-0

(S)-2-(N,N-dimethylamino)-2-phenylethanol

Conditions
ConditionsYield
With HCOOH (98percent) In water for 18h; Heating;100%
4-(4-chlorophenyl)-4-oxobutanoic acid
3984-34-7

4-(4-chlorophenyl)-4-oxobutanoic acid

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(3S,7aS)-7a-(4-Chloro-phenyl)-3-phenyl-tetrahydro-pyrrolo[2,1-b]oxazol-5-one
873577-48-1

(3S,7aS)-7a-(4-Chloro-phenyl)-3-phenyl-tetrahydro-pyrrolo[2,1-b]oxazol-5-one

Conditions
ConditionsYield
In toluene for 16h; Heating;100%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

4-(2,4-dichlorophenyl)-4-oxobutanoic acid
58457-57-1

4-(2,4-dichlorophenyl)-4-oxobutanoic acid

(3S,7aS)-7a-(2,4-Dichloro-phenyl)-3-phenyl-tetrahydro-pyrrolo[2,1-b]oxazol-5-one
808186-29-0

(3S,7aS)-7a-(2,4-Dichloro-phenyl)-3-phenyl-tetrahydro-pyrrolo[2,1-b]oxazol-5-one

Conditions
ConditionsYield
In toluene for 16h; Heating;100%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

4-(2,4-difluorophenyl)-4-oxobutanoic acid
110931-77-6

4-(2,4-difluorophenyl)-4-oxobutanoic acid

(3S,7aS)-7a-(2,4-Difluoro-phenyl)-3-phenyl-tetrahydro-pyrrolo[2,1-b]oxazol-5-one
808186-32-5

(3S,7aS)-7a-(2,4-Difluoro-phenyl)-3-phenyl-tetrahydro-pyrrolo[2,1-b]oxazol-5-one

Conditions
ConditionsYield
In toluene for 16h; Heating;100%
2-methyl-benzyl alcohol
89-95-2

2-methyl-benzyl alcohol

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

2-{(E)-((1S)-2-hydroxy-1-phenylethylimino)methyl}phenol
113866-46-9, 129049-04-3, 129049-05-4

2-{(E)-((1S)-2-hydroxy-1-phenylethylimino)methyl}phenol

Conditions
ConditionsYield
With sodium sulfate In methanol for 12h; Heating;100%
In ethanol at 20℃;
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

ethyl 5-formyl-3-methoxy-4-methyl-1H-pyrrole-2-carboxylate
15431-67-1

ethyl 5-formyl-3-methoxy-4-methyl-1H-pyrrole-2-carboxylate

ethyl 4-methyl-3-methoxy-5-[(L-phenylglycinolimino)methyl]-1H-pyrrole-2-carboxylate

ethyl 4-methyl-3-methoxy-5-[(L-phenylglycinolimino)methyl]-1H-pyrrole-2-carboxylate

Conditions
ConditionsYield
With magnesium sulfate In dichloromethane100%
(3E,5E)-7-(tert-Butyl-dimethyl-silanyloxy)-2-[2-oxo-eth-(Z)-ylidene]-hepta-3,5-dienoic acid ethyl ester

(3E,5E)-7-(tert-Butyl-dimethyl-silanyloxy)-2-[2-oxo-eth-(Z)-ylidene]-hepta-3,5-dienoic acid ethyl ester

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

5-[3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-3-phenyl-2,3,6,8a-tetrahydro-5H-oxazolo[3,2-a]pyridine-7-carboxylic acid ethyl ester

5-[3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-3-phenyl-2,3,6,8a-tetrahydro-5H-oxazolo[3,2-a]pyridine-7-carboxylic acid ethyl ester

Conditions
ConditionsYield
In chloroform-d1 at 24℃;100%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

ethyl (E,E)-4-oxo-2-styrylbut-2-enoate
344907-95-5

ethyl (E,E)-4-oxo-2-styrylbut-2-enoate

3,5-diphenyl-2,3,6,8a-tetrahydro-5H-oxazolo[3,2-a]pyridine-7-carboxylic acid ethyl ester

3,5-diphenyl-2,3,6,8a-tetrahydro-5H-oxazolo[3,2-a]pyridine-7-carboxylic acid ethyl ester

Conditions
ConditionsYield
In chloroform-d1 at 24℃;100%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

acrolein
107-02-8

acrolein

(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine
1055874-41-3

(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

Conditions
ConditionsYield
In chloroform at 20℃; for 0.0833333h;100%
In toluene at 20℃; for 15h; Molecular sieve;36%
hex-5-en-1-al
764-59-0

hex-5-en-1-al

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(4S)-2-(pent-4-en-1-yl)-4-phenyloxazolidine

(4S)-2-(pent-4-en-1-yl)-4-phenyloxazolidine

Conditions
ConditionsYield
With magnesium sulfate In dichloromethane Inert atmosphere;100%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

C49H61O2P

C49H61O2P

C57H70NO2P

C57H70NO2P

Conditions
ConditionsYield
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; Inert atmosphere; Cooling with ice;100%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

tert-butyl N-[(1S)-2-hydroxy-1-phenylethyl]carbamate
117049-14-6

tert-butyl N-[(1S)-2-hydroxy-1-phenylethyl]carbamate

Conditions
ConditionsYield
In acetonitrile at 20℃; for 3h; Acylation;99%
In chloroform at 0 - 20℃;97%
With triethylamine In tetrahydrofuran for 2h;96%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(4S,5S)-2,2-Dimethyl-[1,3]dioxolane-4,5-dicarboxylic acid bis-[((S)-2-hydroxy-1-phenyl-ethyl)-amide]
182966-70-7

(4S,5S)-2,2-Dimethyl-[1,3]dioxolane-4,5-dicarboxylic acid bis-[((S)-2-hydroxy-1-phenyl-ethyl)-amide]

Conditions
ConditionsYield
at 120℃; for 3h;99%
(E)-3-phenylpropenal
14371-10-9

(E)-3-phenylpropenal

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(S)-2-Phenyl-2-[(E)-3-phenyl-prop-2-en-(E)-ylideneamino]-ethanol

(S)-2-Phenyl-2-[(E)-3-phenyl-prop-2-en-(E)-ylideneamino]-ethanol

Conditions
ConditionsYield
In diethyl ether for 1.33333h; Ambient temperature;99%
carbon disulfide
75-15-0

carbon disulfide

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(S)-4-phenyl-1,3-oxazolidine-2-thione
190970-57-1

(S)-4-phenyl-1,3-oxazolidine-2-thione

Conditions
ConditionsYield
With dihydrogen peroxide; potassium carbonate In ethanol at 50℃;99%
Stage #1: carbon disulfide; (2S)-2-phenylglycinol With triethylamine In methanol at 20℃; for 0.5h;
Stage #2: With dihydrogen peroxide In methanol
95%
With dihydrogen peroxide; potassium carbonate In ethanol at 50℃; for 0.0833333h;80%
2-methoxy-6-methyl-benzaldehyde
54884-55-8

2-methoxy-6-methyl-benzaldehyde

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol
702684-35-3

(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

Conditions
ConditionsYield
With 4A MS In ethanol at 20℃; for 26h;99%
(R)-1,1'-spirobiindane-7,7'-dicaboxylic acid
920985-42-8, 856407-39-1

(R)-1,1'-spirobiindane-7,7'-dicaboxylic acid

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(Ra,S,S)-N,N'-bis(2-hydroxy-1-phenylethyl)-1,1'-spirobiindane-7,7'-diamide

(Ra,S,S)-N,N'-bis(2-hydroxy-1-phenylethyl)-1,1'-spirobiindane-7,7'-diamide

Conditions
ConditionsYield
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In tetrahydrofuran at -5 - 20℃;99%
trans-2-phenylvinylboronic acid
6783-05-7

trans-2-phenylvinylboronic acid

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

glyoxalic acid monohydrate
6000-59-5

glyoxalic acid monohydrate

D-homophenylalanine
82795-51-5

D-homophenylalanine

Conditions
ConditionsYield
In dichloromethane99%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

acetoacetic acid methyl ester
105-45-3

acetoacetic acid methyl ester

C14H18O3

C14H18O3

Conditions
ConditionsYield
In toluene at 20℃; for 4h; Molecular sieve;99%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
82911-69-1

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

(2-hydroxy-1-phenylethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
215178-44-2

(2-hydroxy-1-phenylethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
In 1,4-dioxane; water at 20℃; for 16h;99%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

formic acid ethyl ester
109-94-4

formic acid ethyl ester

(+)-(2S)-2-(formylamino)-2-phenylethanol

(+)-(2S)-2-(formylamino)-2-phenylethanol

Conditions
ConditionsYield
Reflux;99%
3,3-dimethylglutaric anhydride
4160-82-1

3,3-dimethylglutaric anhydride

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid
1327278-20-5

3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

Conditions
ConditionsYield
In dichloromethane; toluene at 20 - 60℃; for 5.5h;99%
4-Bromobenzoic acid
586-76-5

4-Bromobenzoic acid

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

(S)-4-bromo-N-(2-hydroxy-1-phenylethyl)benzamide

(S)-4-bromo-N-(2-hydroxy-1-phenylethyl)benzamide

Conditions
ConditionsYield
With 4-methyl-morpholine; benzotriazol-1-ol; 1,2-dichloro-ethane In N,N-dimethyl-formamide at 25℃; for 20h; Solvent; chemoselective reaction;99%
With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate In tetrahydrofuran at 20℃; for 20h;60%
2-amino-3-pyridinecarbonitrile
24517-64-4

2-amino-3-pyridinecarbonitrile

(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

3-[(4S)-4-phenyl-4,5-dihydro-1,3-oxazol-2-yl]pyridine-2-amine

3-[(4S)-4-phenyl-4,5-dihydro-1,3-oxazol-2-yl]pyridine-2-amine

Conditions
ConditionsYield
With zinc(II) chloride In chlorobenzene at 60℃; for 96h; Inert atmosphere;99%

Hot Products

Post buying leads

About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia

Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog

©2008 LookChem.com,License: ICP

NO.:Zhejiang16009103

complaints:service@lookchem.com Desktop View