Conditions | Yield |
---|---|
In not given metathesis;; | |
In not given metathesis;; |
Conditions | Yield |
---|---|
In nitric acid react. of Rb2CO3 with the calcd. amount of dild. HNO3;; evapn. to dryness; heating at m.p.; addn. of H2O; evapn. to dryness; drying at 110°C for 3 h;; | |
In nitric acid aq. HNO3; react. of Rb2CO3 with the calcd. amount of dild. HNO3;; evapn. to dryness; heating at m.p.; addn. of H2O; evapn. to dryness; drying at 110°C for 3 h;; | |
at 120℃; |
Conditions | Yield |
---|---|
With nitric acid | |
With HNO3 |
Conditions | Yield |
---|---|
In neat (no solvent) thermic decomposition on heating at 220 - 240°C;; thermogravimetry and differential thermoanalysis;; |
Conditions | Yield |
---|---|
by heating; | |
With alk. or NaOH In not given byproducts: NaNO2, NaNO3, O2; producing H2O also; |
A
rubidium nitrate
Conditions | Yield |
---|---|
In neat (no solvent) air atm.; |
Conditions | Yield |
---|---|
In water byproducts: NOCl, Cl2, H2O; dried in air with gradual heating up to 140°C; ground; dried to const. wt. at 100°C over P2O5; | |
In nitric acid prepn. by crystn. from soln. of RbCl in concd. HNO3; recrystd. repeatedly; dried in desiccator (NaOH); |
Conditions | Yield |
---|---|
In water addn. of RbF to continuously stirred ZrO(NO3)2*2H2O soln. (5 wt% ZrO2 ininitial soln.) at room temp. with molar ratio RbF/Zr additive = 2, drop ping of concd. H3PO4 with molar ratio PO4(3-)/Zr = 1; pptn. for 7 to 45 days, filtration, washing with H2O and EtOH, drying inair; |
methanol
rubidium nitrate
Conditions | Yield |
---|---|
In methanol; water stirring suspn. of copper compd. in 0.05 M soln. of rubidium nitrate in 4:1 mixt. of methanol and water for 1 wk at room temp.; elem. anal.; | 99% |
rubidium nitrate
Cu(N,N'-ethylene-bis(3-methoxysalicylideneiminato))(H2O)
Conditions | Yield |
---|---|
In ethanol; acetonitrile at 20℃; for 2h; | 95% |
Conditions | Yield |
---|---|
In melt byproducts: HNO3; in RbNO3 melt; elem. anal.; | 93.7% |
In neat (no solvent) reaction in a stream of nitrogen, heating the mixt. to melt the nitrate at a rate of 1.0 K in a min., keeping at 588 K for 30 min.; |
rubidium nitrate
Ni(6,6'-{[ethane-1,2-diylbis(azanylylidene)]bis(methanylylidene)}bis(2-methoxyphenolate))
Conditions | Yield |
---|---|
In ethanol; acetonitrile at 20℃; for 2h; | 89% |
Conditions | Yield |
---|---|
Stage #1: 2,4,6-Trinitrophenol With magnesium oxide In water at 69.84℃; Stage #2: rubidium nitrate In water at 69.84℃; for 0.166667h; | 86% |
Conditions | Yield |
---|---|
Stage #1: styphnic acid With magnesium oxide In water at 69.84℃; Stage #2: rubidium nitrate With nitric acid In water at 69.84℃; for 0.166667h; pH=3 - 4; | 78% |
Conditions | Yield |
---|---|
at 80℃; for 24h; Kinetics; Temperature; Heating; | 76% |
Conditions | Yield |
---|---|
Stage #1: styphnic acid; water With magnesium oxide at 69.84℃; Stage #2: rubidium nitrate at 69.84℃; for 0.166667h; | 72% |
rubidium nitrate
Rb(1+)*UO2(2+)*CrO4(2-)*NO3(1-)=Rb[(UO2)(CrO4)(NO3)]
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) nitrates and oxide mixed in 1:1:1; mixt. loaded into Pt crucible, kept at 270°C for 10 h in air, cooled to 100°C (3°C/h), then to room tmep. (7°C/h); | 71% |
rubidium nitrate
C16H15N4OP
Conditions | Yield |
---|---|
In methanol; water | 70% |
rubidium nitrate
C16H15N4OP
Conditions | Yield |
---|---|
In methanol; water | 65% |
rubidium nitrate
nickel(II) acetate tetrahydrate
cobalt(II) diacetate tetrahydrate
Conditions | Yield |
---|---|
Stage #1: C36H44Au2N2O4P2S2*8H2O; nickel(II) acetate tetrahydrate; cobalt(II) diacetate tetrahydrate With air In methanol at 20℃; for 3h; Stage #2: rubidium nitrate In methanol; water at 20℃; for 168h; | A 65% B 14% |
rubidium nitrate
Conditions | Yield |
---|---|
With boric acid In water at 279.84℃; under 52505.3 Torr; for 432h; Autoclave; | A n/a B n/a C 40% |
rubidium nitrate
oxybis(benzoic acid)
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In methanol at 145℃; for 100h; | 36% |
Conditions | Yield |
---|---|
Stage #1: rhodium sulfate dodecahydrate; water; nitric acid at 20℃; Stage #2: at 80℃; Stage #3: rubidium nitrate at 120℃; for 72h; Sealed tube; High pressure; | 30% |
Conditions | Yield |
---|---|
Stage #1: sodium molybdate dihydrate; 4-azidobenzyl phosphonic acid; water With hydrogenchloride for 0.5h; Reflux; Stage #2: rubidium nitrate | 28% |
Conditions | Yield |
---|---|
In methanol; water; acetonitrile addn. of a soln. of AgNO3 in acetonitrile to a soln. of molybdenum complex in acetonitrile/methanol 2:1 with stirring, addn. of aq. (NH4)2S, stirring for 1 h, addn. of RbNO3 and crown ether in acetonitrile/water 3:1,stirring for 20 min; filtration, slow evapn. at room temp., addn. of benzene, crystn. for 10 d; elem. anal.; | 27% |
rubidium nitrate
Conditions | Yield |
---|---|
Stage #1: nickel(II) nitrate hexahydrate; C9H15NO7P2S(2-)*2Na(1+) With sodium hydroxide In water at 20℃; for 0.166667h; pH=5.5; Stage #2: Na9[A-α-PW9O34]·7H2O In water at 80℃; for 1h; pH=7.5; Stage #3: rubidium nitrate In water at 20℃; for 1h; | 27% |
rubidium nitrate
(1R,2R)-(-)-trans-cyclohexane-1,2-dicarboxylic acid
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water at 150℃; High pressure; | 24% |
Conditions | Yield |
---|---|
With air In neat (no solvent, solid phase) mixing N compd. and V2O5, heating to 600°C (storage for 24 h) or to 380°C (storage for 4 days, cooling, grinding, heating as before) in air; slow cooling to room temp. (6°C/h), XRD; | 11% |
magnesium(II) nitrate
rubidium nitrate
nitric acid
silica gel
ferric nitrate
Conditions | Yield |
---|---|
In water at 250 - 590℃; for 7h; |
Conditions | Yield |
---|---|
In neat (no solvent) reaction under reduced pressure, no quantitative reaction;; |
Conditions | Yield |
---|---|
In solid mixt. (Rb:Nb:U=1.1:1:1) heating in O2 at 1150°C for 4 h; XRD; |
Conditions | Yield |
---|---|
mixt. heating slowly from 400 to 750°C, firing (950°C, platinum crucible), annealing (1000-1200,degree.C, 1-24 h); | 0% |
Conditions | Yield |
---|---|
mixt. heating slowly from 400 to 750°C, firing (950°C, platinum crucible), annealing (1000-1200,degree.C, 1-24 h); | 0% |
rubidium nitrate
trichlorophosphate
phosphoryl(V)-thiocyanate
Conditions | Yield |
---|---|
In benzene react. in dry benzene;; | |
In benzene react. in dry benzene;; |
rubidium nitrate
trichlorophosphate
Conditions | Yield |
---|---|
In not given react. of nitrate with POCl3 forming P2O5, metal chloride and other products; constant ratio metal chloride:P2O5 for corresponding nitrate;; | |
In not given react. of nitrate with POCl3 forming P2O5, metal chloride and other products; constant ratio metal chloride:P2O5 for corresponding nitrate;; |
Rubidium nitrate is an organic compound with the formula RbNO3, and its systematic name is the same with the product name. With the CAS registry number 13126-12-0, it is also named as Nitric acid, rubidium salt. It belongs to the product categories of AAS; AAS CRMsAnalytical Standards; AASSpectroscopy; Alphabetic; Application CRMs; R; Spectroscopy; Hematology Stains Synthetic Reagents; Hematology and Histology; Rubidium; Inorganic Salts; Rubidium Salts; RubidiumMetal and Ceramic Science; Salts; Synthetic Reagents; Metal nitrate salts. Its EINECS number is 236-060-1. In addition, the molecular weight is 147.47. This chemical is stable at common pressure and temperature, and it should be sealed and stored in a cool, ventilated and dry place. Moreover, it should be protected from reducing agents.
Physical properties of Rubidium nitrate are: (1)ACD/LogP: -0.129; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -0.13; (4)ACD/LogD (pH 7.4): -0.13; (5)ACD/BCF (pH 5.5): 1.00; (6)ACD/BCF (pH 7.4): 1.00; (7)#H bond acceptors: 4; (8)#H bond donors: 1; (9)#Freely Rotating Bonds: 0; (10)Polar Surface Area: 66.05 Å2; (11)Enthalpy of Vaporization: 37.72 kJ/mol; (12)Boiling Point: 83 °C at 760 mmHg; (13)Vapour Pressure: 49.8 mmHg at 25°C.
Preparation: rubidium carbonate dissolves in nitric acid, and then concentrate the solution, and the final products are got.
When you are using this chemical, please be cautious about it as the following:
This chemcial is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. When it contacts with combustible material, it may cause fire, so you should keep it away from combustible material. When using it, you need to wear suitable protective clothing, gloves and eye/face protection.
You can still convert the following datas into molecular structure:
(1)SMILES: [Rb+].[O-][N+]([O-])=O
(2)Std. InChI: InChI=1S/NO3.Rb/c2-1(3)4;/q-1;+1
(3)Std. InChIKey: RTHYXYOJKHGZJT-UHFFFAOYSA-N
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