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thiophosgene
sodium 2-naphtholate
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
With chloroform | |
In chloroform at 25℃; for 1h; |
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water for 1h; | |
With sodium hydroxide In dichloromethane; water at 20℃; for 1h; Cooling with ice; |
O-2-naphthalenyl-carbonochloridothioate
methyl-alpha-D-glucopyranoside
methyl 2-O-(2-naphthoxy)thiocarbonyl-α-D-glucopyranoside
Conditions | Yield |
---|---|
Stage #1: methyl-alpha-D-glucopyranoside With di-n-octyltin dichloride In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: O-2-naphthalenyl-carbonochloridothioate With 1,2,2,6,6-pentamethylpiperidine; tetra-(n-butyl)ammonium iodide In tetrahydrofuran at 20℃; for 6h; regioselective reaction; | 99% |
O-2-naphthalenyl-carbonochloridothioate
methyl beta-D-glucopyranoside
methyl-alpha-D-glucopyranoside
A
methyl 2-O-(2-naphthoxy)thiocarbonyl-α-D-glucopyranoside
B
methyl 6-O-(2-naphthoxy)thiocarbonyl-β-D-glucopyranoside
Conditions | Yield |
---|---|
Stage #1: methyl beta-D-glucopyranoside; methyl-alpha-D-glucopyranoside With dibutyltin chloride In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: O-2-naphthalenyl-carbonochloridothioate With 1,2,2,6,6-pentamethylpiperidine; tetra-(n-butyl)ammonium iodide In tetrahydrofuran at 20℃; chemoselective reaction; | A 99% B 2% |
Stage #1: methyl beta-D-glucopyranoside; methyl-alpha-D-glucopyranoside With dimethyltin dichloride In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: O-2-naphthalenyl-carbonochloridothioate With 1,2,2,6,6-pentamethylpiperidine; 3,5-Lutidine In tetrahydrofuran at 20℃; chemoselective reaction; | A 3% B 80% |
O-2-naphthalenyl-carbonochloridothioate
N-methylaniline
O-(2-naphthyl) N-methyl-N-phenyl thiocarbamate
Conditions | Yield |
---|---|
In dichloromethane for 0.166667h; | 88% |
(S)-1-[4-((S)-4-hydroxy-6-aza-spiro[2.5]oct-6-yl)-butyl]-3-methyl-piperazin-2-one
O-2-naphthalenyl-carbonochloridothioate
(S)-4-[4-((S)-4-Hydroxy-6-aza-spiro[2.5]oct-6-yl)-butyl]-2-methyl-3-oxo-piperazine-1-carbothioic acid O-naphthalen-2-yl ester
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran | 64% |
ethanol
O-2-naphthalenyl-carbonochloridothioate
N-(naphthalen-2-yl)benzothioamide
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
With sodium hydroxide; benzene | |
With sodium hydroxide; chloroform |
N-(naphthalen-1-yl)benzothioamide
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
With sodium hydroxide; benzene | |
With sodium hydroxide; chloroform |
O-2-naphthalenyl-carbonochloridothioate
N-Phenylbenzothioamide
Conditions | Yield |
---|---|
With sodium hydroxide; benzene | |
With sodium hydroxide; chloroform |
morpholine
O-2-naphthalenyl-carbonochloridothioate
morpholine-1-carbothioic acid O-naphthalen-2-yl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate |
O-2-naphthalenyl-carbonochloridothioate
(3S,4R)-1-(allyloxycarbonyl)methyl-3-<(R)-1-hydroxyethyl>-4-sulfhydryl-2-azetidinone
(3R,4R)-1-<<(allyloxy)carbonyl>methyl>-3-<(R)-1-hydroxyethyl>-4-β-naphthoxy(thiocarbonyl)thio-2-azetidinone
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 0.833333h; Yield given; |
O-2-naphthalenyl-carbonochloridothioate
(3S,4R)-1-<<(allyloxy)carbonyl>methyl>-3-<(R)-1-hydroxyethyl>-4-<(triphenylmethyl)thio>-2-azetidinone
(3R,4R)-1-<<(allyloxy)carbonyl>methyl>-3-<(R)-1-hydroxyethyl>-4-β-naphthoxy(thiocarbonyl)thio-2-azetidinone
Conditions | Yield |
---|---|
With pyridine; silver nitrate 1) MeOH, RT, 2h, 2a) THF, 40 deg C, 0.5h, 2b) 0.75 h, reflux; Yield given. Multistep reaction; |
O-2-naphthalenyl-carbonochloridothioate
(3S,4R)-1-<<(allyloxy)carbonyl>methyl>-3-<(R)-1-(tetrahydropyranyloxy)ethyl>-4-<(triphenylmethyl)thio>-2-azetidinone
(3S,4R)-1-<<(allyloxy)carbonyl>methyl>-3-<(R)-1-(tetrahydropyranyloxy)ethyl>-4-<<β-naphthoxy(thiocarbonyl)>thio>-2-azetidinone
Conditions | Yield |
---|---|
With pyridine; methanol; silver nitrate 1.) CH3CN, RT, 18 h, 2.) CH2Cl2, 0 deg C, 30 min; Yield given. Multistep reaction; |
O-2-naphthalenyl-carbonochloridothioate
cyclohexylamine
Conditions | Yield |
---|---|
In chloroform at 25℃; for 4h; | 86 mg |
O-2-naphthalenyl-carbonochloridothioate
N-methyl-N-phenyl-2-naphthylamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 0.17 h 2: triethylsilane; 2,2-bis(tert-butylperoxy)butane / benzene / 3.5 h / 135 °C View Scheme |
O-2-naphthalenyl-carbonochloridothioate
A
O-(naphthalen-2-yl) N,N-dimethylcarbamothioate
B
β-naphthyl N-cyclohexyl-N-methylthiocarbamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
O-2-naphthalenyl-carbonochloridothioate
O-(naphthalen-2-yl) N,N-dimethylcarbamothioate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
O-2-naphthalenyl-carbonochloridothioate
β-naphthyl N,N-diethylthiocarbamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme | |
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
O-2-naphthalenyl-carbonochloridothioate
β-naphthyl piperidine-1-thiocarboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
O-2-naphthalenyl-carbonochloridothioate
morpholine-1-carbothioic acid O-naphthalen-2-yl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
O-2-naphthalenyl-carbonochloridothioate
β-naphthyl N-(4-chlorobutyl)-N-methylthiocarbamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
O-2-naphthalenyl-carbonochloridothioate
β-naphthyl N-allyl-N-methylthiocarbamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane / 25 °C 2: dimethyl sulfate; water View Scheme |
N,N'-dimethylbenzylamine
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
In dichloromethane at 25℃; |
Conditions | Yield |
---|---|
In dichloromethane at 25℃; |
N-methylcyclohexylamine
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
In dichloromethane at 25℃; |
4-methyl-morpholine
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
In dichloromethane at 25℃; |
1-Methylpyrrolidine
O-2-naphthalenyl-carbonochloridothioate
Conditions | Yield |
---|---|
In dichloromethane at 25℃; |
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