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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiry4-Chloro-3',4'-dimethoxybenzophenoneAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Ag
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea
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inquiry4-Chloro-3',4'-dimethoxybenzophenone cas 116412-83-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryOur mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
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inquiryHow May We Serve You We can Supply HPLC\HMMR\MS report for you ,pls feel free to contact us! Capability on chemical synthesis ● Shanghai High-Tech Enterprises ● Strong R&D Team from USA, Japan, Korea ● 65000M2+ Factory, 300+ reac
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inquiry1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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inquiryPrice, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
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inquiry1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi
At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App
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inquiryJiangxi Shengwei Chemical Technology Co., Ltd.supplies scientific research products as below:1.High-purity organic chemical reagents;2.Analytical reagents; 3.Biochemical reagents;4.Chemical raw materials;5.Experimental instruments;6.Experimental cons
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inquiryDebyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen
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inquiry1,2-dimethoxybenzene
4-chloro-benzoyl chloride
B
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
A n/a B 93% |
1,2-dimethoxybenzene
para-chlorobenzoic acid
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 80 - 90℃; for 0.05h; Microwave irradiation; chemoselective reaction; | 89% |
3,4-dimethoxy-benzaldehyde
(4-chlorphenyl)magnesium bromide
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
Stage #1: 3,4-dimethoxy-benzaldehyde; (4-chlorphenyl)magnesium bromide In tetrahydrofuran Stage #2: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In dichloromethane | 86% |
1,2-dimethoxybenzene
4-chloro-benzoyl chloride
1,1,2,2-tetrachloroethane
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
With FeCl3; graphite | 84.3% |
With FeCl3; graphite | 84.3% |
graphite | 81.3% |
1,2-dimethoxybenzene
4-chlorotrichloromethylbenzene
1,1,2,2-tetrachloroethane
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
graphite In water | 79.5% |
1,2-dimethoxybenzene
4-chloro-benzoyl chloride
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
With Cl4Fe(1-)*C9H7N3O2*H(1+) In neat (no solvent) at 100℃; for 3h; Friedel-Crafts Acylation; Inert atmosphere; | 70% |
With aluminium trichloride In dichloromethane for 0.5h; Friedel-Crafts reaction; | 53% |
With aluminium trichloride In benzene at 55 - 60℃; for 2.5h; Friedel-Crafts reaction; |
para-chlorobenzoic acid
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Reflux 2: aluminum (III) chloride / dichloromethane / 2 h / 0 °C / Reflux View Scheme |
benzene-1,2-diol
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydroxide / water / 1.33 h / 10 - 15 °C / Inert atmosphere; Large scale 1.2: 4.7 h / 20 - 50 °C / Inert atmosphere; Large scale 2.1: iron(III) chloride / hexane / 2.8 h / 120 °C / Inert atmosphere; Large scale View Scheme |
1,2-dimethoxybenzene
para-chloroacetophenone
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
With iron(III) chloride In hexane at 120℃; for 2.8h; Temperature; Inert atmosphere; Large scale; |
Methyltriphenylphosphonium bromide
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
With sodium hydride | 89% |
4-acetylmorpholine
tert-Amyl alcohol
sodium tert-pentoxide
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
With carbon dioxide In 5,5-dimethyl-1,3-cyclohexadiene; di-isopropyl ether; paraffin oil | 82.2% |
ethylene glycol
4-chloro-3',4'-dimethoxy benzophenone
2-(4-chloro-phenyl)-2-(3,4-dimethoxy-phenyl)-[1,3]dioxolane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 40h; Heating; | 82% |
4-chloro-3',4'-dimethoxy benzophenone
(4-chlorophenyl)-(4,5-dimethoxy-2-nitrophenyl)methanone
Conditions | Yield |
---|---|
With nitric acid; acetic acid at 0 - 20℃; for 0.5h; | 77% |
With nitric acid; acetic acid |
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C 2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating 3: 78 percent / pyridine / 1 h / 20 °C 4: 86 percent / NaBH4 / ethanol / Heating 5: 76 percent / p-TsOH / CH2Cl2 / Heating 6: 81 percent / HCl / ethanol / Heating 7: 91 percent / KOH / methanol / 4 h / Heating View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
2-[4-chlorophenyl(hydroxy)methyl]-4,5-dimethoxy-1-(4-methylphenylsulfonamido)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C 2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating 3: 78 percent / pyridine / 1 h / 20 °C 4: 86 percent / NaBH4 / ethanol / Heating View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
2-(4-chlorobenzoyl)-4,5-dimethoxy-1-(4-methylphenylsufonamido)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C 2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating 3: 78 percent / pyridine / 1 h / 20 °C View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
4-methyl-N-{2-[(4-chlorophenyl)(5-methylfuran-2-yl)methyl]-4,5-dimethoxyphenyl}benzenesulfonamide
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C 2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating 3: 78 percent / pyridine / 1 h / 20 °C 4: 86 percent / NaBH4 / ethanol / Heating 5: 76 percent / p-TsOH / CH2Cl2 / Heating View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
4-[3-(4-chlorophenyl)-5,6-dimethoxy-1-(4-methylphenylsulfonyl)-1H-2-indolyl]-2-butanone
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C 2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating 3: 78 percent / pyridine / 1 h / 20 °C 4: 86 percent / NaBH4 / ethanol / Heating 5: 76 percent / p-TsOH / CH2Cl2 / Heating 6: 81 percent / HCl / ethanol / Heating View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
(2-amino-4,5-dimethoxyphenyl)-(4-chlorophenyl)methanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C 2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating 2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C 2.2: tetrahydrofuran; hexane / 3 h 3.1: 1.35 g / aq. hydrochloric acid / 4 h / Heating View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating 2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C 2.2: sulfur dioxide / tetrahydrofuran; hexane / 12 h / 20 °C 3.1: sulfuryl chloride / hexane / 0.5 h / 0 °C View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
5-chloro-2-[2-(3,4-dimethoxy-phenyl)-[1,3]dioxolan-2-yl]-benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating 2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C 2.2: tetrahydrofuran; hexane / 3 h View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating 2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C 2.2: sulfur dioxide / tetrahydrofuran; hexane / 12 h / 20 °C View Scheme |
4-acetylmorpholine
sodium tert-pentoxide
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
In di-isopropyl ether; toluene |
Conditions | Yield |
---|---|
In toluene; paraffin oil |
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran |
4-acetylmorpholine
p-Tolylaceton
4-chloro-3',4'-dimethoxy benzophenone
Conditions | Yield |
---|---|
With potassium hydroxide In water; toluene |
4-chloro-3',4'-dimethoxy benzophenone
4-chloro-3',4'-dimethoxydiphenylmethane
Conditions | Yield |
---|---|
With aluminum (III) chloride; lithium aluminium tetrahydride for 2h; Reflux; |
4-chloro-3',4'-dimethoxy benzophenone
4-chloro-3',4'-dihydroxydiphenylmethanone
Conditions | Yield |
---|---|
With boron tribromide In dichloromethane at -78 - 20℃; for 4h; |
4-chloro-3',4'-dimethoxy benzophenone
(3,4-dimethoxyphenyl)(4-chlorophenyl)methanone oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium hydroxide In ethanol for 6h; Reflux; |
4-chloro-3',4'-dimethoxy benzophenone
isopropyl((2S)-1-(((3,4-dimethoxylphenyl)(4-chlorophenyl)methyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydroxide; hydroxylamine hydrochloride / ethanol / 6 h / Reflux 2.1: ammonium hydroxide; zinc; ammonium acetate / ethanol / 1 h / Reflux 3.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 1 h / 0 °C 3.2: 2 h / 20 °C View Scheme |
4-chloro-3',4'-dimethoxy benzophenone
(3,4-dimethoxyphenyl)(4-chlorophenyl)methylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydroxide; hydroxylamine hydrochloride / ethanol / 6 h / Reflux 2: ammonium hydroxide; zinc; ammonium acetate / ethanol / 1 h / Reflux View Scheme |
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