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N-acetylcystein
farnesyl bromide
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
With ammonia In methanol for 16h; | 99% |
With ammonia In methanol Alkylation; |
N-acetyl cysteine (S-farnesyl) methyl ester
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
With lithium hydroxide In methanol; water for 24h; | 84% |
trans,trans-farnesyl-L-cysteine
acetic anhydride
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
With sodium hydroxide at 0 - 20℃; | 52% |
Farnesol
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: polymer supported PPh3; CBr4 / CH2Cl2 / 5 h 2: 70 percent / zinc acetate; TFA / dimethylformamide; acetonitrile; H2O / 24 h 3: 84 percent / LiOH / methanol; H2O / 24 h View Scheme |
farnesyl bromide
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 70 percent / zinc acetate; TFA / dimethylformamide; acetonitrile; H2O / 24 h 2: 84 percent / LiOH / methanol; H2O / 24 h View Scheme |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With sodium hydroxide In water Stage #2: With titanium tetrachloride In tetrahydrofuran at 20℃; | 91% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With sodium hydroxide In water at 20℃; for 0.166667h; Stage #2: With silver nitrate In water for 1h; | 84% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
C20H35N3O2S
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine In dichloromethane for 0.5h; Stage #2: With hydrazine In tetrahydrofuran; dichloromethane at 20℃; for 3h; | 80% |
D-(+)-glucosamine hydrochloride
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With sodium hydroxide In ethanol; water Stage #2: D-(+)-glucosamine hydrochloride In ethanol; water for 0.5h; | 76% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
phenylhydrazine
C26H39N3O2S
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With triethylamine; HATU In tetrahydrofuran for 0.5h; Stage #2: phenylhydrazine In tetrahydrofuran | 73% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With sodium hydroxide In water at 20℃; for 0.166667h; Stage #2: With zinc(II) chloride In water for 1h; | 67% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
methylhydrazine
C21H37N3O2S
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With triethylamine; HATU In tetrahydrofuran for 0.5h; Stage #2: methylhydrazine In tetrahydrofuran | 65% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With sodium hydroxide In water Stage #2: With strontium chloride In water | 57% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
C20H34N2O3S
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine In dichloromethane for 0.5h; Stage #2: With hydroxylamine In tetrahydrofuran; dichloromethane; water at 20℃; for 3h; | 45% |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
acetic acid hydrazide
C22H37N3O3S
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With triethylamine; HATU In tetrahydrofuran for 0.5h; Stage #2: acetic acid hydrazide In tetrahydrofuran | 35% |
nicotinamide hydrochloride
N-acetyl-S-trans,trans-farnesyl-L-cysteine
nicotinamide (R)-2-acetamido-3-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)propanoate
Conditions | Yield |
---|---|
Stage #1: N-acetyl-S-trans,trans-farnesyl-L-cysteine With sodium hydroxide In water Stage #2: nicotinamide hydrochloride In ethanol for 1h; | 35% |
(R)-Phenylglycinol
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 20℃; |
Conditions | Yield |
---|---|
With 4-methyl-morpholine In tetrahydrofuran at -15℃; Acetylation; |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
N-[(R)-3-Diazo-2-oxo-1-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienylsulfanylmethyl)-propyl]-acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NMM / tetrahydrofuran / -15 °C 2: diethyl ether / 0 °C View Scheme |
N-acetyl-S-trans,trans-farnesyl-L-cysteine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NMM / tetrahydrofuran / -15 °C 2: diethyl ether / 0 °C 3: HCl / ethyl acetate / 0.17 h / 0 °C View Scheme |
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