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inquiryN,N'-BIS(1-HEXYLHEPTYL)-PERYLENE-3,4:9,10-BIS-(DICARBOXIMIDE) CAS:110590-84-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermedia
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N,N'-BIS(1-HEXYLHEPTYL)-PERYLENE-3,4:9,10-BIS-(DICARBOXIMIDE)
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inquiry1-hexylheptylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With 1H-imidazole at 180℃; for 5h; | 100% |
With 1H-imidazole In dichloromethane at 150℃; for 5h; | 100% |
With 1H-imidazole; zinc diacetate at 155℃; for 4h; | 99% |
1H-imidazole
1-hexylheptylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
C
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
at 160℃; for 4h; | A 0.7% B 0.07% C 82% |
propyl bromide
A
N-(1-hexylheptyl)-9,10-bis(propyloxycarbonyl)perylene-3,4-dicarboximide
B
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 25℃; for 16h; | A 58% B 15% |
1-hexylheptylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
A
PERYLENE
B
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
C
2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione
Conditions | Yield |
---|---|
With 1H-imidazole; zinc diacetate; water at 190℃; for 24h; | A n/a B 15% C 27% |
tridecan-7-one
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / NH4OAc; NaBH3CN / methanol / 48 h / 20 °C 2: imidazole / 5 h / 180 °C View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate; sodium cyanoborohydride / methanol / 56 h / 20 °C 2: 1H-imidazole / 3 h / 130 °C View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate; sodium cyanoborohydride / methanol / 60 h / 20 °C 2: 1H-imidazole / 4 h / 160 °C View Scheme |
tridecan-7-one oxime
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium-dihydrobis(2-methoxyethoxy)aluminate / toluene / 4 h / 140 °C 2: 41 percent / imidazole / 4 h / 160 °C View Scheme | |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran 2: 1H-imidazole / 150 °C View Scheme |
1-hexylheptylamine
4-(5,5-dimethyl-1,3-dioxan-2-yl)benzylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
B
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With 1H-imidazole at 160℃; for 24h; |
1-hexylheptylamine
A
N-(1-hexylheptyl)-9,10-bis(propyloxycarbonyl)perylene-3,4-dicarboximide
B
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 16 h / 25 °C 1.2: 72 h / 25 °C 2.1: N,N-dimethyl-formamide / 16 h / 25 °C View Scheme |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
A
N-(1-hexylheptyl)-9,10-bis(propyloxycarbonyl)perylene-3,4-dicarboximide
B
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 16 h / 25 °C 1.2: 72 h / 25 °C 2.1: N,N-dimethyl-formamide / 16 h / 25 °C View Scheme |
tridecan-7-one
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
Stage #1: tridecan-7-one With ammonium acetate; sodium cyanoborohydride In methanol at 20℃; for 48h; Inert atmosphere; Stage #2: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With 1H-imidazole at 130℃; for 3h; Inert atmosphere; | 8.57 g |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
N,N’-di-(1-hexylheptyl)-1-nitroperylene-3,4,9,10-tetracarboxydianhydride
Conditions | Yield |
---|---|
With nitric acid In dichloromethane at 20℃; | 96% |
With methanesulfonic acid; dinitrogen tetraoxide In dichloromethane at 20℃; for 7h; Substitution; | 93% |
styrene
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; [RhCl2(p-cymene)]2; copper(II) acetate monohydrate; Trimethylacetic acid In 1,2-dichloro-ethane at 20 - 120℃; for 96h; Reagent/catalyst; Time; Schlenk technique; stereoselective reaction; | 96% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With bromine; potassium carbonate In chlorobenzene at 60℃; for 24h; Bromination; | 86% |
With bromine at 20℃; for 96h; | 65% |
With bromine In dichloromethane at 20℃; for 48h; | 45% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; (p-cymene)ruthenium(II) chloride; copper(II) acetate monohydrate; acetic acid In 1,2-dichloro-ethane at 20 - 120℃; for 96h; Schlenk technique; stereoselective reaction; | 82% |
tetrabutylammomium bromide
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
Stage #1: N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide With hydroxy-2-propanone; sodium hydroxide In ethanol; water at 50 - 55℃; for 0.166667h; Inert atmosphere; Stage #2: tetrabutylammomium bromide In ethanol; water Inert atmosphere; | 82% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
bis(pinacol)diborane
N,N'-bis(1-hexylheptyl)-2,5,8,11-tetra(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)perylene-3,4:9,10-tetracarboxylic acid bisimide
Conditions | Yield |
---|---|
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; tris(pentafluorophenyl)phosphine In 1,4-dioxane at 110℃; for 48h; Inert atmosphere; regioselective reaction; | 78% |
acrylic acid n-butyl ester
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; (p-cymene)ruthenium(II) chloride; copper(II) acetate monohydrate; acetic acid In 1,2-dichloro-ethane at 20 - 120℃; for 96h; Schlenk technique; stereoselective reaction; | 78% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
acrylic acid methyl ester
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; (p-cymene)ruthenium(II) chloride; copper(II) acetate monohydrate; acetic acid In 1,2-dichloro-ethane at 20 - 120℃; for 96h; Solvent; Reagent/catalyst; Schlenk technique; stereoselective reaction; | 77% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
N-(1-hexylheptyl)-perylene-3,4,9,10-tetracarboxylic-3,4-carboximide-9,10-anhydride
Conditions | Yield |
---|---|
Stage #1: N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide With potassium tert-butylate; water In tert-butyl alcohol for 2h; Reflux; Stage #2: With hydrogenchloride In water; acetic acid; tert-butyl alcohol at 20℃; | 76% |
With potassium hydroxide In tert-butyl alcohol for 0.333333h; Heating; | 59% |
With potassium hydroxide In tert-butyl alcohol at 90℃; for 0.5h; | 46% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
butan-1-ol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 24h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | A 75% B 72 %Spectr. C 28 %Spectr. |
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; | A 6% B 72 %Spectr. C 28%Spectr. |
maleic anhydride
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
2,10-bis(1-hexylheptyl)furo[3′,4′:4,5]pyreno-[2,1,10-def:7,8,9-d′e′f ′]diisoquinoline-1,3,5,7,9,11(2H,10H)-hexone
Conditions | Yield |
---|---|
With chloranil In acetone at 125℃; for 96h; Aromatisation; Diels-Alder reaction; | 71% |
Hexanethiol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In tetrahydrofuran at 70℃; for 24h; Reagent/catalyst; Inert atmosphere; | A 66% B n/a C 15% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
ethyl acrylate
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; (p-cymene)ruthenium(II) chloride; copper(II) acetate monohydrate; acetic acid In 1,2-dichloro-ethane at 20 - 120℃; for 96h; Schlenk technique; stereoselective reaction; | 65% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
A
N-(1-hexylheptyl)-perylene-3,4,9,10-tetracarboxylic-3,4-carboximide-9,10-anhydride
B
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
With potassium hydroxide In tert-butyl alcohol for 0.166667h; Heating; | A 63% B n/a |
With potassium hydroxide In tert-butyl alcohol Heating; | A 40% B n/a |
1-Decanol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; | A 62% B 74%Spectr. C 26%Spectr. |
piperidine
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
A
C55H71N3O4
B
C60H80N4O4
Conditions | Yield |
---|---|
With copper dichloride at 60℃; for 24h; | A 60% B 28% |
1-Decanol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; | 60% |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
A
C50H60Br2N2O4
B
N,N’-di(1’-hexylheptyl)-1,7(6)-dibromo-3,4:9,10-perylenetetracarboxydiimide
Conditions | Yield |
---|---|
With bromine In dichloromethane at 20℃; for 96h; | A n/a B n/a C 57% |
With bromine In chloroform at 20℃; for 64h; | A n/a B n/a C 51% |
pyrrolidine
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
at 23℃; for 216h; | A 53% B 2% |
Octanethiol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; | A 53% B n/a C 20% |
decylthiol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; | A 25% B 53% C n/a |
pyrrolidine
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
C58H76N4O4
Conditions | Yield |
---|---|
With copper diacetate at 95℃; for 24h; Reagent/catalyst; Temperature; | 52% |
1-methyl-1-propanethiol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In tetrahydrofuran at 70℃; for 72h; Inert atmosphere; | A 50% B n/a C n/a |
2-methyl-propan-1-ol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; | A 46% B 73 %Spectr. C 27 %Spectr. |
2-phenylethanol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 72h; Inert atmosphere; | A 44% B 70 %Spectr. C 30 %Spectr. |
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; | A 23% B 72%Spectr. C 28%Spectr. |
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
ethylene glycol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 70℃; for 72h; Inert atmosphere; | 43% |
Octanethiol
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In tetrahydrofuran at 70℃; for 12h; Inert atmosphere; | 43% |
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