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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

4-Chloro-3',4'-dimethoxybenzophenone Manufacturer/High quality/Best price/In stock

Cas:116412-83-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 4-chloro-3',4'-dimethoxybenzophenone

Cas:116412-83-0

Min.Order:1

Negotiable

Type:Other

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

TIANFU-CHEM_4-Chloro-3,4'-DimethoxyBenzophenone 116412-83-0

Cas:116412-83-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

4-Chloro-3,4'-DimethoxyBenzophenone CAS 116412-83-0

Cas:116412-83-0

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Methanone,(4-chlorophenyl)(3,4-dimethoxyphenyl)-

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

4-chloro-3',4'-dimethoxybenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

(4-Chlorophenyl)(3,4-diMethoxyphenyl)Methanone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

4-Chloro 3,4'-dimethoxy benzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

1-(tert-Butoxycarbonyl)-3-(3,4-dichlorobenzyl)-3-piperidinecarboxylic acid

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

4-Chloro-3,4'-DimethoxyBenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

4-Chloro-3',4'-dimethoxybenzophenoneAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Ag

4-Chloro-3',4'-dimethoxybenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea

4-Chloro-3,4'-DimethoxyBenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

4-Chloro-3',4'-dimethoxybenzophenone cas 116412-83-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

4-Chloro-3',4'-dimethoxybenzophenone cas 116412-83-0

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Other

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

4-Chloro-3,4'-DimethoxyBenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Bide Pharmatech Ltd

Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical

(4-Chlorophenyl)(3,4-dimethoxyphenyl)methanone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Other

inquiry

Yurui(Shanghai)Chemical Co.,Ltd

How May We Serve You We can Supply HPLC\HMMR\MS report for you ,pls feel free to contact us! Capability on chemical synthesis ● Shanghai High-Tech Enterprises ● Strong R&D Team from USA, Japan, Korea ● 65000M2+ Factory, 300+ reac

4-Chloro-3',4'-dimethoxybenzophenone

Cas:116412-83-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

(4-chloro-3-methoxyphenyl)-(4-methoxyphenyl)methanone

Cas:116412-83-0

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

4-Chloro-3,4'-DimethoxyBenzophenone

Cas:116412-83-0

Min.Order:1 Metric Ton

Negotiable

Type:Trading Company

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

4-Chloro-3',4'-dimethoxybenzophenone CAS NO.116412-83-0

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

4-Chloro-3,4'-DimethoxyBenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Other

inquiry

Capot Chemical Co., Ltd.

At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

4&#39-Chloro-3,4-dimethoxybenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GZ HONESTCHEM CO., LTD

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

(4-Chlorophenyl)(3,4-diMethoxyphenyl)Methanone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Jiangxi shengwei chemical technology co. LTD

Jiangxi Shengwei Chemical Technology Co., Ltd.supplies scientific research products as below:1.High-purity organic chemical reagents;2.Analytical reagents; 3.Biochemical reagents;4.Chemical raw materials;5.Experimental instruments;6.Experimental cons

4-Chloro-3',4'-dimethoxybenzophenone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

(4-Chlorophenyl)(3,4-dimethoxyphenyl)methanone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai chamflyer chemicals Co., Ltd

High quality Application:Pharmaceutial

(4-Chlorophenyl)(3,4-diMethoxyphenyl)Methanone

Cas:116412-83-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

1,2-dimethoxybenzene
91-16-7

1,2-dimethoxybenzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

A

FeCl3

FeCl3

B

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
A n/a
B 93%
1,2-dimethoxybenzene
91-16-7

1,2-dimethoxybenzene

para-chlorobenzoic acid
74-11-3

para-chlorobenzoic acid

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
With boron trifluoride diethyl etherate at 80 - 90℃; for 0.05h; Microwave irradiation; chemoselective reaction;89%
3,4-dimethoxy-benzaldehyde
120-14-9

3,4-dimethoxy-benzaldehyde

(4-chlorphenyl)magnesium bromide
873-77-8

(4-chlorphenyl)magnesium bromide

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
Stage #1: 3,4-dimethoxy-benzaldehyde; (4-chlorphenyl)magnesium bromide In tetrahydrofuran
Stage #2: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In dichloromethane
86%
1,2-dimethoxybenzene
91-16-7

1,2-dimethoxybenzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
With FeCl3; graphite84.3%
With FeCl3; graphite84.3%
graphite81.3%
1,2-dimethoxybenzene
91-16-7

1,2-dimethoxybenzene

4-chlorotrichloromethylbenzene
5216-25-1

4-chlorotrichloromethylbenzene

1,1,2,2-tetrachloroethane
79-34-5

1,1,2,2-tetrachloroethane

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
graphite In water79.5%
1,2-dimethoxybenzene
91-16-7

1,2-dimethoxybenzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
With Cl4Fe(1-)*C9H7N3O2*H(1+) In neat (no solvent) at 100℃; for 3h; Friedel-Crafts Acylation; Inert atmosphere;70%
With aluminium trichloride In dichloromethane for 0.5h; Friedel-Crafts reaction;53%
With aluminium trichloride In benzene at 55 - 60℃; for 2.5h; Friedel-Crafts reaction;
para-chlorobenzoic acid
74-11-3

para-chlorobenzoic acid

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Reflux
2: aluminum (III) chloride / dichloromethane / 2 h / 0 °C / Reflux
View Scheme
benzene-1,2-diol
120-80-9

benzene-1,2-diol

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydroxide / water / 1.33 h / 10 - 15 °C / Inert atmosphere; Large scale
1.2: 4.7 h / 20 - 50 °C / Inert atmosphere; Large scale
2.1: iron(III) chloride / hexane / 2.8 h / 120 °C / Inert atmosphere; Large scale
View Scheme
1,2-dimethoxybenzene
91-16-7

1,2-dimethoxybenzene

para-chloroacetophenone
99-91-2

para-chloroacetophenone

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

Conditions
ConditionsYield
With iron(III) chloride In hexane at 120℃; for 2.8h; Temperature; Inert atmosphere; Large scale;
Methyltriphenylphosphonium bromide
1779-49-3

Methyltriphenylphosphonium bromide

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

C16H15ClO2

C16H15ClO2

Conditions
ConditionsYield
With sodium hydride89%
4-acetylmorpholine
1696-20-4

4-acetylmorpholine

tert-Amyl alcohol
75-85-4

tert-Amyl alcohol

sodium tert-pentoxide
14593-46-5

sodium tert-pentoxide

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

dimethomorph

dimethomorph

Conditions
ConditionsYield
With carbon dioxide In 5,5-dimethyl-1,3-cyclohexadiene; di-isopropyl ether; paraffin oil82.2%
ethylene glycol
107-21-1

ethylene glycol

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

2-(4-chloro-phenyl)-2-(3,4-dimethoxy-phenyl)-[1,3]dioxolane
812685-05-5

2-(4-chloro-phenyl)-2-(3,4-dimethoxy-phenyl)-[1,3]dioxolane

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene for 40h; Heating;82%
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

(4-chlorophenyl)-(4,5-dimethoxy-2-nitrophenyl)methanone
681469-99-8

(4-chlorophenyl)-(4,5-dimethoxy-2-nitrophenyl)methanone

Conditions
ConditionsYield
With nitric acid; acetic acid at 0 - 20℃; for 0.5h;77%
With nitric acid; acetic acid
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

4-[3-(4-chlorophenyl)-5,6-dimethoxy-1H-2-indolyl]-2-butanone

4-[3-(4-chlorophenyl)-5,6-dimethoxy-1H-2-indolyl]-2-butanone

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C
2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating
3: 78 percent / pyridine / 1 h / 20 °C
4: 86 percent / NaBH4 / ethanol / Heating
5: 76 percent / p-TsOH / CH2Cl2 / Heating
6: 81 percent / HCl / ethanol / Heating
7: 91 percent / KOH / methanol / 4 h / Heating
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

2-[4-chlorophenyl(hydroxy)methyl]-4,5-dimethoxy-1-(4-methylphenylsulfonamido)benzene
924635-48-3

2-[4-chlorophenyl(hydroxy)methyl]-4,5-dimethoxy-1-(4-methylphenylsulfonamido)benzene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C
2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating
3: 78 percent / pyridine / 1 h / 20 °C
4: 86 percent / NaBH4 / ethanol / Heating
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

2-(4-chlorobenzoyl)-4,5-dimethoxy-1-(4-methylphenylsufonamido)benzene
886493-87-4

2-(4-chlorobenzoyl)-4,5-dimethoxy-1-(4-methylphenylsufonamido)benzene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C
2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating
3: 78 percent / pyridine / 1 h / 20 °C
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

4-methyl-N-{2-[(4-chlorophenyl)(5-methylfuran-2-yl)methyl]-4,5-dimethoxyphenyl}benzenesulfonamide
924635-54-1

4-methyl-N-{2-[(4-chlorophenyl)(5-methylfuran-2-yl)methyl]-4,5-dimethoxyphenyl}benzenesulfonamide

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C
2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating
3: 78 percent / pyridine / 1 h / 20 °C
4: 86 percent / NaBH4 / ethanol / Heating
5: 76 percent / p-TsOH / CH2Cl2 / Heating
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

4-[3-(4-chlorophenyl)-5,6-dimethoxy-1-(4-methylphenylsulfonyl)-1H-2-indolyl]-2-butanone
920457-61-0

4-[3-(4-chlorophenyl)-5,6-dimethoxy-1-(4-methylphenylsulfonyl)-1H-2-indolyl]-2-butanone

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C
2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating
3: 78 percent / pyridine / 1 h / 20 °C
4: 86 percent / NaBH4 / ethanol / Heating
5: 76 percent / p-TsOH / CH2Cl2 / Heating
6: 81 percent / HCl / ethanol / Heating
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

(2-amino-4,5-dimethoxyphenyl)-(4-chlorophenyl)methanone
886494-44-6

(2-amino-4,5-dimethoxyphenyl)-(4-chlorophenyl)methanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / HNO3; AcOH / 0.5 h / 0 - 20 °C
2: 67 percent / Fe; AcOH / H2O; ethyl acetate / 6 h / Heating
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

3-chloro-6-(3,4-dimethoxybenzoyl)benzoic acid

3-chloro-6-(3,4-dimethoxybenzoyl)benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating
2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C
2.2: tetrahydrofuran; hexane / 3 h
3.1: 1.35 g / aq. hydrochloric acid / 4 h / Heating
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

5-chloro-2-[2-(3,4-dimethoxy-phenyl)-[1,3]dioxolan-2-yl]-benzenesulfonyl chloride

5-chloro-2-[2-(3,4-dimethoxy-phenyl)-[1,3]dioxolan-2-yl]-benzenesulfonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating
2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C
2.2: sulfur dioxide / tetrahydrofuran; hexane / 12 h / 20 °C
3.1: sulfuryl chloride / hexane / 0.5 h / 0 °C
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

5-chloro-2-[2-(3,4-dimethoxy-phenyl)-[1,3]dioxolan-2-yl]-benzoic acid
1027937-58-1

5-chloro-2-[2-(3,4-dimethoxy-phenyl)-[1,3]dioxolan-2-yl]-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating
2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C
2.2: tetrahydrofuran; hexane / 3 h
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

lithium; 5-chloro-2-[2-(3,4-dimethoxy-phenyl)-[1,3]dioxolan-2-yl]-benzenesulfinate

lithium; 5-chloro-2-[2-(3,4-dimethoxy-phenyl)-[1,3]dioxolan-2-yl]-benzenesulfinate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 82 percent / p-toluenesulfonic acid / toluene / 40 h / Heating
2.1: butyllithium / hexane; tetrahydrofuran / 2 h / -20 °C
2.2: sulfur dioxide / tetrahydrofuran; hexane / 12 h / 20 °C
View Scheme
4-acetylmorpholine
1696-20-4

4-acetylmorpholine

sodium tert-pentoxide
14593-46-5

sodium tert-pentoxide

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

dimethomorph

dimethomorph

Conditions
ConditionsYield
In di-isopropyl ether; toluene
tert-butyl alcohol
75-65-0

tert-butyl alcohol

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

dimethomorph

dimethomorph

Conditions
ConditionsYield
In toluene; paraffin oil
4-acetylmorpholine
1696-20-4

4-acetylmorpholine

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

dimethomorph

dimethomorph

Conditions
ConditionsYield
With potassium hydroxide In tetrahydrofuran
4-acetylmorpholine
1696-20-4

4-acetylmorpholine

p-Tolylaceton
2096-86-8

p-Tolylaceton

4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

A

3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-3-hydroxy-1-morpholinopropan-1-one

3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-3-hydroxy-1-morpholinopropan-1-one

B

dimethomorph

dimethomorph

Conditions
ConditionsYield
With potassium hydroxide In water; toluene
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

4-chloro-3',4'-dimethoxydiphenylmethane
1239703-27-5

4-chloro-3',4'-dimethoxydiphenylmethane

Conditions
ConditionsYield
With aluminum (III) chloride; lithium aluminium tetrahydride for 2h; Reflux;
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

4-chloro-3',4'-dihydroxydiphenylmethanone
134612-84-3

4-chloro-3',4'-dihydroxydiphenylmethanone

Conditions
ConditionsYield
With boron tribromide In dichloromethane at -78 - 20℃; for 4h;
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

(3,4-dimethoxyphenyl)(4-chlorophenyl)methanone oxime
1385825-44-4

(3,4-dimethoxyphenyl)(4-chlorophenyl)methanone oxime

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium hydroxide In ethanol for 6h; Reflux;
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

isopropyl((2S)-1-(((3,4-dimethoxylphenyl)(4-chlorophenyl)methyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate
1496524-38-9

isopropyl((2S)-1-(((3,4-dimethoxylphenyl)(4-chlorophenyl)methyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydroxide; hydroxylamine hydrochloride / ethanol / 6 h / Reflux
2.1: ammonium hydroxide; zinc; ammonium acetate / ethanol / 1 h / Reflux
3.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 1 h / 0 °C
3.2: 2 h / 20 °C
View Scheme
4-chloro-3',4'-dimethoxy benzophenone
116412-83-0

4-chloro-3',4'-dimethoxy benzophenone

(3,4-dimethoxyphenyl)(4-chlorophenyl)methylamine
1016697-21-4

(3,4-dimethoxyphenyl)(4-chlorophenyl)methylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydroxide; hydroxylamine hydrochloride / ethanol / 6 h / Reflux
2: ammonium hydroxide; zinc; ammonium acetate / ethanol / 1 h / Reflux
View Scheme

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