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Wuhan Jadechem International Trade Co.,Ltd.

1.Our own factory in Yingcheng, Hubei province, China. It has strong production capacity, perfect equipments, advanced technique and complete quality supervision system. Welcome to visit our factory at any convenient time for business or coope

3-Prop-2-ynoxypropane-1,2-diol POPDH

Cas:13580-38-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Hangzhou Think Chemical Co. Ltd

3-Prop-2-ynoxypropane-1,2-diol (POPDH), CAS No.:13580-38-6 Name 3-Prop-2-ynoxypropane-1,2-diol Synonyms 3-(2-Propynyloxy)propane-1,2-diol; Propargyl-oxo-propane-2,3-dihy

3-Prop-2-ynoxypropane-1,2-diol (POPDH), CAS No.:13580-38-6

Cas:13580-38-6

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Other

inquiry

Henan Allgreen Chemical Co.,Ltd

Good price Good quality Appearance:powder Storage:dry condition Package:According to the demand of customer Application:intermediate Transportation:By sea or by air Port:Shanghai Port

13580-38-6, 3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Gram

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Popdh 50%

Cas:13580-38-6

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality Oled CAS 13580-38-6 1,2-Propanediol,3-(2-propyn-1-yloxy)-

Cas:13580-38-6

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

1-Propargyl glycerol ether

Cas:13580-38-6

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Trading Company

inquiry

Leader Biochemical Group

About Product Details

China Biggest factory Supply High Quality 3-Prop-2-ynoxypropane-1,2-diol CAS 13580-38-6

Cas:13580-38-6

Min.Order:1 Kilogram

FOB Price: $3.0 / 5.0

Type:Lab/Research institutions

inquiry

Henan Sinotech Import&Export Corporation

Chemical Name POPDH Synonyms 3-(2-Propynyloxy)propane-1,2-diol; Propargyl-oxo-propane-2,3-dihydroxy; 3-Prop-2-ynoxypropane-1,2-diol CAS No. 13580-38-6

3-(2-Propynyloxy)propane-1,2-diol

Cas:13580-38-6

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,2-Propanediol,3-(2-propyn-1-yloxy)- 13580-38-6

Cas:13580-38-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

3-Prop-2-ynoxypropane-1,2-diol CAS:13580-38-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or

3-Prop-2-ynoxypropane-1,2-diol CAS:13580-38-6

Cas:13580-38-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,2-Propanediol,3-(2-propyn-1-yloxy)-

Cas:13580-38-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

HUBEI RISON CHEMICAL CO.,LTD.

Located in Wuhan City of Hubei Province, Wuhan Rison Trading co., Ltd is engaged in the supply of fine specialty chemicals. Our business includes metal surface treatment, such as nickel/zinc/copper plating, perfluoro chemicals, tin salts (stannous su

Hiigh quality/ Propargyl-oxo-propane-2,3-dihydroxy

Cas:13580-38-6

Min.Order:3000 Kilogram

Negotiable

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,2-Propanediol,3-(2-propyn-1-yloxy)-

Cas:13580-38-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Price, service, company and transport advantage : 1. best service, high quality and reasonable price 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's customers' r

Beat price/3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

POPDH 50%

Cas:13580-38-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Wuhan Kemi-Works Chemical Co., Ltd

Propargyl-oxo-propane-2, 3-dihydroxy CAS No 13580-38-6 Molecular Formular C6H10O3 Molecular weight 130.14 Assay 50%min Appearance Clear colorless liquid Density g/cm3 (20℃) 1.06~1.11… Superiority 1.Powerful R & D team

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

POPS 30290-53-0 Propargyl-3-sulfopropyl ether sodium salt

Cas:13580-38-6

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 3-Prop-2-ynoxypropane-1,2-diol CAS: 13580-38-6 MF: C6H10O3 MW: 130.14 EINECS: 237-012-2 Product Categories: Mol File: 13580-38-6.mol 3-Prop-2-ynoxypropane-1,2-diol Structure 3-Prop-2-ynoxypropane-1,2-diol Chemical

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

3-Prop-2-ynoxypropane-1,2-diol

Cas:13580-38-6

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Synthetic route

prop-2-ynyloxymethyl-oxirane
18180-30-8

prop-2-ynyloxymethyl-oxirane

3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

Conditions
ConditionsYield
With water at 100℃;96%
propargyl bromide
106-96-7

propargyl bromide

(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol
100-79-8

(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

Conditions
ConditionsYield
Stage #1: propargyl bromide; (R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol With sodium hydride In tetrahydrofuran Reflux;
Stage #2: With hydrogenchloride In tetrahydrofuran; methanol; water at 20℃; for 8h;
90%
4-(prop-2-yn-1-yloxymethyl)-2,2-dimethyl-1,3-dioxolane

4-(prop-2-yn-1-yloxymethyl)-2,2-dimethyl-1,3-dioxolane

3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

Conditions
ConditionsYield
With hydrogenchloride In tetrahydrofuran at 20℃;75%
With hydrogenchloride; water In tert-butyl methyl ether at 20 - 25℃; for 6h; Inert atmosphere; Industry scale;85 %Chromat.
With methanol
oxiranyl-methanol
556-52-5

oxiranyl-methanol

propargyl alcohol
107-19-7

propargyl alcohol

3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

Conditions
ConditionsYield
In N,N-dimethyl-formamide51%
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

1,2-di-O-tert-butyldimethylsilyl-3-(prop-2-yn-1-yloxy)propan-1,2-diol

1,2-di-O-tert-butyldimethylsilyl-3-(prop-2-yn-1-yloxy)propan-1,2-diol

Conditions
ConditionsYield
With 1H-imidazole In N,N-dimethyl-formamide80%
sodium hypochlorite
7681-52-9

sodium hypochlorite

3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

3-(2,3,3-triiodo-2-propenyloxy)-propane-1,2-diol

3-(2,3,3-triiodo-2-propenyloxy)-propane-1,2-diol

Conditions
ConditionsYield
With sodium hydroxide; Ki; aqueous H2SO4 In water76%
With sodium hydroxide; Ki; aqueous H2SO4 In water76%
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

4‐((prop‐2‐yn‐1‐yloxy)methyl)‐1,3‐dioxolan‐2‐one
949015-02-5

4‐((prop‐2‐yn‐1‐yloxy)methyl)‐1,3‐dioxolan‐2‐one

Conditions
ConditionsYield
With tetrabutylammomium bromide at 180℃; under 8250.83 Torr; for 0.05h; Flow reactor;69%
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

trityl chloride
76-83-5

trityl chloride

1-(prop-2-yn-1-yloxy)-3-(trityloxy)propan-2-ol

1-(prop-2-yn-1-yloxy)-3-(trityloxy)propan-2-ol

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;66%
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-hexadecylcarboxylic acid
57-10-3

1-hexadecylcarboxylic acid

(2,3-dihexadecanoyl)-(1-propargyloxy)propionate

(2,3-dihexadecanoyl)-(1-propargyloxy)propionate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 0 - 20℃; for 16h; Steglich Esterification;51%
lauric acid
143-07-7

lauric acid

3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

(2,3-didodecanoyl)-(1-propargyloxy)propionate

(2,3-didodecanoyl)-(1-propargyloxy)propionate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 0 - 20℃; for 16h; Steglich Esterification;48%
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

3-(2,3-diiodo-2-propenyloxy)-propane-1,2-diol

3-(2,3-diiodo-2-propenyloxy)-propane-1,2-diol

Conditions
ConditionsYield
With I2; Ki In water
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

2-(prop-2-yn-1-yloxy)acetaldehyde
801294-16-6

2-(prop-2-yn-1-yloxy)acetaldehyde

Conditions
ConditionsYield
With sodium periodate; water at 10 - 25℃; pH=~ 7; Inert atmosphere; Industry scale;
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-(prop-2-yn-1-yloxy)-3-(trityloxy)propan-2-one

1-(prop-2-yn-1-yloxy)-3-(trityloxy)propan-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: dipyridinium dichromate / dichloromethane / 20 °C / Molecular sieve
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-hydroxy-3-(prop-2-yn-1-yloxy)propan-2-one

1-hydroxy-3-(prop-2-yn-1-yloxy)propan-2-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: dipyridinium dichromate / dichloromethane / 20 °C / Molecular sieve
3: trifluoroacetic acid / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-{2-[2-(2-hydroxyethoxy)ethoxy]ethyl}-4-{[(1,2-didodecanoyloxy-carbonyl)propyloxy]methoxy}-1,2,3-triazole

1-{2-[2-(2-hydroxyethoxy)ethoxy]ethyl}-4-{[(1,2-didodecanoyloxy-carbonyl)propyloxy]methoxy}-1,2,3-triazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C
2: copper(I) bromide; N,N,N',N'',N'''-pentamethyldiethylenetriamine / N,N-dimethyl-formamide; dichloromethane / 16 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-{2-[2-(2-(β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-di-dodecanoyloxycarbonyl)propyloxy]methoxy}-1,2,3-triazole

1-{2-[2-(2-(β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-di-dodecanoyloxycarbonyl)propyloxy]methoxy}-1,2,3-triazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C
2: copper(I) bromide; N,N,N',N'',N'''-pentamethyldiethylenetriamine / N,N-dimethyl-formamide; dichloromethane / 16 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-{2-[2-(2-(β-D-galactopyranosyl-(1→4)β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-didodecanoyloxycarbonyl)propyloxy]methoxy}-1,2,3-triazole

1-{2-[2-(2-(β-D-galactopyranosyl-(1→4)β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-didodecanoyloxycarbonyl)propyloxy]methoxy}-1,2,3-triazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C
2: copper(I) bromide; N,N,N',N'',N'''-pentamethyldiethylenetriamine / N,N-dimethyl-formamide; dichloromethane / 16 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-{2-[2-(2-hydroxyethoxy)ethoxy]ethyl}-4-{[(1,2-dihexadecanoyloxy-carbonyl)propyloxy]methoxy}-1,2,3-triazole

1-{2-[2-(2-hydroxyethoxy)ethoxy]ethyl}-4-{[(1,2-dihexadecanoyloxy-carbonyl)propyloxy]methoxy}-1,2,3-triazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C
2: copper(I) bromide; N,N,N',N'',N'''-pentamethyldiethylenetriamine / N,N-dimethyl-formamide; dichloromethane / 16 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-{2-[2-(2-(β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-di-hexadecanoyloxycarbonyl)propyloxy]methoxy}-1,2,3-triazole

1-{2-[2-(2-(β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-di-hexadecanoyloxycarbonyl)propyloxy]methoxy}-1,2,3-triazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C
2: copper(I) bromide; N,N,N',N'',N'''-pentamethyldiethylenetriamine / N,N-dimethyl-formamide; dichloromethane / 16 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1-{2-[2-(2-(β-D-galactopyranosyl-(1→4)β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-dihexadecanoyloxycarbonyl)propyl-oxy]methoxy}-1,2,3-triazole

1-{2-[2-(2-(β-D-galactopyranosyl-(1→4)β-D-glucopyranosyloxy)ethoxy)ethoxy]ethyl}-4-{[(1,2-dihexadecanoyloxycarbonyl)propyl-oxy]methoxy}-1,2,3-triazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C
2: copper(I) bromide; N,N,N',N'',N'''-pentamethyldiethylenetriamine / N,N-dimethyl-formamide; dichloromethane / 16 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1,3-di-[1-(4-deoxypodophyllotoxin-4β-yl)-1,2,3-triazol-4-yl-methoxy]-propan-2-ol

1,3-di-[1-(4-deoxypodophyllotoxin-4β-yl)-1,2,3-triazol-4-yl-methoxy]-propan-2-ol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide
2.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Reflux
4.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 4 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1,3-di-[1-(4-deoxy-4′-demethylpodophyllotoxin-4β-yl)-1,2,3-triazol-4-yl-methoxy]-propan-2-ol

1,3-di-[1-(4-deoxy-4′-demethylpodophyllotoxin-4β-yl)-1,2,3-triazol-4-yl-methoxy]-propan-2-ol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide
2.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Reflux
4.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 4 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

2-O-tert-butyldimethylsilyl-3-(prop-2-yn-1-yloxy)propan-1,2-diol

2-O-tert-butyldimethylsilyl-3-(prop-2-yn-1-yloxy)propan-1,2-diol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1H-imidazole / N,N-dimethyl-formamide
2: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

2-O-tert-butyldimethylsilyl-1,3-di-(prop-2-yn-1-yloxy)propan-1,2-diol

2-O-tert-butyldimethylsilyl-1,3-di-(prop-2-yn-1-yloxy)propan-1,2-diol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide
2.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Reflux
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1,3-bis(prop-2-yn-1-yloxy)propane-2-ol
16169-22-5

1,3-bis(prop-2-yn-1-yloxy)propane-2-ol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide
2.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Reflux
4.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1,3-di-(prop-2-yn-1-yloxy)prop-2-yl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

1,3-di-(prop-2-yn-1-yloxy)prop-2-yl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide
2.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Reflux
4.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1,3-di-(prop-2-yn-1-yloxy)prop-2-yl β-D-glucopyranoside

1,3-di-(prop-2-yn-1-yloxy)prop-2-yl β-D-glucopyranoside

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide
2.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Reflux
4.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere
6.1: sodium methylate / methanol
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

1,3-di-(prop-2-yn-1-yloxy)prop-2-yl 2,3,4,6-tetra-O-butyryl-β-D-glucopyranoside

1,3-di-(prop-2-yn-1-yloxy)prop-2-yl 2,3,4,6-tetra-O-butyryl-β-D-glucopyranoside

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide
2.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Reflux
4.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere
6.1: sodium methylate / methanol
7.1: pyridine / 12 h / 0 - 20 °C
View Scheme
3-(prop-2-yn-1-yloxy)propan-1,2-diol
13580-38-6

3-(prop-2-yn-1-yloxy)propan-1,2-diol

stearic acid
57-11-4

stearic acid

C24H44O4

C24H44O4

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

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