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inquiryProduct Name: Rubidium nitrate Synonyms: RUBIDIUM NITRATE, 99.99%, EXTRA PURE;Rubidium nitrate, 99.8%, pure;Rubidium nitrate, extra pure;Rubidium nitrate, pure;Rubidium nitrate, Puratronic (metals basis);RUBIDIUM NITRATE REAGENT;Rubid
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inquiryProduct Description Product website: http://www.finerchem.com Product Name Rubidium nitrate CAS No. 13126-12-0
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Rubidium nitrate CAS No.:13126-12-0 MF: NO3Rb MW: 147.47300 Exact Mass: 146.90000 Melting point:310 °C Density: 3.11 g/mL at 25 °C(lit.) Water Solubility: 44.28 g/100 mL (16 ºC) Appeara
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Product Name: Rubidium nitrate CAS: 13126-12-0 MF: NO3Rb MW: 147.47 EINECS: 236-060-1 Mol File: 13126-12-0.mol Rubidium nitrate Structure Rubidium nitrate Chemical Properties Melting point 310 °C density 3.11 g/mL at 2
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Conditions | Yield |
---|---|
In not given metathesis;; | |
In not given metathesis;; |
Conditions | Yield |
---|---|
In nitric acid react. of Rb2CO3 with the calcd. amount of dild. HNO3;; evapn. to dryness; heating at m.p.; addn. of H2O; evapn. to dryness; drying at 110°C for 3 h;; | |
In nitric acid aq. HNO3; react. of Rb2CO3 with the calcd. amount of dild. HNO3;; evapn. to dryness; heating at m.p.; addn. of H2O; evapn. to dryness; drying at 110°C for 3 h;; | |
at 120℃; |
Conditions | Yield |
---|---|
With nitric acid | |
With HNO3 |
Conditions | Yield |
---|---|
In neat (no solvent) thermic decomposition on heating at 220 - 240°C;; thermogravimetry and differential thermoanalysis;; |
Conditions | Yield |
---|---|
by heating; | |
With alk. or NaOH In not given byproducts: NaNO2, NaNO3, O2; producing H2O also; |
A
rubidium nitrate
Conditions | Yield |
---|---|
In neat (no solvent) air atm.; |
Conditions | Yield |
---|---|
In water byproducts: NOCl, Cl2, H2O; dried in air with gradual heating up to 140°C; ground; dried to const. wt. at 100°C over P2O5; | |
In nitric acid prepn. by crystn. from soln. of RbCl in concd. HNO3; recrystd. repeatedly; dried in desiccator (NaOH); |
Conditions | Yield |
---|---|
In water addn. of RbF to continuously stirred ZrO(NO3)2*2H2O soln. (5 wt% ZrO2 ininitial soln.) at room temp. with molar ratio RbF/Zr additive = 2, drop ping of concd. H3PO4 with molar ratio PO4(3-)/Zr = 1; pptn. for 7 to 45 days, filtration, washing with H2O and EtOH, drying inair; |
methanol
rubidium nitrate
Conditions | Yield |
---|---|
In methanol; water stirring suspn. of copper compd. in 0.05 M soln. of rubidium nitrate in 4:1 mixt. of methanol and water for 1 wk at room temp.; elem. anal.; | 99% |
rubidium nitrate
Cu(N,N'-ethylene-bis(3-methoxysalicylideneiminato))(H2O)
Conditions | Yield |
---|---|
In ethanol; acetonitrile at 20℃; for 2h; | 95% |
Conditions | Yield |
---|---|
In melt byproducts: HNO3; in RbNO3 melt; elem. anal.; | 93.7% |
In neat (no solvent) reaction in a stream of nitrogen, heating the mixt. to melt the nitrate at a rate of 1.0 K in a min., keeping at 588 K for 30 min.; |
rubidium nitrate
Ni(6,6'-{[ethane-1,2-diylbis(azanylylidene)]bis(methanylylidene)}bis(2-methoxyphenolate))
Conditions | Yield |
---|---|
In ethanol; acetonitrile at 20℃; for 2h; | 89% |
Conditions | Yield |
---|---|
Stage #1: 2,4,6-Trinitrophenol With magnesium oxide In water at 69.84℃; Stage #2: rubidium nitrate In water at 69.84℃; for 0.166667h; | 86% |
Conditions | Yield |
---|---|
Stage #1: styphnic acid With magnesium oxide In water at 69.84℃; Stage #2: rubidium nitrate With nitric acid In water at 69.84℃; for 0.166667h; pH=3 - 4; | 78% |
Conditions | Yield |
---|---|
at 80℃; for 24h; Kinetics; Temperature; Heating; | 76% |
Conditions | Yield |
---|---|
Stage #1: styphnic acid; water With magnesium oxide at 69.84℃; Stage #2: rubidium nitrate at 69.84℃; for 0.166667h; | 72% |
rubidium nitrate
Rb(1+)*UO2(2+)*CrO4(2-)*NO3(1-)=Rb[(UO2)(CrO4)(NO3)]
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) nitrates and oxide mixed in 1:1:1; mixt. loaded into Pt crucible, kept at 270°C for 10 h in air, cooled to 100°C (3°C/h), then to room tmep. (7°C/h); | 71% |
rubidium nitrate
C16H15N4OP
Conditions | Yield |
---|---|
In methanol; water | 70% |
rubidium nitrate
C16H15N4OP
Conditions | Yield |
---|---|
In methanol; water | 65% |
rubidium nitrate
nickel(II) acetate tetrahydrate
cobalt(II) diacetate tetrahydrate
Conditions | Yield |
---|---|
Stage #1: C36H44Au2N2O4P2S2*8H2O; nickel(II) acetate tetrahydrate; cobalt(II) diacetate tetrahydrate With air In methanol at 20℃; for 3h; Stage #2: rubidium nitrate In methanol; water at 20℃; for 168h; | A 65% B 14% |
rubidium nitrate
Conditions | Yield |
---|---|
With boric acid In water at 279.84℃; under 52505.3 Torr; for 432h; Autoclave; | A n/a B n/a C 40% |
rubidium nitrate
oxybis(benzoic acid)
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In methanol at 145℃; for 100h; | 36% |
Conditions | Yield |
---|---|
Stage #1: rhodium sulfate dodecahydrate; water; nitric acid at 20℃; Stage #2: at 80℃; Stage #3: rubidium nitrate at 120℃; for 72h; Sealed tube; High pressure; | 30% |
Conditions | Yield |
---|---|
Stage #1: sodium molybdate dihydrate; 4-azidobenzyl phosphonic acid; water With hydrogenchloride for 0.5h; Reflux; Stage #2: rubidium nitrate | 28% |
Conditions | Yield |
---|---|
In methanol; water; acetonitrile addn. of a soln. of AgNO3 in acetonitrile to a soln. of molybdenum complex in acetonitrile/methanol 2:1 with stirring, addn. of aq. (NH4)2S, stirring for 1 h, addn. of RbNO3 and crown ether in acetonitrile/water 3:1,stirring for 20 min; filtration, slow evapn. at room temp., addn. of benzene, crystn. for 10 d; elem. anal.; | 27% |
rubidium nitrate
Conditions | Yield |
---|---|
Stage #1: nickel(II) nitrate hexahydrate; C9H15NO7P2S(2-)*2Na(1+) With sodium hydroxide In water at 20℃; for 0.166667h; pH=5.5; Stage #2: Na9[A-α-PW9O34]·7H2O In water at 80℃; for 1h; pH=7.5; Stage #3: rubidium nitrate In water at 20℃; for 1h; | 27% |
rubidium nitrate
(1R,2R)-(-)-trans-cyclohexane-1,2-dicarboxylic acid
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water at 150℃; High pressure; | 24% |
Conditions | Yield |
---|---|
With air In neat (no solvent, solid phase) mixing N compd. and V2O5, heating to 600°C (storage for 24 h) or to 380°C (storage for 4 days, cooling, grinding, heating as before) in air; slow cooling to room temp. (6°C/h), XRD; | 11% |
magnesium(II) nitrate
rubidium nitrate
nitric acid
silica gel
ferric nitrate
Conditions | Yield |
---|---|
In water at 250 - 590℃; for 7h; |
Conditions | Yield |
---|---|
In neat (no solvent) reaction under reduced pressure, no quantitative reaction;; |
Conditions | Yield |
---|---|
In solid mixt. (Rb:Nb:U=1.1:1:1) heating in O2 at 1150°C for 4 h; XRD; |
Conditions | Yield |
---|---|
mixt. heating slowly from 400 to 750°C, firing (950°C, platinum crucible), annealing (1000-1200,degree.C, 1-24 h); | 0% |
Conditions | Yield |
---|---|
mixt. heating slowly from 400 to 750°C, firing (950°C, platinum crucible), annealing (1000-1200,degree.C, 1-24 h); | 0% |
rubidium nitrate
trichlorophosphate
phosphoryl(V)-thiocyanate
Conditions | Yield |
---|---|
In benzene react. in dry benzene;; | |
In benzene react. in dry benzene;; |
rubidium nitrate
trichlorophosphate
Conditions | Yield |
---|---|
In not given react. of nitrate with POCl3 forming P2O5, metal chloride and other products; constant ratio metal chloride:P2O5 for corresponding nitrate;; | |
In not given react. of nitrate with POCl3 forming P2O5, metal chloride and other products; constant ratio metal chloride:P2O5 for corresponding nitrate;; |
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