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Dayang Chem (Hangzhou) Co.,Ltd.

img heightAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals,

Celestolide Manufacturer/High quality/Best price/In stock

Cas:13171-00-1

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Celestolide supplier in China

Cas:13171-00-1

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 6-tert-butyl-1,1-dimethylindan-4-yl methyl ketone

Cas:13171-00-1

Min.Order:1

Negotiable

Type:Other

inquiry

Nanjing Yuance Industry&Trade Co., Ltd.

We are a leading manufacturer of flavors and fragrances located in Eastern China. We can supply many kinds of aroma chemicals. Appearance:White to off-white powder or crystal Storage:Keep in low temperature sealed container (0-10oC). Package:25kg/C

Celestolide

Cas:13171-00-1

Min.Order:200 Kilogram

Negotiable

Type:Trading Company

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4-Acetyl-6-tert-butyl-1,1-dimethylindane

Cas:13171-00-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Celestolide

Cas:13171-00-1

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

China Gold Supplier CAS 13171-00-1 with best quality

Cas:13171-00-1

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Celestolide 13171-00-1

Cas:13171-00-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

Celestolide CAS: 13171-00-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate

Celestolide CAS: 13171-00-1

Cas:13171-00-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Celestolide

Cas:13171-00-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

Celestolide CAS NO.13171-00-1

Cas:13171-00-1

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Celestolide

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Celestolide

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Celestolide

Cas:13171-00-1

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

Celestolide factory price, Cas No: 13171-00-1Appearance:white powder Storage:Store in a cool dry place and keep away from strong light Package:according to customers' requirements Application:in research Transportation:By air(EMS or EUB or FedEx or

Celestolide factory price, Cas No: 13171-00-1

Cas:13171-00-1

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Henan Tianfu Chemical Co., Ltd.

Celestolide Basic information Identification Description Regulatory Status Natural occurrence Product Name: Celestolide

13171-00-1 Celestolide C17H24O

Cas:13171-00-1

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Celestolide

Cas:13171-00-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Celestolide Basic information Product Name: Celestolide Synonyms: 1-(6-tert-Butyl-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethanone;1-[6-(1,1-dimethylethyl)-2,3-dihydro-1,1-dimethyl-1h-inden-4-yl]-ethanon;1-[6-(1,1-dimethylethyl)-2,3-dihydro-1,1

Celestolide

Cas:13171-00-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

4-ACETYL-6-TERT-BUTYL-1,1-DIMETHYLINDANE CAS NO.13171-00-1 CAS NO.13171-00-1

Cas:13171-00-1

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an

Celestolide

Cas:13171-00-1

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Celestolide factory price, Cas No: 13171-00-1

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

NIGNXIA XINDACHANG TECHNOLOGY CO.,LTD

Name: Celestolide Molecular Formula: C17H24O Odor: Musk, wood, fragrant smell, the smell feel soft and strong, with great durability. Flashing point: … Appearance:White crystal Storage:normal temp Package:1kg/5kg/25kg/50kg/180/kg Applicatio

Celestolide

Cas:13171-00-1

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Wuhan Kemi-Works Chemical Co., Ltd

Celestolide CAS No. 13171-00-1 Molecular Formula:C17H24O Molecular Weight:244.37 Appearance:White crystals ISO9001 Appearance:white crystal Storage:store in dry and cool place Package: 25kg/drum, or as per your request. Application:Ph

Celestolide

Cas:13171-00-1

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Celestolide cas no. 13171-00-1 98%

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Vanz Pharm Co.,Ltd

ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai

Celestolide

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

6-tert-butyl-1,1-dimethylindan-4-yl methyl ketone

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

1-(6-(tert-Butyl)-1,1-diMethyl-2,3-dihydro-1H-inden-4-yl)ethanone

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

4-Acetyl-6-tert-Butyl-1,1-dimethylindane

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 4-Acetyl-6-tert-butyl-1,1-dimethylindan 5g

Cas:13171-00-1

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

4-Acetyl-6-tert-butyl-1,1-diMethylindan

Cas:13171-00-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

6-tert-butyl-1,1-dimethylindane
3605-31-0

6-tert-butyl-1,1-dimethylindane

acetyl chloride
75-36-5

acetyl chloride

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
With aluminium trichloride In dichloromethane Friedel-Crafts reaction;62%
With tetrachloromethane; aluminium trichloride
aluminium trichloride In hexane
6-tert-butyl-1,1-dimethylindane
3605-31-0

6-tert-butyl-1,1-dimethylindane

acetyl chloride
75-36-5

acetyl chloride

A

6-acetyl-1,1-dimethyl-4-tertbutylindane
102296-26-4

6-acetyl-1,1-dimethyl-4-tertbutylindane

B

Celestolide
13171-00-1

Celestolide

C

1-(3,3-dimethylindan-5-yl)ethanone
102296-45-7

1-(3,3-dimethylindan-5-yl)ethanone

D

1-(1,1-dimethyl-2,3-dihydro-1H-inden-5-yl)ethan-1-one
102296-44-6

1-(1,1-dimethyl-2,3-dihydro-1H-inden-5-yl)ethan-1-one

Conditions
ConditionsYield
With aluminium trichloride In various solvent(s) at 0 - 5℃; for 1h; Further byproducts given;A n/a
B 50.4%
C n/a
D n/a
With aluminium trichloride In various solvent(s) at 0 - 5℃; for 1h; Further byproducts given;
6-tert-butyl-1,1-dimethylindane
3605-31-0

6-tert-butyl-1,1-dimethylindane

acetyl chloride
75-36-5

acetyl chloride

A

Celestolide
13171-00-1

Celestolide

B

1-(3,3-dimethylindan-5-yl)ethanone
102296-45-7

1-(3,3-dimethylindan-5-yl)ethanone

Conditions
ConditionsYield
With tetrachloromethane; aluminium trichloride
5-(tert-butyl)-1,1-dimethyl-2,3-dihydro-1H-indene
38393-97-4

5-(tert-butyl)-1,1-dimethyl-2,3-dihydro-1H-indene

acetyl chloride
75-36-5

acetyl chloride

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
With aluminium trichloride; nitrobenzene; 1,2-dichloro-ethane
6-tert-butyl-1,1-dimethylindane
3605-31-0

6-tert-butyl-1,1-dimethylindane

acetyl chloride
75-36-5

acetyl chloride

A

6-acetyl-1,1-dimethyl-4-tertbutylindane
102296-26-4

6-acetyl-1,1-dimethyl-4-tertbutylindane

B

Celestolide
13171-00-1

Celestolide

C

1-(3,3-dimethylindan-5-yl)ethanone
102296-45-7

1-(3,3-dimethylindan-5-yl)ethanone

D

5-acetyl-1,1-dimethyl-6-tert-butylindane
133631-95-5

5-acetyl-1,1-dimethyl-6-tert-butylindane

Conditions
ConditionsYield
With aluminium trichloride In various solvent(s) at 0 - 5℃; for 1h; Further byproducts given. Title compound not separated from byproducts;
6-tert-butyl-1,1-dimethylindane
3605-31-0

6-tert-butyl-1,1-dimethylindane

acetyl chloride
75-36-5

acetyl chloride

A

6-acetyl-1,1-dimethyl-4-tertbutylindane
102296-26-4

6-acetyl-1,1-dimethyl-4-tertbutylindane

B

Celestolide
13171-00-1

Celestolide

C

1-(1,1-dimethyl-2,3-dihydro-1H-inden-5-yl)ethan-1-one
102296-44-6

1-(1,1-dimethyl-2,3-dihydro-1H-inden-5-yl)ethan-1-one

D

6-acetyl-1,1-dimethyl-5-tert-butylindane
132684-99-2

6-acetyl-1,1-dimethyl-5-tert-butylindane

Conditions
ConditionsYield
With aluminium trichloride In various solvent(s) at 0 - 5℃; for 1h; Further byproducts given. Title compound not separated from byproducts;
aluminium trichloride
7446-70-0

aluminium trichloride

6-tert-butyl-1,1-dimethylindane
3605-31-0

6-tert-butyl-1,1-dimethylindane

nitrobenzene
98-95-3

nitrobenzene

1,2-dichloro-ethane
107-06-2

1,2-dichloro-ethane

acetyl chloride
75-36-5

acetyl chloride

Celestolide
13171-00-1

Celestolide

aluminium trichloride
7446-70-0

aluminium trichloride

6-tert-butyl-1,1-dimethylindane
3605-31-0

6-tert-butyl-1,1-dimethylindane

acetyl chloride
75-36-5

acetyl chloride

CCl2

CCl2

Celestolide
13171-00-1

Celestolide

tert-butylbenzene
253185-03-4, 253185-04-5

tert-butylbenzene

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 50 percent / AlCl3 / nitromethane
2: 62 percent / AlCl3 / CH2Cl2
View Scheme
isoprene
78-79-5

isoprene

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 50 percent / AlCl3 / nitromethane
2: 62 percent / AlCl3 / CH2Cl2
View Scheme
6-tert-butyl-1,1-dimethyl-4-indancarboxylic acid
61813-34-1

6-tert-butyl-1,1-dimethyl-4-indancarboxylic acid

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: quinoline; CuO; copper-powder / 200 - 230 °C
2: AlCl3; CCl4
View Scheme
1,1-dimethylindan
4912-92-9

1,1-dimethylindan

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: AlCl3; CS2
2: AlCl3; CCl4
View Scheme
Multi-step reaction with 2 steps
1: AlCl3; CS2
2: AlCl3; 1,2-dichloro-ethane; nitrobenzene
View Scheme
Multi-step reaction with 2 steps
1: concentrated H2SO4
2: AlCl3; CCl4
View Scheme
Multi-step reaction with 2 steps
1: concentrated H2SO4
2: AlCl3; CCl4
View Scheme
4-Phenyl-2-butanone
2550-26-7

4-Phenyl-2-butanone

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: H2SO4
2: methyl magnesium bromide; diethyl ether
3: aqueous H2SO4
4: AlCl3; CCl4
View Scheme
4-(4-tert-butylphenyl)butan-2-one
65170-86-7

4-(4-tert-butylphenyl)butan-2-one

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: methyl magnesium bromide; diethyl ether
2: aqueous H2SO4
3: AlCl3; CCl4
View Scheme
4-(4-tert-butyl-phenyl)-2-methyl-butan-2-ol
72390-27-3

4-(4-tert-butyl-phenyl)-2-methyl-butan-2-ol

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aqueous H2SO4
2: AlCl3; CCl4
View Scheme
Multi-step reaction with 2 steps
1: aqueous H2SO4
2: AlCl3; CCl4
View Scheme
6-tert-butyl-3,3-dimethyl-1-indanone
38393-94-1

6-tert-butyl-3,3-dimethyl-1-indanone

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N2H4+H2O; KOH; triethylene glycol / 210 °C
2: AlCl3; 1,2-dichloro-ethane; nitrobenzene
View Scheme
3-(4-tert-butyl-phenyl)propionic acid methyl ester
1211-99-0

3-(4-tert-butyl-phenyl)propionic acid methyl ester

Celestolide
13171-00-1

Celestolide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: methyl magnesium bromide; diethyl ether
2: aqueous H2SO4
3: AlCl3; CCl4
View Scheme
Multi-step reaction with 3 steps
1: methyl magnesium bromide; diethyl ether
2: aqueous H2SO4
3: AlCl3; CCl4
View Scheme
Celestolide
13171-00-1

Celestolide

1-(6-tert-butyl-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethanol

1-(6-tert-butyl-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethanol

Conditions
ConditionsYield
With methanol; sodium tetrahydroborate at 0℃; for 4.33333h; Time;98.2%
Celestolide
13171-00-1

Celestolide

6-tert-butyl-1,1-dimethyl-2,3-dihydro-1H-inden-4-amine
132567-92-1

6-tert-butyl-1,1-dimethyl-2,3-dihydro-1H-inden-4-amine

Conditions
ConditionsYield
With methanol; O-benzenesulfonyl-acetohydroxamic acid ethyl ester; toluene-4-sulfonic acid at 23℃; for 24h; Inert atmosphere;95%
Multi-step reaction with 3 steps
1: NH2OH*HCl; pyridine / ethanol
2: SOCl2 / CH2Cl2
3: aq. HCl / ethanol / Heating
View Scheme
Celestolide
13171-00-1

Celestolide

1-(3-azido-6-(tert-butyl)-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethan-1-one

1-(3-azido-6-(tert-butyl)-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethan-1-one

Conditions
ConditionsYield
With trimethylsilylazide; copper diacetate; (S,S)-4,4'-bis(phenylmethyl)-2,2',5,5'-tetrahydro-2,2'-bioxazole; N-fluorobis(benzenesulfon)imide In nitromethane at 30℃; for 24h; Inert atmosphere; Sealed tube;92%
With sodium azide; iodosylbenzene; C32H46ClMnN2O2 In water; ethyl acetate at 23℃;74%
With sodium azide; lithium perchlorate In acetic acid; acetonitrile at 25℃; for 10h; Inert atmosphere; Electrochemical reaction;65%
With sodium azide; 1,10-Phenanthroline; manganese(II) fluoride; lithium perchlorate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetic acid; 1,2-dichloro-ethane; acetonitrile at 35℃; for 21h; Inert atmosphere; Electrolysis; Irradiation; Schlenk technique;51%
Celestolide
13171-00-1

Celestolide

1-(6-(tert-butyl)-3-chloro-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethan-1-one

1-(6-(tert-butyl)-3-chloro-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethan-1-one

Conditions
ConditionsYield
With dichloro(1,10-phenanthroline) copper(II); 1-azido-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one In acetonitrile at 20℃; for 48h; Reagent/catalyst; Solvent; Inert atmosphere; Sealed tube;91%
Celestolide
13171-00-1

Celestolide

1-(6-(tert-butyl)-3-fluoro-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethan-1-one

1-(6-(tert-butyl)-3-fluoro-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)ethan-1-one

Conditions
ConditionsYield
With xanth-9-one; Selectfluor In acetonitrile at 60℃; for 0.15h; Inert atmosphere; Flow reactor; Irradiation;88%
With (S,S)-chloro[2,2'-[1,2-cyclohexanediylbis(nitrilomethylidyne)]bis-[4,6-bis(1,1-dimethylethyl)phenolato]](2-)-N,N',O,O'-manganese; iodosylbenzene; triethylamine tris(hydrogen fluoride) In acetonitrile at 50℃; Reagent/catalyst; Temperature; Time; Schlenk technique; Inert atmosphere;67%
With (S,S)-chloro[2,2'-[1,2-cyclohexanediylbis(nitrilomethylidyne)]bis-[4,6-bis(1,1-dimethylethyl)phenolato]](2-)-N,N',O,O'-manganese; iodosylbenzene; triethylamine tris(hydrogen fluoride) In acetonitrile at 50℃; Schlenk technique; Inert atmosphere;
With dihydroxy-methyl-borane; bathophenanthroline; copper (I) acetate; lithium carbonate; N-fluorobis(benzenesulfon)imide In chlorobenzene at 45℃; for 16h; Glovebox; Inert atmosphere;
Celestolide
13171-00-1

Celestolide

N-(6-tert-butyl-1,1-dimethylindan-4-yl)acetamide
101866-05-1

N-(6-tert-butyl-1,1-dimethylindan-4-yl)acetamide

Conditions
ConditionsYield
With O-benzenesulfonyl-acetohydroxamic acid ethyl ester; toluene-4-sulfonic acid In water; acetonitrile at 23℃; for 24h; Inert atmosphere;87%
Multi-step reaction with 2 steps
1: NH2OH*HCl; pyridine / ethanol
2: SOCl2 / CH2Cl2
View Scheme
2-(aminoxy)acetic acid hydrochloride

2-(aminoxy)acetic acid hydrochloride

Celestolide
13171-00-1

Celestolide

C19H27NO3

C19H27NO3

Conditions
ConditionsYield
With sodium acetate In methanol at 20℃;85.9%
Celestolide
13171-00-1

Celestolide

7-acetyl-5-tert-butyl-3,3-dimethyl-indan-1-one

7-acetyl-5-tert-butyl-3,3-dimethyl-indan-1-one

Conditions
ConditionsYield
With tert.-butylhydroperoxide In water; acetonitrile at 50℃; for 15h; Electrolysis;74%
With tetra-O-acetyl riboflavin; ferrous perchlorate; oxygen In water; acetonitrile at 50℃; for 0.416667h; UV-irradiation; Flow reactor;7%
Celestolide
13171-00-1

Celestolide

t-butyldimethylsiyl triflate
69739-34-0

t-butyldimethylsiyl triflate

tert-butyl((1-(6-(tert-butyl)-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)vinyl)oxy)dimethylsilane

tert-butyl((1-(6-(tert-butyl)-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl)vinyl)oxy)dimethylsilane

Conditions
ConditionsYield
Stage #1: Celestolide With triethylamine In dichloromethane at 20℃; for 1h; Schlenk technique; Inert atmosphere;
Stage #2: t-butyldimethylsiyl triflate In dichloromethane for 3h; Schlenk technique; Inert atmosphere;
70%
2-((trifluoromethyl)thio)isoindoline-1,3-dione
719-98-2

2-((trifluoromethyl)thio)isoindoline-1,3-dione

Celestolide
13171-00-1

Celestolide

C18H23F3OS

C18H23F3OS

Conditions
ConditionsYield
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; potassium carbonate In acetonitrile at 20℃; for 12h; Inert atmosphere; Irradiation;62%
Celestolide
13171-00-1

Celestolide

(2,2’-bipyridine)Zn(CF3)2

(2,2’-bipyridine)Zn(CF3)2

1-(6-(tert-butyl)-1,1-dimethyl-3-(trifluoromethyl)-2,3-dihydro-1H-inden-4-yl)ethanone

1-(6-(tert-butyl)-1,1-dimethyl-3-(trifluoromethyl)-2,3-dihydro-1H-inden-4-yl)ethanone

Conditions
ConditionsYield
With zinc diacetate; copper(l) cyanide; zinc trifluoromethanesulfonate; N-fluorobis(benzenesulfon)imide at 20℃; for 24h; Sealed tube; Inert atmosphere;53%
[bis(acetoxy)iodo]benzene
3240-34-4

[bis(acetoxy)iodo]benzene

Celestolide
13171-00-1

Celestolide

7-acetyl-5-(tert-butyl)-3,3-dimethyl-2,3-dihydro-1H-inden-1-yl acetate

7-acetyl-5-(tert-butyl)-3,3-dimethyl-2,3-dihydro-1H-inden-1-yl acetate

Conditions
ConditionsYield
With 9-mesityl-1,3,6,8-tetramethoxy-10-phenylacridin-10-ium tetrafluoroborate In dichloromethane at 25 - 40℃; for 24h; Schlenk technique; Inert atmosphere; Irradiation;41%
Celestolide
13171-00-1

Celestolide

6-tert-butyl-1,1-dimethyl-4-indancarboxylic acid
61813-34-1

6-tert-butyl-1,1-dimethyl-4-indancarboxylic acid

Conditions
ConditionsYield
With sodium hypochlorite; sodium hypobromide
With 1,4-dioxane; potassium hypobromite
With sodium hypobromide In 1,4-dioxane
Celestolide
13171-00-1

Celestolide

4-ethyl-6-tert-butyl-1,1-dimethyl-indan
3247-65-2

4-ethyl-6-tert-butyl-1,1-dimethyl-indan

Conditions
ConditionsYield
With methanol; platinum on activated charcoal; palladium dichloride Hydrogenation;
Celestolide
13171-00-1

Celestolide

diethyl chlorophosphate
814-49-3

diethyl chlorophosphate

phosphoric acid 1-(6-tert-butyl-1,1-dimethyl-indan-4-yl)-vinyl ester diethyl ester

phosphoric acid 1-(6-tert-butyl-1,1-dimethyl-indan-4-yl)-vinyl ester diethyl ester

Conditions
ConditionsYield
Stage #1: Celestolide With lithium diisopropyl amide In tetrahydrofuran at -78℃;
Stage #2: diethyl chlorophosphate In tetrahydrofuran
Stage #1: Celestolide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere;
Stage #2: diethyl chlorophosphate In tetrahydrofuran at -78 - 20℃; for 1h; Inert atmosphere;
Celestolide
13171-00-1

Celestolide

1-(6-tert-butyl-1,1-dimethyl-indan-4-yl)-ethanone oxime
175136-27-3

1-(6-tert-butyl-1,1-dimethyl-indan-4-yl)-ethanone oxime

Conditions
ConditionsYield
With pyridine; hydroxylamine hydrochloride In ethanol
With hydroxylamine hydrochloride; sodium acetate In ethanol at 90℃; for 2h; Sealed tube; Inert atmosphere;
Celestolide
13171-00-1

Celestolide

(2E,4E)-6-(6-tert-Butyl-1,1-dimethyl-indan-4-ylamino)-3-methyl-hexa-2,4-dienoic acid ethyl ester
889444-00-2

(2E,4E)-6-(6-tert-Butyl-1,1-dimethyl-indan-4-ylamino)-3-methyl-hexa-2,4-dienoic acid ethyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: NH2OH*HCl; pyridine / ethanol
2: SOCl2 / CH2Cl2
3: aq. HCl / ethanol / Heating
4: NaCNBH3; ZnCl2 / methanol
View Scheme
Celestolide
13171-00-1

Celestolide

(2E,4E)-6-[(6-tert-Butyl-1,1-dimethyl-indan-4-yl)-isopropyl-amino]-3-methyl-hexa-2,4-dienoic acid ethyl ester
886861-94-5

(2E,4E)-6-[(6-tert-Butyl-1,1-dimethyl-indan-4-yl)-isopropyl-amino]-3-methyl-hexa-2,4-dienoic acid ethyl ester

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: NH2OH*HCl; pyridine / ethanol
2: SOCl2 / CH2Cl2
3: aq. HCl / ethanol / Heating
4: NaCNBH3; ZnCl2 / methanol
5: K2CO3 / N,N-dimethyl-acetamide
View Scheme
Celestolide
13171-00-1

Celestolide

(2E,4E)-6-[(6-tert-Butyl-1,1-dimethyl-indan-4-yl)-isopropyl-amino]-3-methyl-hexa-2,4-dienoic acid

(2E,4E)-6-[(6-tert-Butyl-1,1-dimethyl-indan-4-yl)-isopropyl-amino]-3-methyl-hexa-2,4-dienoic acid

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: NH2OH*HCl; pyridine / ethanol
2: SOCl2 / CH2Cl2
3: aq. HCl / ethanol / Heating
4: NaCNBH3; ZnCl2 / methanol
5: K2CO3 / N,N-dimethyl-acetamide
6: KOH / methanol
View Scheme
Celestolide
13171-00-1

Celestolide

(2E,4E)-6-[(6-tert-Butyl-1,1-dimethyl-indan-4-yl)-propyl-amino]-3-methyl-hexa-2,4-dienoic acid

(2E,4E)-6-[(6-tert-Butyl-1,1-dimethyl-indan-4-yl)-propyl-amino]-3-methyl-hexa-2,4-dienoic acid

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: NH2OH*HCl; pyridine / ethanol
2: SOCl2 / CH2Cl2
3: aq. HCl / ethanol / Heating
4: NaCNBH3; ZnCl2 / methanol
5: K2CO3 / N,N-dimethyl-acetamide
6: KOH / methanol
View Scheme

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