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inquirySulfamic acid [(1S,2S,4R)-4-[4-[[(1S)-2,3-dihydro-1H-inden-1-yl]amino]-7H-pyrrolo[2,3-d]pyrimidin-7-yl]-2-hydroxycyclopentyl]methyl ester hydrochloride CAS:1160295-21-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological co
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inquiry[(1s,2s,4r)-4-[4-[[(1s)-2,3-dihydro-1h-inden-1-yl]amino]pyrrolo[2,3-d]pyrimidin-7-yl]-2-hydroxycyclopentyl]methyl Sulfamate Hydrochloride Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical resear
Cas:1160295-21-5
Min.Order:0
Negotiable
Type:Trading Company
inquiry(1S,2S,4R)-4-{4-[(1S)-2,3-dihydro-1H-inden-1-ylamino]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-2-(hydroxymethyl)-cyclopentanol
(1,4-diazabicyclo[2.2.2]octan-1-ium-1-ylsulfonyl)(tert-butoxycarbonyl)amide
((1S,2S,4R)-4-(4-(((S)-2,3-dihydro-1H-inden-1-yl)amino)-7H-pyrrolo[2,3-d]pyrimidin-7-yl)-2-hydroxycyclopentyl)-methyl sulfamate hydrochloride
Conditions | Yield |
---|---|
Stage #1: (1S,2S,4R)-4-{4-[(1S)-2,3-dihydro-1H-inden-1-ylamino]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-2-(hydroxymethyl)-cyclopentanol; (1,4-diazabicyclo[2.2.2]octan-1-ium-1-ylsulfonyl)(tert-butoxycarbonyl)amide In acetonitrile at 55℃; for 8h; Stage #2: With hydrogenchloride In water; acetonitrile at 20℃; for 2h; | 42% |
((1S,2S,4R)-4-(4-(((S)-2,3-dihydro-1H-inden-1-yl)amino)-7H-pyrrolo[2,3-d]pyrimidin-7-yl)-2-hydroxycyclopentyl)-methyl sulfamate hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 50℃; Product distribution / selectivity; Reflux; |
((1S,2S,4R)-4-(4-(((S)-2,3-dihydro-1H-inden-1-yl)amino)-7H-pyrrolo[2,3-d]pyrimidin-7-yl)-2-hydroxycyclopentyl)-methyl sulfamate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: di-tert-butyl-diazodicarboxylate; phosphorous acid trimethyl ester / toluene / 3 h / 12 °C 2.1: N-ethyl-N,N-diisopropylamine / butan-1-ol / 24 h / 25 °C 3.1: hydrogenchloride; water / tetrahydrofuran / 4.5 h / 40 °C 4.1: acetonitrile / 8 h / 55 °C 4.2: 2 h / 20 °C View Scheme |
4-chloro-1H-pyrrolo[2,3-d]pyrimidine
((1S,2S,4R)-4-(4-(((S)-2,3-dihydro-1H-inden-1-yl)amino)-7H-pyrrolo[2,3-d]pyrimidin-7-yl)-2-hydroxycyclopentyl)-methyl sulfamate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: di-tert-butyl-diazodicarboxylate; phosphorous acid trimethyl ester / toluene / 3 h / 12 °C 2.1: N-ethyl-N,N-diisopropylamine / butan-1-ol / 24 h / 25 °C 3.1: hydrogenchloride; water / tetrahydrofuran / 4.5 h / 40 °C 4.1: acetonitrile / 8 h / 55 °C 4.2: 2 h / 20 °C View Scheme |
((1S,2S,4R)-4-(4-(((S)-2,3-dihydro-1H-inden-1-yl)amino)-7H-pyrrolo[2,3-d]pyrimidin-7-yl)-2-hydroxycyclopentyl)-methyl sulfamate hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: N-ethyl-N,N-diisopropylamine / butan-1-ol / 24 h / 25 °C 2.1: hydrogenchloride; water / tetrahydrofuran / 4.5 h / 40 °C 3.1: acetonitrile / 8 h / 55 °C 3.2: 2 h / 20 °C View Scheme |
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