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inquiryProduct name: Ethanone, 2-chloro-1-(1-chlorocyclopropyl)- CAS NO.: 120983-72-4 Molecular formula: C5H6Cl2O Molecular weight: 153.01 Structural formu
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inquiryEthanone, 2-chloro-1-(1-chlorocyclopropyl)- (9CI) CAS:120983-72-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializi
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryProduct name: 2-Chloro-1-(1-Chlorocyclopropyl)Ethanone CAS No.:120983-72-4 Molecule Formula:C5H6Cl2O Molecule Weight:153.00 Purity: 90.0% Package: 200kg/drum Description:Colorless to yellow liquid Manufacture Standards:Enterprise Stan
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inquiryProduct Name: Ethanone, 2-chloro-1-(1-chlorocyclopropyl)- (9CI) Synonyms: Ethanone, 2-chloro-1-(1-chlorocyclopropyl)- (9CI);Ethanone, 2-chloro-1-(1-chlorocyclopropyl)-;2-CHLORO-1-(1-CHLOROCYCLOPROPYL)ETHAN-1-ONE;2-chloro-1-(1-chlorocyclopropyl)
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inquiryC5H6Cl2O Ethanone, 2-chloro-1-(1-chlorocyclopropyl)- (9CI) 120983-72-4 Application:C5H6Cl2O Ethanone, 2-chloro-1-(1-chlorocyclopropyl)- (9CI) 120983-72-4
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inquiry1-chlorocyclopropyl methyl ketone
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
With chlorine at 10 - 25℃; under 760.051 Torr; for 2h; Temperature; Reagent/catalyst; | 98.5% |
With sodium nitrate; trichloroisocyanuric acid; antimonypentachloride at 60℃; for 4h; Reagent/catalyst; Solvent; Temperature; | 96.8% |
With iron(III) chloride; tetrabutylammomium bromide; chlorine In dichloromethane at 15 - 25℃; for 5h; Reagent/catalyst; Temperature; | 93.1% |
Cyclopropyl methyl ketone
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
With N-chloro-succinimide In dichloromethane at 0 - 20℃; | 92% |
With phosgene In methanol; chloroform at 5 - 15℃; for 3h; Temperature; Reagent/catalyst; Solvent; Reflux; | 71.95% |
5-chloro-2-pentanone
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Stage #1: 5-chloro-2-pentanone With thionyl chloride In dichloromethane at 0 - 40℃; for 4h; Stage #2: With tetrabutylammomium bromide; sodium hydroxide In dichloromethane at 40℃; for 3h; Solvent; Temperature; Reagent/catalyst; | 60% |
3, 5-dichloro-2-pentanone
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium hydroxide In water at 20 - 90℃; for 0.583333h; Reagent/catalyst; Heating; |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water at 0℃; for 0.166667h; Reagent/catalyst; Flow reactor; |
1-chlorocyclopropyl-2-chloro-ethan-1-one
1-chloro-2-(chloromethyl)benzene
Conditions | Yield |
---|---|
Stage #1: 1-chloro-2-(chloromethyl)benzene With iodine; magnesium In 2-methyltetrahydrofuran; tert-butyl methyl ether at 50℃; for 0.5h; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one In tert-butyl methyl ether at 0℃; for 0.00833333h; | 95.3% |
Stage #1: 1-chloro-2-(chloromethyl)benzene With iodine; magnesium In 2-methyltetrahydrofuran; tert-butyl methyl ether at 25 - 50℃; for 4.5h; Inert atmosphere; Large scale; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one In 2-methyltetrahydrofuran; tert-butyl methyl ether at 0 - 5℃; for 1h; Solvent; Large scale; | 94% |
Stage #1: 1-chloro-2-(chloromethyl)benzene With iodine; magnesium In tetrahydrofuran for 1h; Cooling with ice; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one In tetrahydrofuran for 1h; Cooling with ice; | 89% |
Stage #1: 1-chloro-2-(chloromethyl)benzene With iodine; magnesium In 1,2-dimethoxyethane Grignard Reaction; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one In 1,2-dimethoxyethane; toluene at 20 - 25℃; for 2h; Solvent; Grignard Reaction; | 81% |
1-chlorocyclopropyl-2-chloro-ethan-1-one
allylmagnesium bromide
1-chloro-2-(1-chlorocyclopropyl)-4-pentene-2-ol
Conditions | Yield |
---|---|
With ammonium chloride In diethyl ether at -50℃; for 1.33333h; Inert atmosphere; | 77% |
Stage #1: 1-chlorocyclopropyl-2-chloro-ethan-1-one; allylmagnesium bromide In diethyl ether at -50℃; for 2.33333h; Inert atmosphere; Cooling with ice; Stage #2: With ammonium chloride In diethyl ether; water Cooling with ice; |
3-chloro-4-methylpyridine
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Stage #1: 3-chloro-4-methylpyridine With lithium diisopropyl amide In tetrahydrofuran at -70 - -30℃; for 0.0833333h; Inert atmosphere; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one In tetrahydrofuran at -70 - 20℃; for 1h; Inert atmosphere; | 73% |
Stage #1: 3-chloro-4-methylpyridine With lithium diisopropyl amide In tetrahydrofuran at -70℃; for 0.0833333h; Inert atmosphere; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one In tetrahydrofuran at -70 - -30℃; for 1h; Inert atmosphere; | 73% |
1-chlorocyclopropyl-2-chloro-ethan-1-one
vinyl magnesium bromide
Conditions | Yield |
---|---|
Stage #1: 1-chlorocyclopropyl-2-chloro-ethan-1-one; vinyl magnesium bromide In tetrahydrofuran at -20 - 0℃; Inert atmosphere; Stage #2: With ammonium chloride In tetrahydrofuran; water Cooling with ice; | 67% |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
With potassium iodide In methanol at 70℃; for 46h; | 46% |
With potassium iodide In methanol at 70℃; for 46h; |
1H-tetrazole
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Stage #1: 1H-tetrazole With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 21℃; for 0.0833333h; Inert atmosphere; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one In acetonitrile at 21 - 40℃; for 2h; | A 10.4% B 34.7% |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In ethanol at 70℃; for 1h; | 30% |
1-chlorocyclopropyl-2-chloro-ethan-1-one
1-bromovinylbenzene
Conditions | Yield |
---|---|
With magnesium In diethyl ether |
1-chlorocyclopropyl-2-chloro-ethan-1-one
4-chloro-phenol
Conditions | Yield |
---|---|
With potassium carbonate In water; toluene |
1-chlorocyclopropyl-2-chloro-ethan-1-one
4-chloro-phenol
Conditions | Yield |
---|---|
With potassium carbonate In ethyl acetate; acetonitrile |
1-chlorocyclopropyl-2-chloro-ethan-1-one
4-Fluorobenzyl bromide
Conditions | Yield |
---|---|
With magnesium; acetic acid In diethyl ether; water |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tetrahydrofuran / -20 - 0 °C / Inert atmosphere 1.2: Cooling with ice 2.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water / 32 h / 60 - 80 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tetrahydrofuran / -20 - 0 °C / Inert atmosphere 1.2: Cooling with ice 2.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water / 32 h / 60 - 80 °C 3.1: potassium carbonate; potassium tert-butylate / 1-methyl-pyrrolidin-2-one / 5 h / 80 °C / Inert atmosphere View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: diethyl ether / 2.33 h / -50 °C / Inert atmosphere; Cooling with ice 1.2: Cooling with ice 2.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water / 7 h / 20 - 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: zinc; ammonium chloride / water; tetrahydrofuran / 3.17 h / 35 °C 2: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water / 7 h / 20 - 80 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: diethyl ether / 2.33 h / -50 °C / Inert atmosphere; Cooling with ice 1.2: Cooling with ice 2.1: sodium hydroxide; water / tetrahydrofuran / 4 h / 20 °C 3.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 15 h / 60 °C View Scheme | |
Multi-step reaction with 3 steps 1: zinc; ammonium chloride / water; tetrahydrofuran / 3.17 h / 35 °C 2: sodium hydroxide; water / tetrahydrofuran / 4 h / 20 °C 3: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 15 h / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: ammonium chloride / diethyl ether / 1.33 h / -50 °C / Inert atmosphere 2: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water / 7 h / 20 - 80 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: diethyl ether / 2.33 h / -50 °C / Inert atmosphere; Cooling with ice 1.2: Cooling with ice 2.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water / 7 h / 20 - 80 °C 3.1: potassium carbonate; sodium t-butanolate / N,N-dimethyl-formamide / 2 h / 90 °C View Scheme | |
Multi-step reaction with 3 steps 1: zinc; ammonium chloride / water; tetrahydrofuran / 3.17 h / 35 °C 2: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water / 7 h / 20 - 80 °C 3: potassium carbonate; sodium t-butanolate / N,N-dimethyl-formamide / 2 h / 90 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: diethyl ether / 2.33 h / -50 °C / Inert atmosphere; Cooling with ice 1.2: Cooling with ice 2.1: sodium hydroxide; water / tetrahydrofuran / 4 h / 20 °C 3.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 15 h / 60 °C 4.1: potassium carbonate; sodium t-butanolate / N,N-dimethyl-formamide / 2 h / 90 °C View Scheme | |
Multi-step reaction with 4 steps 1: zinc; ammonium chloride / water; tetrahydrofuran / 3.17 h / 35 °C 2: sodium hydroxide; water / tetrahydrofuran / 4 h / 20 °C 3: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 15 h / 60 °C 4: potassium carbonate; sodium t-butanolate / N,N-dimethyl-formamide / 2 h / 90 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
2-(1-chlorocyclopropyl)-2-(2-propenyl)oxirane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: diethyl ether / 2.33 h / -50 °C / Inert atmosphere; Cooling with ice 1.2: Cooling with ice 2.1: sodium hydroxide; water / tetrahydrofuran / 4 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: zinc; ammonium chloride / water; tetrahydrofuran / 3.17 h / 35 °C 2: sodium hydroxide; water / tetrahydrofuran / 4 h / 20 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
allyl bromide
1-chloro-2-(1-chlorocyclopropyl)-4-pentene-2-ol
Conditions | Yield |
---|---|
With ammonium chloride; zinc In tetrahydrofuran; water at 35℃; for 3.16667h; |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -70 - -30 °C / Inert atmosphere 1.2: 1 h / -70 - 20 °C / Inert atmosphere 2.1: potassium tert-butylate; potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C 3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 - 10 °C 3.2: -10 - 20 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -70 - -30 °C / Inert atmosphere 1.2: 1 h / -70 - 20 °C / Inert atmosphere 2.1: potassium tert-butylate; potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
di-{1-[2-(1-chlorocyclopropyl)-3-(2-chloro-phenyl)-2-hydroxy-propyl-1]-1,2,4-triazol-5-yl} disulphide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: iodine; magnesium / tetrahydrofuran / 1 h / Cooling with ice 1.2: 1 h / Cooling with ice 2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 50 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
prothioconazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: iodine; magnesium / tetrahydrofuran / 1 h / Cooling with ice 1.2: 1 h / Cooling with ice 2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 50 °C 3.1: zinc / methanol / 3 h / 30 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
With potassium iodide In methanol at 20 - 70℃; for 22h; | 34.6 g |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h / 21 °C / Inert atmosphere 1.2: 2 h / 21 - 40 °C 2.1: ethylene dibromide; magnesium / diethyl ether / 0.67 h / 0 - 5 °C / Inert atmosphere 2.2: 0.83 h / 0 - 5 °C 3.1: hydrogen; palladium on activated charcoal / methanol / 21 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h / 21 °C / Inert atmosphere 1.2: 2 h / 21 - 40 °C 2.1: manganese chloride bis(lithium chloride) / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere 2.2: 2 h / 0 °C View Scheme |
1-chlorocyclopropyl-2-chloro-ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h / 21 °C / Inert atmosphere 1.2: 2 h / 21 - 40 °C 2.1: ethylene dibromide; magnesium / diethyl ether / 0.67 h / 0 - 5 °C / Inert atmosphere 2.2: 0.83 h / 0 - 5 °C View Scheme |
formaldehyd
1-chlorocyclopropyl-2-chloro-ethan-1-one
ammonium thiocyanate
1-chloro-2-(chloromethyl)benzene
prothioconazole
Conditions | Yield |
---|---|
Stage #1: 1-chloro-2-(chloromethyl)benzene With iodine; magnesium at 30℃; for 3h; Inert atmosphere; Stage #2: 1-chlorocyclopropyl-2-chloro-ethan-1-one for 2h; Inert atmosphere; Stage #3: formaldehyd; ammonium thiocyanate Further stages; |
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