As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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ACY-1215/1316214-52-4/high purity 99% in stockAppearance:white or off-white powder Storage:keep away from heat,sparks and flames Package:according to customers' requirements Application:pharmaceutical research Transportation:By air(EMS or EUB or FedE
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Wuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryLow price and high quality Appearance:white powder Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:ACY1215,Rocilinostat Transportation:shipping,land,ai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryGMP factory Packing with pallet as buyer's special request Best service after shipment with e-mail Cargos together with container sales seervice available Api, inhibitor, and fine chemicals for more than 6 years. Application:Inhibitor
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate
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inquiryFactory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
ACY-1215Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
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inquiryACY-1215/1316214-52-4/high purity 99% in stockAppearance:white or off-white powder Storage:keep away from heat,sparks and flames Package:1g/bag 10/bag 100g/bag 1kg/bag 10kg/bag 100kg/bag Application:pharmaceutical research Transportation:by air or by
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inquiryOur mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
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inquiryC25H28N4O3
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Stage #1: C25H28N4O3 With sodium hydroxide In methanol; dichloromethane at 0℃; for 0.166667h; Stage #2: With hydroxylamine In methanol; dichloromethane; water at 0 - 20℃; for 0.333333h; Stage #3: With hydrogenchloride In water | 48% |
Stage #1: C25H28N4O3 With methanol; sodium hydroxide In dichloromethane at 0℃; for 0.166667h; Stage #2: With hydroxylamine In dichloromethane at 0 - 20℃; for 0.333333h; | 48% |
Stage #1: C25H28N4O3 With sodium hydroxide In methanol; dichloromethane at 0℃; for 0.166667h; Stage #2: With hydroxylamine In methanol; dichloromethane at 0 - 20℃; for 20h; | 48% |
ethyl 2-chloropyrimidine-5-carboxylate
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C 2.1: caesium carbonate / copper(l) iodide / tetraethoxy orthosilicate / 14 h / 140 °C 3.1: water / ethanol / 0.5 h / 60 °C 4.1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C 5.1: sodium hydroxide / dichloromethane; methanol / 0.17 h / 0 °C 5.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C / Inert atmosphere 2.1: tetraethoxy orthosilicate; copper(l) iodide; caesium carbonate / 14 h / 140 °C / Inert atmosphere 3.1: sodium hydroxide; ethanol / 0.5 h / 60 °C 4.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 5.1: sodium hydroxide; methanol / dichloromethane / 0.17 h / 0 °C 5.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C / Inert atmosphere 2.1: copper(l) iodide; caesium carbonate; tetraethoxy orthosilicate / 14 h / 140 °C / Inert atmosphere 3.1: sodium hydroxide / ethanol / 0.5 h / 60 °C 4.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 5.1: sodium hydroxide / methanol; dichloromethane / 0.17 h / 0 °C 5.2: 20 h / 0 - 20 °C View Scheme |
aniline
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C 2.1: caesium carbonate / copper(l) iodide / tetraethoxy orthosilicate / 14 h / 140 °C 3.1: water / ethanol / 0.5 h / 60 °C 4.1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C 5.1: sodium hydroxide / dichloromethane; methanol / 0.17 h / 0 °C 5.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C / Inert atmosphere 2.1: tetraethoxy orthosilicate; copper(l) iodide; caesium carbonate / 14 h / 140 °C / Inert atmosphere 3.1: sodium hydroxide; ethanol / 0.5 h / 60 °C 4.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 5.1: sodium hydroxide; methanol / dichloromethane / 0.17 h / 0 °C 5.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C / Inert atmosphere 2.1: copper(l) iodide; caesium carbonate; tetraethoxy orthosilicate / 14 h / 140 °C / Inert atmosphere 3.1: sodium hydroxide / ethanol / 0.5 h / 60 °C 4.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 5.1: sodium hydroxide / methanol; dichloromethane / 0.17 h / 0 °C 5.2: 20 h / 0 - 20 °C View Scheme |
ethyl 2-(phenylamino)pyrimidine-5-carboxylate
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: caesium carbonate / copper(l) iodide / tetraethoxy orthosilicate / 14 h / 140 °C 2.1: water / ethanol / 0.5 h / 60 °C 3.1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C 4.1: sodium hydroxide / dichloromethane; methanol / 0.17 h / 0 °C 4.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: tetraethoxy orthosilicate; copper(l) iodide; caesium carbonate / 14 h / 140 °C / Inert atmosphere 2.1: sodium hydroxide; ethanol / 0.5 h / 60 °C 3.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 4.1: sodium hydroxide; methanol / dichloromethane / 0.17 h / 0 °C 4.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: copper(l) iodide; caesium carbonate; tetraethoxy orthosilicate / 14 h / 140 °C / Inert atmosphere 2.1: sodium hydroxide / ethanol / 0.5 h / 60 °C 3.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 4.1: sodium hydroxide / methanol; dichloromethane / 0.17 h / 0 °C 4.2: 20 h / 0 - 20 °C View Scheme |
C19H17N3O2
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: water / ethanol / 0.5 h / 60 °C 2.1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C 3.1: sodium hydroxide / dichloromethane; methanol / 0.17 h / 0 °C 3.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide; ethanol / 0.5 h / 60 °C 2.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 3.1: sodium hydroxide; methanol / dichloromethane / 0.17 h / 0 °C 3.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide / ethanol / 0.5 h / 60 °C 2.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 3.1: sodium hydroxide / methanol; dichloromethane / 0.17 h / 0 °C 3.2: 20 h / 0 - 20 °C View Scheme |
C17H13N3O2
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C 2.1: sodium hydroxide / dichloromethane; methanol / 0.17 h / 0 °C 2.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 2.1: sodium hydroxide; methanol / dichloromethane / 0.17 h / 0 °C 2.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 2.1: sodium hydroxide / methanol; dichloromethane / 0.17 h / 0 °C 2.2: 20 h / 0 - 20 °C View Scheme |
2-hydroxy-pyrimidine-5-carboxylic acid ethyl ester
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: dmap; trichlorophosphate / 1.5 h / Reflux 1.2: pH 7 2.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C 3.1: caesium carbonate / copper(l) iodide / tetraethoxy orthosilicate / 14 h / 140 °C 4.1: water / ethanol / 0.5 h / 60 °C 5.1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C 6.1: sodium hydroxide / dichloromethane; methanol / 0.17 h / 0 °C 6.2: 0.33 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 6 steps 1.1: trichlorophosphate; dmap / 1.5 h / Reflux 1.2: pH 7 2.1: potassium carbonate / N,N-dimethyl-formamide / 120 °C / Inert atmosphere 3.1: tetraethoxy orthosilicate; copper(l) iodide; caesium carbonate / 14 h / 140 °C / Inert atmosphere 4.1: sodium hydroxide; ethanol / 0.5 h / 60 °C 5.1: HATU; N-ethyl-N,N-diisopropylamine / 20 °C 6.1: sodium hydroxide; methanol / dichloromethane / 0.17 h / 0 °C 6.2: 0.33 h / 0 - 20 °C View Scheme |
4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
With sodium hydroxide; hydroxylamine |
iodobenzene
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: copper(l) iodide; caesium carbonate / 14 h / 140 °C / Inert atmosphere 2.1: sodium hydroxide / ethanol / 0.5 h / 60 °C 3.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C 4.1: sodium hydroxide / methanol; dichloromethane / 0.17 h / 0 °C 4.2: 0.33 h / 0 - 20 °C View Scheme |
methyl 7-aminoheptanoate
C17H13N3O2
N-[7-(hydroxyamino)-7-oxo-heptyl]-2-(N-phenylanilino)pyrimidine-5-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C 2.1: sodium hydroxide / methanol; dichloromethane / 0.17 h / 0 °C 2.2: 0.33 h / 0 - 20 °C View Scheme |
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