CAS No.60-34-4,Methylhydrazine Suppliers

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Synthetic route

: 67-56-1
methanol

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With sodium tosylate; hydrazine hydrate; sodium hydrogensulfite at 75℃; for 4h; Temperature; Autoclave;	98.2%
With hydrazine hydro-chloride In water at 80 - 90℃; under 2250.23 - 3000.3 Torr; for 4h; Sealed tube;	40%
Stage #1: methanol With hydrazine dihydrochloride; hydrazine hydrochloride In water at 110℃; under 3000.3 Torr; Stage #2: With ethanolamine In water at 103 - 150℃;

: 5756-69-4
3-hydroxy-3-methyl-1-phenyl-1-triazene

A: 62-53-3
aniline

B: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With sodium acetate In methanol; water for 24h; Electrolysis;	A 81.45% B 78.02%

: 74-87-3
methylene chloride

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With hydrogenchloride; hydrazine hydrate In ethanol at 73℃; for 2.3h; Concentration; Temperature;	39.2%
Stage #1: methylene chloride With hydrazine hydrate at 80℃; under 3000.3 Torr; Stage #2: With ethanolamine at 90℃; Product distribution / selectivity;
With hydrogenchloride; hydrazine hydrate In water at 85℃;	99.3 g

: 186581-53-3, 908094-01-9
diazomethane

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With sodium amalgam; ethanol

: 1483-24-5
1-methyl-1-benzoylhydrazine

A: 21150-15-2
N,N'-dibenzoyl-N-methyl-hydrazine

B: 60-34-4
methylhydrazine

: 584-13-4
4-amino-1,2,4-triazole

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With acetic acid; zinc

: N-methyl-hydrazidosulfuric acid

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With hydrogenchloride

: 67-66-3
chloroform

A: 186581-53-3, 908094-01-9
diazomethane

B: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With potassium hydroxide; ethanol; hydrazine
With potassium hydroxide; hydrazine

: 4143-42-4
(Z)-azomethane

A: 50-00-0
formaldehyd

B: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With hydrogenchloride
With hydrogenchloride

: 684-93-5
1-methyl-1-nitrosourea

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With water; acetic acid; zinc ueber mehrere Stufen;

: 77-78-1
dimethyl sulfate

: 28867-76-7
benzaldehyde benzylidenehydrazone

A: (E,E)-dibenzylidenehydrazine; compound with dimethyl sulfate

B: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With benzene

...Expand

: 74-89-5
methylamine

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With sulfoperamic acid; water
With chloroamine
With sodium hydroxide; chloroamine In water at 25℃;
With chloroamine
With sodium hydroxide; sulfoperamic acid

: 74-88-4
methyl iodide

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With water; hydrazine hydrate

: 2257-52-5
N-isopropylhydrazine

: 107590-20-5
5-methylene-3,4,4-trimethyl-1-phenyl-2-pyrazoline

A: 107535-59-1
1-isopropyl-5-methylene-3,4,4-trimethyl-2-pyrazoline

B: 107590-19-2
1-phenyl-5-phenylhydrazino-3,4,4,5-tetramethyl-2-pyrazoline

C: 60-34-4
methylhydrazine

...Expand

: 30090-45-0
5-hydrazinomethyl-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-ol

A: 1210-35-1
10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one

B: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
In chlorobenzene for 24h; Heating;
at 200℃; Product distribution; reflux in chlorobenzene, 24 h.;

: 39885-14-8
N-Nitroso-N-methylmethoxymethylamine

A: 67-56-1
methanol

B: 124-40-3
dimethyl amine

C: 60-34-4
methylhydrazine

D: 74-89-5
methylamine

Conditions

Conditions	Yield
With hydrogenchloride; zinc In water Product distribution; Ambient temperature;	A 96 % Chromat. B 71 % Chromat. C 1 % Chromat. D 28 % Chromat.
With aluminum amalgam In water Product distribution; Ambient temperature;	A 102 % Chromat. B 40 % Chromat. C 24 % Chromat. D 48 % Chromat.
With potassium hydroxide; aluminium In water Product distribution; Ambient temperature;	A 109 % Chromat. B 25 % Chromat. C 35 % Chromat. D 54 % Chromat.

...Expand

: 39885-14-8
N-Nitroso-N-methylmethoxymethylamine

A: 67-56-1
methanol

B: 60-34-4
methylhydrazine

C: 74-89-5
methylamine

Conditions

Conditions	Yield
With titanium(III) chloride In water Product distribution; Ambient temperature;	A 110 % Chromat. B 100 % Chromat. C 30 % Chromat.

...Expand

: 5771-02-8
N-isopropylidene-N'-methylhydrazine

: 36016-40-7
mesitylenesulfonylhydroxylamine

A: 81549-07-7
acetone O-(2,4,6-trimethylphenylsulfonyl)oxime

B: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With triethylamine 1.) ether, 1 h, RT, 2.) ether; Yield given. Multistep reaction;

...Expand

: 100-63-0
phenylhydrazine

A: 107535-59-1
1-isopropyl-5-methylene-3,4,4-trimethyl-2-pyrazoline

B: 107590-19-2
1-phenyl-5-phenylhydrazino-3,4,4,5-tetramethyl-2-pyrazoline

C: 60-34-4
methylhydrazine

...Expand

: 598-50-5
N-Methylurea

A: 67-56-1
methanol

B: 36214-48-9
formaldehyde monomethylhydrazone

C: 57-14-7
1,1-dimethylhydrazine

D: 60-34-4
methylhydrazine

E: 1-methyltriazane

F: 2,3,4-triaza penta-1,3-diene

Conditions

Conditions	Yield
With chloroamine In diethyl ether; water for 5h; Product distribution; Mechanism; other solvent, exposition;

...Expand

: 186581-53-3, 908094-01-9
diazomethane

: 64-17-5
ethanol

sodium amalgam: sodium amalgam

: 60-34-4
methylhydrazine

...Expand

: 584-13-4
4-amino-1,2,4-triazole

: 64-19-7
acetic acid

zinc: zinc

: 60-34-4
methylhydrazine

...Expand

1,3,5-trinitro-<1,3,5>triazine: 1,3,5-trinitro-<1,3,5>triazine

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With sodium hydroxide; zinc

hydrochloride of hydrazinecarboxylic acid methyl ester: hydrochloride of hydrazinecarboxylic acid methyl ester

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
at 150 - 160℃;

: 74-89-5
methylamine

O-amino-sulfuric acid: O-amino-sulfuric acid

: 60-34-4
methylhydrazine

sodium methyl isodiazotate: sodium methyl isodiazotate

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
With aluminium durch Reduktion in alkal. Loesung;

: 74-89-5
methylamine

sulfoperamic acid: sulfoperamic acid

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
at 100℃; durch aequivalente Mengen Sulfoperamidsaeure; zu 43-46prozent in Methylhydrazin uebergefuehrt;

: 74-89-5
methylamine

diluted NaOH-solution: diluted NaOH-solution

sulfoperamic acid: sulfoperamic acid

: 60-34-4
methylhydrazine

Conditions

Conditions	Yield
at 100℃; durch aequivalente Mengen Sulfoperamidsaeure; erhaelt man in einer Ausbeute von 65prozent Methylhydrazin;

...Expand

: 57-14-7
1,1-dimethylhydrazine

A: 60-34-4
methylhydrazine

B CH, CN: CH, CN

Conditions

Conditions	Yield
With O(3P) under 2.02516E-08 Torr; emission of collisions product;

: 24424-99-5
di-tert-butyl dicarbonate

: 60-34-4
methylhydrazine

: 21075-83-2
1-methyl-1-tert-butoxycarbonylhydrazine

Conditions

Conditions	Yield
With sodium hydrogencarbonate In ethyl acetate at 0 - 20℃; for 3h;	100%
In dichloromethane at 0 - 20℃; for 3h;	100%
In dichloromethane	97%

: 115975-33-2
N,N-Dimethyl-2,4-bis(trifluoroacetyl)-1-naphthylamine

: 60-34-4
methylhydrazine

: 129602-64-8
2,2,2-Trifluoro-1-(2-methyl-3-trifluoromethyl-2H-benzo[g]indazol-5-yl)-ethanone

Conditions

Conditions	Yield
In chloroform for 18h; Heating;	100%

: 80099-81-6
3-benzoyl-2-chloro-pyridine

: 60-34-4
methylhydrazine

: 116834-95-8
1-methyl-3-phenyl-pyrazolo<3,4-b>pyridine

Conditions

Conditions	Yield
In ethanol for 10h; Heating;	100%

: 123532-14-9
N1-2-(2-hydroxybenzoyl)vinyl-N1-methylhydrazine

: 60-34-4
methylhydrazine

: 123532-18-3
3-(2-hydroxyphenyl)-1-methyl-1H-pyrazole

Conditions

Conditions	Yield
In ethanol for 48h;	100%

: 60-34-4
methylhydrazine

: 123532-15-0
N1-2-(2-hydroxy-5-methylbenzoyl)vinyl-N1-methylhydrazine

: 3-(2'-hydroxy-5'-methylphenyl)-1-methylpyrazole

Conditions

Conditions	Yield
In ethanol for 48h;	100%

: 60-34-4
methylhydrazine

: 123532-16-1
N1-2-(2-hydroxy-3-methylbenzoyl)vinyl-N1-methylhydrazine

: 123532-20-7
3-(2-hydroxy-3-methylphenyl)-1-methylpyrazole

Conditions

Conditions	Yield
In ethanol for 48h;	100%

: 60-34-4
methylhydrazine

: 7152-15-0
ethyl 4-methyl-3-oxo-pentanoate

: 31272-05-6
4,5-dihydro-1-methyl-3-isopropyl-5H-pyrazol-5-one

Conditions

Conditions	Yield
In tetrahydrofuran; ethanol at 0℃; for 36h; Inert atmosphere; Reflux;	100%
In ethanol for 18h; Heating;	99%

: 123-72-8
butyraldehyde

: 60-34-4
methylhydrazine

: N-butylidene-N'-methyl-hydrazine

Conditions

Conditions	Yield
With magnesium sulfate In dichloromethane Condensation;	100%

: 1193-21-1
4,6-dichloropyrimidine

: 60-34-4
methylhydrazine

: 618428-20-9
4,6-bis(1-methylhydrazino)pyrimidine

Conditions

Conditions	Yield
for 2h; Heating;	100%
for 2h; Inert atmosphere; Reflux;	86%
Reflux; Inert atmosphere;

: 60-34-4
methylhydrazine

: 21139-61-7
2-(4-methylphenyl)-4,6-dichloropyrimidine

: 618428-24-3
4,6-bis(1-methylhydrazino)-2-(1-methylphenyl)pyrimidine

Conditions

Conditions	Yield
for 2h; Heating;	100%

: 38109-77-2
3-amino-2-cyano-acrylic acid ethyl ester

: 60-34-4
methylhydrazine

: 31037-02-2
ethyl 5-amino-1-methyl-1H-pyrazole-4-carboxylate

Conditions

Conditions	Yield
at 80℃;	100%

: 141-97-9
ethyl acetoacetate

: 60-34-4
methylhydrazine

: 2749-59-9
1,3-dimethyl-5-pyrazolone

Conditions

Conditions	Yield
	100%
In ethanol at 0 - 60℃; for 16h; Inert atmosphere;	100%
at 40℃;	100%

: 60-34-4
methylhydrazine

: 641571-44-0
(2R,3R,4R,5R)-2-(2-amino-6-chloro-9H-purin-9-yl)-5-(benzoyloxymethyl)-3-methyltetrahydrofuran-3,4-diyl dibenzoate

: 915023-63-1
2-amino-6-(1-methylhydrazino)-9-(2',3',5'-tri-O-benzoyl-2'-methyl-β-D-ribofuranosyl)purine

Conditions

Conditions	Yield
In tetrahydrofuran at 45℃; for 0.0833333h;	100%
With TEA In tetrahydrofuran at 20℃; for 8h;

: 60-34-4
methylhydrazine

: 167412-38-6
2-anthracen-9-yl-4,6-dichloropyrimidine

: 2-(9-anthracenyl)-4,6-bis(1-methylhydrazino)pyrimidine

Conditions

Conditions	Yield
for 2h; Heating;	100%

: 905599-19-1
2-chloro-3-octadecyloxy-pyridine

: 60-34-4
methylhydrazine

: 905599-10-2
2-(1-methylhydrazino)-3-octadecyloxypyridine

Conditions

Conditions	Yield
for 26h; Heating;	100%

: 60-34-4
methylhydrazine

: 5759-75-1
6-chloro-3-phenylpyrimidine-2,4(1H,3H)-dione

: C11H14N4O2

Conditions

Conditions	Yield
In ethanol at 20℃; for 2.5h; Heating / reflux;	100%

: 87276-51-5
[2-(1,3-dioxo-1,3-dihydroisoindol-2-yloxy)-ethyl]carbamic acid tert-butyl ester

: 60-34-4
methylhydrazine

: 75051-55-7
(2-aminoxyethyl)carbamic acid tert-butyl ester

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 72h;	100%

: [6S/R,9R/S,11R/S]-2',3',4',5,5',6,7,8,9,10-decahydro-2-carboxaldehyde-5'-(2,2,2-trifluoroethyl)-spiro[6,9-methanobenzocyclooctene-11,3'-(1,2,5)thiadiazole]-1',1'-dioxide

: 60-34-4
methylhydrazine

: [6S/R,9R/S,11R/S]-2',3',4',5,5',6,7,8,9,10-decahydro-2-carboxaldehydemethylhydrazone-5'-(2,2,2-trifluoroethyl)-spiro[6,9-methanobenzocyclooctene-11,3'-(1,2,5)thiadiazole]-1',1'-dioxide

Conditions

Conditions	Yield
In tetrahydrofuran; diethyl ether at 20℃; for 1.5h;	100%

: 2946-39-6
8-bromoadenosine

: 60-34-4
methylhydrazine

: 2-[6-amino-8-(N'-methyl-hydrazino)-purin-9-yl]-5-hydroxymethyl-tetrahydro-furan-3,4-diol

Conditions

Conditions	Yield
In DMF (N,N-dimethyl-formamide) at 85℃; for 3h;	100%

: 10591-23-8
2-formyl-4,5-dimethyl-pyrrole-3-carboxylic acid ethyl ester

: 60-34-4
methylhydrazine

: 183170-57-2
2,3,5-Trimethyl-1H-pyrrolo[2,3-d]pyridazin-4(5H)-one

Conditions

Conditions	Yield
With sulfuric acid In ethanol	100%

: 57-71-6, 17019-25-9, 110828-81-4
2,3-Butanedione monoxime

: 60-34-4
methylhydrazine

: 3-(methyl-hydrazono)-butan-2-one oxime

Conditions

Conditions	Yield
In ethanol at 20 - 80℃; for 53h;	100%

: 40138-16-7
2-formylbenzene boronic acid

: 60-34-4
methylhydrazine

: 101942-82-9
(C7H5N2BC6H5)2O

Conditions

Conditions	Yield
	100%

: 956111-57-2
3-acetyl-4-methoxy-1-methyl-2(1H)-quinolinone

: 60-34-4
methylhydrazine

: 1062227-76-2
2,3,5-trimethyl-2,5-dihydro-4H-pyrazolo[4,3-c]quinolin-4-one

Conditions

Conditions	Yield
In ethanol for 3h; Heating;	100%

: 58966-24-8
2-(chloromethyl)-4-nitrotoluene

: 60-34-4
methylhydrazine

: 1101120-82-4
1-methyl-1-(2-methyl-5-nitrobenzyl)hydrazine

Conditions

Conditions	Yield
In ethanol for 1h; Reflux;	100%
Stage #1: 2-(chloromethyl)-4-nitrotoluene; methylhydrazine In ethanol for 1h; Heating / reflux; Stage #2: With sodium hydroxide; water In dichloromethane	100%