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High quality lower price Dioctylamine Basic information Product Name: Dioctylamine Synonyms: 1-Octanamine,N-octyl-;di-Normal-octylamine;N,N-Dioctylamine;N-n-Octyl-n-octylamine;n-octyl-
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inquiryProduct Name: Dioctylamine CAS: 1120-48-5 MF: C16H35N MW: 241.46 EINECS: 214-311-6 Mol File: 1120-48-5.mol Dioctylamine Structure Dioctylamine Chemical Properties Melting point 13-16 °C (lit.) Boiling point 297-298 &de
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N-(benzyloxycarbonyl)dioctylamine
n-dioctylamine
Conditions | Yield |
---|---|
With N1,N1,N12,N12-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine In N,N-dimethyl-formamide for 72h; Inert atmosphere; Glovebox; UV-irradiation; | 99% |
With lithium triethylborohydride In tetrahydrofuran at 0 - 20℃; for 1h; | 72% |
With naphthalen-1-yl-lithium In tetrahydrofuran at 0℃; for 5h; | 71 % Chromat. |
n-dioctylamine
Conditions | Yield |
---|---|
With naphthalene; lithium In tetrahydrofuran; methanol at 20℃; for 3h; | 97% |
Conditions | Yield |
---|---|
With [{CyPN(H)P}Co(CH2SiMe3)]-BArF4 In toluene at 120℃; for 24h; Schlenk technique; Sealed tube; | 96% |
With hydrogen In 1,3,5-trimethyl-benzene at 140℃; under 760.051 Torr; for 24h; Reagent/catalyst; | 93% |
With Co2Rh2/C In toluene at 180℃; under 760.051 Torr; for 6h; Autoclave; Inert atmosphere; | 88% |
n-dioctylamine
Conditions | Yield |
---|---|
With C24H32N8Ni(2+)*2I(1-); sodium amalgam In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere; | 95% |
With N1,N1,N12,N12-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine In N,N-dimethyl-formamide at 20℃; for 72h; UV-irradiation; | 59% |
With C84H70N6P4 In toluene at 110℃; for 24h; Temperature; Inert atmosphere; | 56% |
n-dioctylamine
Conditions | Yield |
---|---|
Stage #1: N,N-dioctyltritylamine With naphthalene; lithium In tetrahydrofuran at 0℃; for 3.5h; Stage #2: With water In tetrahydrofuran at 0 - 20℃; | 90% |
Tri-n-octylamine
anthranilic acid amide
A
Octanal
B
n-dioctylamine
C
2-heptyl-3,4-dihydroquinazoline-4(3H)-one
Conditions | Yield |
---|---|
With diphenyl-phosphinic acid; oxygen In 1,4-dioxane at 25℃; for 12h; | A n/a B n/a C 82% |
Conditions | Yield |
---|---|
With 5-methyl-1,3,4-thiadiazol-2-amine; potassium carbonate In ethanol; water at 25℃; for 1h; | 81% |
Multi-step reaction with 2 steps 1: 1.) sodium hydride / 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h View Scheme | |
Multi-step reaction with 3 steps 1: 1.) sodium hydride / 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h 2: 1.) NaH / 1.) DMF, 1 h, 2.) 70 deg C, 6 h 3: 77 percent / NaBH4 / ethanol / 15 h / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydride, trifluoroacetamide / dimethylformamide / 18 h / 80 °C View Scheme | |
Multi-step reaction with 3 steps 1: sodium hydride, trifluoroacetamide / dimethylformamide / 18 h / 80 °C 2: 1.) NaH / 1.) DMF, 1 h, 2.) 70 deg C, 6 h 3: 77 percent / NaBH4 / ethanol / 15 h / 60 °C View Scheme |
morpholine
n-Octylamine
A
N-1-octyl morpholine
B
n-dioctylamine
Conditions | Yield |
---|---|
With platinum-nickel nanoclusters on activated carbon; hydrogen at 180℃; under 760.051 Torr; Reagent/catalyst; Flow reactor; chemoselective reaction; | A 81% B 18% |
N-Octylideneoctylamine N-oxide
n-dioctylamine
Conditions | Yield |
---|---|
With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride In tetrahydrofuran at 20℃; for 6h; | 80% |
N,N-Dioctyl-trifluoracetamid
n-dioctylamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 60℃; for 15h; | 77% |
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran at 0 - 20℃; for 1h; | 76% |
Tri-n-octylamine
1,2-diamino-benzene
A
2-heptyl-1H-benzoimidazole
B
n-dioctylamine
Conditions | Yield |
---|---|
With but-2-enenitrile; 10% Pd/C In water; toluene at 170℃; under 15514.9 Torr; for 1.5h; Microwave irradiation; Inert atmosphere; | A n/a B 76% |
Octanoic acid
A
n-Octylamine
B
octane
C
n-dioctylamine
D
caprylic acid octylamide
E
n-octanamide
Conditions | Yield |
---|---|
Stage #1: Octanoic acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Reagent/catalyst; Cooling with ice; Green chemistry; | A 76% B 2% C 8% D 4% E 5% |
methyl octanate
A
n-Octylamine
B
octane
C
n-dioctylamine
D
caprylic acid octylamide
E
n-octanamide
Conditions | Yield |
---|---|
Stage #1: methyl octanate With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A 76% B 11% C 8% D 7% E 5% |
n-dioctylamine
Conditions | Yield |
---|---|
Stage #1: N,N-dioctylmethanesulfonamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.25h; Inert atmosphere; Stage #2: In tetrahydrofuran; hexane at 20℃; for 1h; Stage #3: With water In tetrahydrofuran; hexane | 72% |
With C84H70N6P4 In toluene at 110℃; for 48h; Inert atmosphere; | 6% |
With naphthalene; water; lithium 1.) THF, 20 deg C, 24 h; Yield given. Multistep reaction; |
n-dioctylamine
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran at 0 - 20℃; for 1h; | 66% |
Conditions | Yield |
---|---|
With 2-6-bis((1H-pyrazol-1-yl)methyl)pyridine; borane-ammonia complex; nickel(II) chloride hexahydrate In methanol at 25℃; for 0.5h; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 63% |
With hydrogen In neat (no solvent) at 110℃; under 5250.53 Torr; for 1h; Autoclave; | 30% |
With hydrogen at 90℃; under 18751.9 Torr; for 22h; Catalytic behavior; Autoclave; Sealed tube; | 22% |
With ethanol; nickel at 80℃; under 55163.1 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With ammonium carbonate In 5,5-dimethyl-1,3-cyclohexadiene for 24h; Inert atmosphere; Sealed tube; Reflux; | 61% |
pyrrolidine
n-Octylamine
A
Tri-n-octylamine
B
HRS-1-97
C
n-dioctylamine
Conditions | Yield |
---|---|
With hydrogen at 180℃; under 760.051 Torr; Flow reactor; chemoselective reaction; | A 16% B 61% C 22% |
Conditions | Yield |
---|---|
With ruthenium trichloride; triphenylphosphine In tetrahydrofuran at 185℃; for 8h; | A 58% B 21 % Chromat. |
With ruthenium trichloride; triphenylphosphine In tetrahydrofuran at 185℃; for 8h; Title compound not separated from byproducts; | A 47 % Chromat. B 51 % Chromat. |
In neat (no solvent) at 180℃; Reagent/catalyst; |
Conditions | Yield |
---|---|
With dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); ammonia In tert-Amyl alcohol at 170℃; for 23.5h; Inert atmosphere; Schlenk technique; Autoclave; | A 13.5% B 43% |
With 1-hydroxytetraphenylcyclopentadienyl(tetraphenyl-2,4-cyclopentadien-1-one)-μ-hydrotetracarbonyldiruthenium(II); ammonia; water In tert-Amyl alcohol; tert-butyl methyl ether at 170℃; for 40h; pressure tube; Inert atmosphere; | A 71 %Chromat. B 25 %Chromat. |
n-Octylamine
N-butylamine
A
tributyl-amine
B
N-n-butyl-N-n-octylamine
C
n-dioctylamine
Conditions | Yield |
---|---|
With platinum-nickel nanoclusters on activated carbon; hydrogen at 190℃; under 760.051 Torr; Flow reactor; chemoselective reaction; | A 14.5% B 28% C 40.3% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 80℃; for 12h; | 30.8% |
With potassium carbonate In dimethyl sulfoxide at 80℃; for 12h; |
Conditions | Yield |
---|---|
With ethanol; ammonia at 140℃; | |
Multi-step reaction with 2 steps 1: 1.) sodium hydride / 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h View Scheme | |
Multi-step reaction with 3 steps 1: 1.) sodium hydride / 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h 2: 1.) NaH / 1.) DMF, 1 h, 2.) 70 deg C, 6 h 3: 77 percent / NaBH4 / ethanol / 15 h / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydride, trifluoroacetamide / dimethylformamide / 18 h / 80 °C View Scheme | |
Multi-step reaction with 3 steps 1: sodium hydride, trifluoroacetamide / dimethylformamide / 18 h / 80 °C 2: 1.) NaH / 1.) DMF, 1 h, 2.) 70 deg C, 6 h 3: 77 percent / NaBH4 / ethanol / 15 h / 60 °C View Scheme |
Conditions | Yield |
---|---|
With ethanol; ammonia at 100℃; | |
With ammonia |
Conditions | Yield |
---|---|
With ammonia at 25℃; | |
With ammonia; sodium amide at -50℃; | |
With ammonia at 25℃; |
Conditions | Yield |
---|---|
With 1,4-dioxane; copper chromite at 275 - 290℃; under 147102 Torr; Hydrogenation; |
n-octyl methanesulfonate
2,2,2-trifluoro-N-octylacetamide
A
n-Octylamine
B
n-dioctylamine
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
With borane pyridine In acetic acid; Petroleum ether for 4h; Yield given. Yields of byproduct given; |
1,2,3-Benzotriazole
formaldehyd
n-dioctylamine
1-(benzotriazol-1'-yl)methyl-N,N-dioctylamine
Conditions | Yield |
---|---|
1.) methanol, water, 7 h, 2.) Et2O, reflux, overnight; | 100% |
Conditions | Yield |
---|---|
100% |
Conditions | Yield |
---|---|
With 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at 20℃; for 20h; Tsuji-Trost amination; | 100% |
With (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane; bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at 55℃; for 48h; | 99% |
With sodium chloride; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp In water at 55℃; for 20h; | 80% |
Conditions | Yield |
---|---|
bis(η3-allyl-μ-chloropalladium(II)); Tedicyp In water at 55℃; for 20h; | 100% |
bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane In water at 55℃; for 20h; | 100% |
Conditions | Yield |
---|---|
Stage #1: n-dioctylamine With n-butyllithium In tetrahydrofuran; hexane at -40℃; for 0.25h; Stage #2: N,N-diethyl-4-fluorobenzenesulfonamide In tetrahydrofuran; hexane at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | 100% |
n-dioctylamine
6-chloropyrazine-2-carboxylic acid chloride
6-chloro-N,N-dioctylpyrazine-2-carboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.0833333h; Solvent; Time; | 100% |
n-dioctylamine
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; for 0.5h; | 100% |
1,3,5-trichloro-2,4,6-triazine
n-dioctylamine
2-chloro-4,6-bis-(di-n-octylamino)-s-triazine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 25h; Cooling with ice; | 99% |
With triethylamine In dichloromethane at 20℃; for 24h; | 97% |
With triethylamine In dichloromethane at 25℃; for 24h; | 97% |
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 0 - 20℃; for 2h; | 99% |
1,4-dioxane-2,6-dione
n-dioctylamine
2-(2-(di-n-octylamino)-2-oxoethoxy)acetic acid
Conditions | Yield |
---|---|
In acetone at 20℃; Product distribution / selectivity; | 98.1% |
In dichloromethane at 20℃; | 94.3% |
In dichloromethane at 20℃; Cooling with ice; | 94.2% |
Conditions | Yield |
---|---|
In toluene for 5h; Reflux; | 98% |
In benzene at 79.9℃; for 1h; | 87.6% |
n-dioctylamine
N-n-octylidene-n-octylamine
Conditions | Yield |
---|---|
With copper(ll) bromide; lithium tert-butoxide In tetrahydrofuran for 0.0833333h; | 98% |
Conditions | Yield |
---|---|
With sodium carbonate for 15h; Reflux; | 98% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.666667h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane for 2h; | 98% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 97% |
In dichloromethane; triethylamine at 20℃; for 2h; | 96% |
With pyridine In dichloromethane at 20℃; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
bis(η3-allyl-μ-chloropalladium(II)); Tedicyp In water at 50℃; for 20h; | 97% |
With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane In water at 25℃; for 20h; | 97% |
With (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane; bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at 25℃; for 24h; | 95% |
With 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran at 50℃; for 20h; Tsuji-Trost amination; | 59% |
n-dioctylamine
3-tert-butyl-5-(chloromethyl)-2-hydroxybenzaldehyde
Conditions | Yield |
---|---|
In benzene for 6h; Heating; | 97% |
n-dioctylamine
N-octyl-α-heptylnitrone
Conditions | Yield |
---|---|
With Ti(OCH(CH3)2)N(CH2C6H3C(CH3)3O)3; dihydrogen peroxide In methanol; water at 60℃; for 3.5h; Inert atmosphere; chemoselective reaction; | 97% |
With Cumene hydroperoxide; C27H31NO4Ti; isopropyl alcohol In chloroform at 60℃; for 3h; Inert atmosphere; Molecular sieve; | 95% |
With dihydrogen peroxide In methanol at 60℃; for 8.5h; Reflux; | 76% |
With peroxomonosulfate; ethylenediaminetetraacetic acid; sodium hydrogencarbonate In tetrahydrofuran; water; acetonitrile at 5℃; for 2.33333h; Inert atmosphere; | 72% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 4.5h; | 97% |
With dmap; triethylamine In dichloromethane at 20℃; for 2.5h; | 5.09 g |
Conditions | Yield |
---|---|
In toluene for 12h; Inert atmosphere; Reflux; | 97% |
n-dioctylamine
chloroacetyl chloride
N,N-di-n-octylcarbamoyl methyl chloride
Conditions | Yield |
---|---|
96% | |
With potassium carbonate In dichloromethane for 2h; | 95% |
With triethylamine In dichloromethane at 20℃; for 3h; Cooling with ice; Inert atmosphere; | 87.5% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90 - 110℃; for 12h; | 96% |
Stage #1: n-dioctylamine; 11-bromo-undecanoic acid methyl ester In N,N-dimethyl-formamide for 0.25h; Stage #2: In N,N-dimethyl-formamide at 110℃; for 12h; | |
With potassium carbonate In N,N-dimethyl-formamide at 20 - 110℃; for 12h; |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine In tetrahydrofuran at 20℃; for 12h; | 95% |
n-dioctylamine
(2,4,9,11,16,18,23,25-octakis(dioctylaminosulfonyl)phthalocyaninato)cobalt(II)
Conditions | Yield |
---|---|
In acetone extn. of (2,4,9,11,16,18,23,25-oktakis(sulfonyl chloride)phthalocyaninato)Co(II) into acetone; addn. of dioctylamine (1.5 equiv.); keeping at 30°C for 1 h; filtration, evapn.; chromy. on silica gel; using CHCl3-MeOH (10:1) as eluent; elem. anal.; | 95% |
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