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inquirysodium anthraquinone-2-sulfonate
AQDSNH4
Conditions | Yield |
---|---|
Stage #1: sodium anthraquinone-2-sulfonate In water Stage #2: With ammonium hydroxide In water | 98% |
sodium anthraquinone-2-sulfonate
9,10-dioxo-9,10-dihydro-2-anthracenesulfonyl chloride
Conditions | Yield |
---|---|
With trichlorophosphate for 4h; Heating; | 95% |
With phosphorus pentachloride at 120℃; for 0.5h; | 91.7% |
With phosphorus pentachloride at 120℃; for 0.5h; | 91% |
sodium anthraquinone-2-sulfonate
2,9-bis(trifluoromethyl)-1,10-phenanthroline
[Cu(2,9-bis(trifluoromethyl)-1,10-phenanthroline)2][9,10-anthraquinone-2-sulfonate]*CH3CN
Conditions | Yield |
---|---|
With L-ascorbic acid In water; acetonitrile Cu-salt, Na-anthraquinonesulfonate and L-ascorbic acid were dissolved inhot (80°C) water, phenanthroline-compound in acetonitrile was ad ded, the soln. was stirred for 20 min at 80°C, cooled to room temp.; ppt. was filtered, dried in air; crystd. by vapor diffusion of diethyl ether into the acetonitrile-soln.; | 90% |
sodium anthraquinone-2-sulfonate
2,9-bis(trifluoromethyl)-1,10-phenanthroline
Conditions | Yield |
---|---|
With L-ascorbic acid In water; acetonitrile Cu-salt, Na-anthraquinonesulfonate and L-ascorbic acid were dissolved inhot (80°C) water, phenanthroline-compound in acetonitrile was ad ded, the soln. was stirred for 20 min at 80°C, cooled to room temp.; ppt. was filtered, dried in air; crystd. by vapor diffusion of diethyl ether into the acetonitrile-soln.; | 90% |
sodium anthraquinone-2-sulfonate
anthracene-2-sulfonic acid potassium salt
Conditions | Yield |
---|---|
Stage #1: sodium anthraquinone-2-sulfonate With ammonium carbonate In water at 80℃; Stage #2: With hydrogenchloride; zinc In water at 80℃; for 72h; Further stages; | 87% |
2.9-dimethyl-1,10-phenanthroline
sodium anthraquinone-2-sulfonate
bis(2,9-dimethyl-1,10-phenanthroline)copper(I) 9,10-anthraquinone-2-sulfonate
Conditions | Yield |
---|---|
With L-ascorbic acid In ethanol; water stoich. amt. of Na salt and Cu salt dissolved in H2O at 70°C; stoich. amt. of ligand in EtOH added; ascorbic acid added; stirred at 70°C for 2 h; cooled to room temp.; filtered; solid washed with Et2O; dried in air; | 86% |
2,11-diisopropyl-1,12-diazaperylene
sodium anthraquinone-2-sulfonate
bis(2,11-diisopropyl-1,12-diazaperylene)copper(I) 9,10-dihydro-9,10-dioxo-2-anthracenesulfonate
Conditions | Yield |
---|---|
With sodium ascorbate In ethanol; chloroform; water N2; aq. soln. of CuCl2 (0.25 mmol) added to EtOH/CHCl3 (2/1) soln. of ligand (0.5 mmol), mixt. stirred for 20 min at room temp., sodium ascorbate (0.75 mmol) in EtOH/H2O (3/1) added, stirred for 1 h, aq. soln. of NaAQSO3 (1.5 mmol) added; CHCl3 evapd., ppt. filtered off, washed (water), dried (vac., CaCl2), recrystd. (CH2Cl2/Et2O), elem. anal.; | 75% |
Conditions | Yield |
---|---|
With alkali hydroxide at 130℃; unter Druck; |
potassium phenolate
sodium anthraquinone-2-sulfonate
2-phenoxyanthraquinone
Conditions | Yield |
---|---|
at 200℃; |
Conditions | Yield |
---|---|
With sodium hydroxide at 160 - 165℃; unter Druck; man loest die Schmelze in Wasser, faellt siedend heiss mit Salzsaeure, filtriert und behandelt den Niederschlag mit siedender Barytloesung, um Alizarin abzuscheiden; die erkaltete Barytloesung faellt man mit Salzsaeure; |
Conditions | Yield |
---|---|
With potassium hydroxide; ethanol beim nachfolgende Luftoxydation; |
Conditions | Yield |
---|---|
With hydrogenchloride Sonnenlicht; | |
With hydrogenchloride; sodium chlorate at 100℃; |
sodium anthraquinone-2-sulfonate
9,10-anthracendiol-2-monosulfonic acid
Conditions | Yield |
---|---|
With iron at 85℃; Electrolysis; | |
With rongalite |
Conditions | Yield |
---|---|
With mercuri sulfate; sulfuric acid Erhitzen die Sufonsaeure mit Kalkmilch unter Druck; | |
With mercuri sulfate; sulfuric acid Erhitzen die Sufonsaeure mit Kalkmilch unter Druck; |
sodium anthraquinone-2-sulfonate
A
5-nitro-9,10-dioxo-9,10-dihydro-anthracene-2-sulfonic acid
B
1-nitroanthraquinone-7-sulphonic acid
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid |
sodium anthraquinone-2-sulfonate
Conditions | Yield |
---|---|
With phosphorus; hydrogen iodide |
Conditions | Yield |
---|---|
With ammonia; sodium chloride; calcium chloride at 105℃; unter Druck; | |
With ammonia; calcium chloride; magnesium chloride at 105℃; unter Druck; | |
With sodium nitrate; ammonium chloride; ammonia |
sodium anthraquinone-2-sulfonate
p-toluidine
2-p-toluidino-anthraquinone
Conditions | Yield |
---|---|
With sodium hydroxide; air |
Conditions | Yield |
---|---|
With sodium hydroxide; air |
Conditions | Yield |
---|---|
With sodium hydroxide |
sodium anthraquinone-2-sulfonate
dimethyl sulfate
anthraquinone-2-methylsulfonate
Conditions | Yield |
---|---|
at 160 - 170℃; |
sodium anthraquinone-2-sulfonate
2-aminoanthraquinone
2,2'-imino-di-anthraquinone
Conditions | Yield |
---|---|
With alkali carbonate |
sodium anthraquinone-2-sulfonate
diallyl-phenyl-phosphane
Conditions | Yield |
---|---|
(i) NH2Cl, NH3, Et2O, (ii) /BRN= 3580452/; Multistep reaction; |
sodium anthraquinone-2-sulfonate
sodium 1-hydroxyanthraquinone-2-sulphonate
Conditions | Yield |
---|---|
With water Mechanism; Irradiation; | |
With water Irradiation; | |
With dihydrogen peroxide Irradiation; |
sodium anthraquinone-2-sulfonate
A
C14H7O5S(2-)
Conditions | Yield |
---|---|
In water Quantum yield; Product distribution; Irradiation; anaerobic conditions, different pH, with different additives as well; |
sodium anthraquinone-2-sulfonate
9,10-anthraquinone-2-sodiumsulphonate radical anion
Conditions | Yield |
---|---|
With sodium hydroxide; triethanolamine; Eosin Y In water; isopropyl alcohol Quantum yield; Irradiation; | |
With sulfite(2-) In water; acetonitrile Quantum yield; | |
With cysteine thiol; Zn-TPPyS; cetyltrimethylammonim bromide In water Quantum yield; Irradiation; var. of reagent; |
sodium anthraquinone-2-sulfonate
Conditions | Yield |
---|---|
With fluorosulfonylchloride; fluorosulphonic acid at -20.1 - 4.9℃; Irradiation; |
sodium anthraquinone-2-sulfonate
dimethyl sulfate
9,10-dimethoxy-2-anthracenesulfonic acid sodium salt
Conditions | Yield |
---|---|
With sodium hydroxide; zinc In ethanol at 80℃; |
Conditions | Yield |
---|---|
(i) H2SO4, (ii) HNO3, H2SO4, (iii) aq. HCl, NaClO3; Multistep reaction; |
sodium anthraquinone-2-sulfonate
anthracene 2-monosulphonate sodium salt
Conditions | Yield |
---|---|
With ammonium hydroxide; zinc for 3h; | |
With ammonium hydroxide; zinc |
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