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inquiry-[2-1-NAPHTHOXY)ETHYL]BENZYLAMINE / 3-(1-NAPHTHOXY)-1-PHENYL PROPYLAMINE CAS:119356-76-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical int
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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inquiryN,N-Dimethyl-alpha-[2-(1-naphthalenyloxy)ethyl]benzenemethanamine cas 119356-76-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
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inquiryN,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; acetic acid In methanol | 98.2% |
α-naphthol
3-chloropropiophenone
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide at 60 - 65℃; for 5h; Reagent/catalyst; Temperature; | 97.7% |
C21H22ClNO
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; acetic acid In methanol | 94.2% |
3-(naphthalen-1-yloxy)-1-phenylpropan-1-one
dimethyl amine
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With formic acid at 170 - 180℃; for 18h; Time; | 88.5% |
C20H20O4S
dimethyl amine
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran at 0 - 35℃; for 40h; |
dimethyl amine
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Stage #1: 3-(naphthalen-1-yloxy)-1-phenyl-propan-1-ol With dmap; methanesulfonyl chloride; triethylamine In tetrahydrofuran at -5 - 0℃; Stage #2: dimethyl amine In tetrahydrofuran at 0 - 20℃; for 40h; Stage #3: With sodium hydroxide In tetrahydrofuran; water for 9 - 10h; |
3-Amino-3-phenylpropionic acid
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium tetrahydroborate; iodine / tetrahydrofuran / 18 h / 66 °C 2.1: 8 h / 95 °C 3.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 50 °C / Inert atmosphere 3.2: 6 h / 100 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium tetrahydroborate / tetrahydrofuran / 0.17 h / Cooling with ice 1.2: 7.5 h / 10 - 65 °C 2.1: water / 10 h / 90 °C / Cooling with ice 3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 60 °C / Cooling with ice 3.2: 9 h / 100 °C View Scheme |
1-Fluoronaphthalene
3-(dimethylamino)-3-phenylpropan-1-ol
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Stage #1: 3-(dimethylamino)-3-phenylpropan-1-ol With sodium hydride In N,N-dimethyl-formamide at 50℃; for 1.5h; Inert atmosphere; Stage #2: 1-Fluoronaphthalene In N,N-dimethyl-formamide at 100℃; for 6h; | 38.6 g |
Stage #1: 3-(dimethylamino)-3-phenylpropan-1-ol With sodium hydride In N,N-dimethyl-formamide at 60℃; for 1h; Cooling with ice; Stage #2: 1-Fluoronaphthalene In N,N-dimethyl-formamide at 100℃; for 9h; |
benzaldehyde
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: ammonium acetate / ethanol / 8 h / 80 °C 2.1: sodium tetrahydroborate; iodine / tetrahydrofuran / 18 h / 66 °C 3.1: 8 h / 95 °C 4.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 50 °C / Inert atmosphere 4.2: 6 h / 100 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / ethanol / 6 h / 78 °C 2.1: sodium tetrahydroborate / tetrahydrofuran / 0.17 h / Cooling with ice 2.2: 7.5 h / 10 - 65 °C 3.1: water / 10 h / 90 °C / Cooling with ice 4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 60 °C / Cooling with ice 4.2: 9 h / 100 °C View Scheme |
3-amino-3-phenyl-1-propanol
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 8 h / 95 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 50 °C / Inert atmosphere 2.2: 6 h / 100 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: water / 10 h / 90 °C / Cooling with ice 2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 60 °C / Cooling with ice 2.2: 9 h / 100 °C View Scheme |
formaldehyd
1-phenyl-3-(naphthyl-1-oxy)propylamine
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With formic acid In water at 90℃; for 6h; |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 5 h / Irradiation; Reflux 2: acetone / 5 h / 50 °C / Cooling with ice 3: acetic acid; palladium 10% on activated carbon / methanol View Scheme | |
Multi-step reaction with 3 steps 1: dibenzoyl peroxide; N-chloro-succinimide / tetrachloromethane / 5 h / Reflux; Irradiation 2: acetone / 6 h / 50 °C / Cooling with ice 3: acetic acid; palladium 10% on activated carbon / methanol View Scheme |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetone / 5 h / 50 °C / Cooling with ice 2: acetic acid; palladium 10% on activated carbon / methanol View Scheme |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetone / 6 h / 50 °C / Cooling with ice 2: acetic acid; palladium 10% on activated carbon / methanol View Scheme |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With hydrogenchloride In ethyl acetate for 2h; pH=2; Cooling with ice; | 85.8% |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol pH=2 - 3; pH-value; | 84.8% |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With hydrogenchloride; (1S)-10-camphorsulfonic acid In ethanol; water at 20℃; for 15h; Temperature; Solvent; Reagent/catalyst; | 76% |
Multi-step reaction with 3 steps 1: ethanol; water 2: sodium hydroxide / pH >= 13 3: hydrogenchloride / acetone View Scheme |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With L-Tartaric acid In ethanol; water at 20℃; Cooling with ice; | 37% |
Multi-step reaction with 2 steps 1: ethanol; water 2: sodium hydroxide / pH >= 13 View Scheme |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
(2S,3S)-di-4-toluoyltartaric acid
Conditions | Yield |
---|---|
In dichloromethane at 25 - 35℃; for 0.5h; |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
ammonium bromocamphorsulfonate
Conditions | Yield |
---|---|
In methanol; ethyl acetate |
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
D-tartaric acid
S-(+)-N,N-dimethyl-3-(naphthalen-1-yloxy)-1-phenylpropan-1-amine tartrate
Conditions | Yield |
---|---|
In ethanol; water | 3.5 g |
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